Preparation method for rose extract and cosmetic

A technology for rose flower extract and cosmetics, which is applied in the field of preparation of rose flower extract, can solve the problems of colorless rose water, destruction of effective components of petals, easy pigment dissolution, etc., and achieves high activity of functional components and good market prospects. Effect

Active Publication Date: 2013-01-30
GUANGZHOU RIDGEPOLE BIOLOGICAL TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The rose water obtained by this method has the following problems: (1) the active ingredient content is small, only part of the water-soluble ingredients enter the rose water, and most of the active ingredients remain in the rose residue; (two) the active ingredients are low in activity, Most of the active ingredients in the petals are heat-sensitive, and high temperature and high pressure for a long time will destroy the heat-sensitive ingredients in the petals; (3) Most of the rose water is colorless and has no natural rose color. Add it to cosmetics, if necessary To achieve the rose color, additional pigments need to be added; (4) Rose flower water has a cooking smell. Due to long-term high-temperature distillation, the flower water has an acidic cooking smell. Adding it to the product will affect the fragrance of the product, which needs to be processed by essence, etc. adjust
[0006] The specific problems are: 1. Fresh roses are used as raw materials and added to products through pasteurization pretreatment. The disadvantages are that it is easy to cause color fading, loss of nutrients and changes in shape, which affects the desire to buy. Artificial pigme

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0031] The extraction process of embodiment 1 fresh rose petals

[0032] a Rose petal extraction process: selection

[0033] At room temperature below 15°C, fresh roses are removed from calyxes, stamens, and residual petals, and impurities such as leaves, flower insects, and flower branches are removed. The time for choosing a workshop should not exceed 2 hours.

[0034] to clean

[0035] When the room temperature is below 15°C, pour the picked rose petals into a cleaning tank with a water temperature of 10-15°C, put 5 petals in each tank, put the petals into the sieve tray for half a minute after submerging in the water, and drain the water. The whole process takes no more than 2 hours.

[0036] color protection

[0037] Pour 1 volume of cleaned petals into 1 volume of color protection solution, the content of citric acid in the color protection solution is 3%, the content of magnesium chloride is 3%, soak for 3 hours, soak at a temperature below 10°C, remove aft...

Embodiment 2

[0056] Example 2 Extraction process of dried rose petals

[0057] Dried rose petals need to be rehydrated before the extraction process, and then enzymatically hydrolyzed according to the enzymatic hydrolysis process of fresh rose petals.

[0058] Refining

[0059] Mix the dried rose petals and deionized water at a ratio of 1:10 (w / w), adjust the mixture to PH=5.0 with citric acid, put it into a colloid mill, and carry out the colloid mill at a temperature below 10°C.

[0060] extract

[0061] Add the feed liquid into the enzyme reactor, the enzymatic hydrolysis temperature is 48°C, pH=5.0, the amount of cellulase added is 0.02% of the weight of the feed liquid, the amount of pectinase added is 0.04% of the weight of the feed liquid, and the enzymatic hydrolysis time 1.5h. Enzyme inactivation parameters were raised to 82°C in a water bath for 6 min, and then cooled rapidly.

[0062] centrifugal

[0063] Centrifuge the mixture in a centrifuge at 10°C, 8000r / min for 1...

Embodiment 3

[0072] Example 3 The color protection / shape protection technology of rose petals

[0073] In the present invention, no matter fresh rose petals or dried rose petals, they are preferably treated with color-protecting and / or shape-protecting processes, and the specific steps are as follows.

[0074] excerpt

[0075] At room temperature below 15°C, fresh roses are removed from calyxes, stamens, and residual petals, and impurities such as leaves, flower insects, and flower branches are removed. The time for choosing a workshop should not exceed 2 hours.

[0076] b. Cleaning

[0077] When the room temperature is below 15°C, pour the picked rose petals into a cleaning tank with a water temperature of 10-15°C, put 5 petals in each tank, put the petals into the sieve tray for half a minute after submerging in the water, and drain the water. The whole process takes no more than 2 hours.

[0078] c. Color protection

[0079] Pour 1 volume of cleaned petals into 1 volume of color ...

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Abstract

The invention relates to a preparation method for rose extract. The preparation method comprises the following steps of: (a) mixing dry roseleaves or enzyme-inactivated fresh roseleaves with deionized water; regulating potential of hydrogen (pH) to 4.5-5.5; and grinding to obtain feed liquid; (b) adding the feed liquid obtained in the step (a) to an enzyme reactor; adding cellulase accounting for 0.02-0.05 percent of the weight of the feed liquid and pectinase accounting for 0.02-0.04 percent of the weight of the feed liquid; performing enzymolysis for 0.5-1.5 hours at the temperature of 45-50 DEG C at the pH of 4.5-5.5; and then, inactivating enzymes to obtain mixed feed liquid; (c) centrifuging the mixed feed liquid obtained in the step (b), and fetching supernate; (d) filtering the supernate by using a membrane to obtain filtrate; and (e) adding tea polyphenol to the filtrate, sterilizing and packaging. According to the preparation method for the rose extract, cell walls of the roses are broken by adopting the enzymolysis technology to enable active principles to be released from the cells, and moreover, the rose color and flavor are kept. Meanwhile, polysaccharide generated by proper enzymolysis also has a certain cosmetic effect. Moreover, the invention provides a cosmetic containing roseleaf and rose extracts and the tea polyphenol.

Description

technical field [0001] The invention relates to a process for extracting roses, in particular to a method for preparing rose extracts and cosmetics containing the extracts. Background technique [0002] At present, the world's cosmetics market tends to add pure natural raw materials, and cosmetics made of rose extracts are also called biological cosmetics. gaze. The annual increase rate of national demand for rose cosmetics is more than 12%, and the potential in the international market is also great. Therefore, the development of rose cosmetics has a broad market prospect. [0003] In terms of the realization of the functional ingredients of roses, it is generally achieved by adding rose essential oil and rose water. Rose water is a by-product of rose essential oil extraction. The production process of rose water is generally to put fresh roses into a distillation tank , steam heating and pressure distillation, the steam after distillation is cooled and condensed to form...

Claims

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Application Information

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IPC IPC(8): A61K8/97A61Q19/00A61Q19/10
Inventor 曾飒殷露琴钟娜蔡波唐新明
Owner GUANGZHOU RIDGEPOLE BIOLOGICAL TECH CO LTD
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