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Preparation method of WGM (whispering gallery mode) ZnO ultraviolet micro-laser for constructing electric pump

A micro-laser, whispering gallery mode technology, applied in the structural details of semiconductor lasers, lasers, laser parts and other directions, can solve the problems of laser loss, sacrificing carrier concentration, etc., achieve small optical loss, good electrical contact, improve Effects of lasing and transmittance

Inactive Publication Date: 2013-01-30
SOUTHEAST UNIV
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  • Abstract
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  • Claims
  • Application Information

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Problems solved by technology

However, due to the opacity of the metal electrode, the laser will cause a lot of loss when it is emitted.
Using transparent conductive films (such as: indium tin oxide (ITO), zinc aluminum oxide (ZAO), etc.) as electrodes, although the light transmittance is enhanced, the carrier concentration is sacrificed

Method used

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  • Preparation method of WGM (whispering gallery mode) ZnO ultraviolet micro-laser for constructing electric pump
  • Preparation method of WGM (whispering gallery mode) ZnO ultraviolet micro-laser for constructing electric pump
  • Preparation method of WGM (whispering gallery mode) ZnO ultraviolet micro-laser for constructing electric pump

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Embodiment Construction

[0031] The preparation method of constructing the electrically pumped whispering gallery mode ZnO ultraviolet micro-laser of the present invention is:

[0032]Step 1: Mix and grind ZnO powder and carbon powder with a purity of 99.99% at a mass ratio of 1:1 to 1:2.5, and fill 0.3 to 0.5 grams of the mixture into a ceramic boat. The silicon wafer with an area close to the opening area of ​​the ceramic boat was ultrasonically cleaned with acetone, absolute ethanol and deionized water in sequence, then blown dry with nitrogen, and covered the silicon wafer with the polished side down on the ceramic boat. The ceramic boat is then pushed into a tube furnace at a temperature of 1000-1200 degrees Celsius. After 30-40 minutes of reaction, ZnO microrod arrays grow on the surface of the silicon wafer (see figure 1 ), a single ZnO microrod is the crystal structure of hexagonal wurtzite (see figure 1 illustration in ).

[0033] The second step: the buffer layer is divided into two types...

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Abstract

The invention discloses a preparation method of a WGM (whispering gallery mode) ZnO ultraviolet micro-laser for constructing an electric pump. The method comprises the following steps of: preparing a ZnO micro bar single crystal by utilizing a gas phase transmission method or a hydrothermal method; then transferring a single ZnO micro bar onto p-type gallium nitride (GaN) with a buffer layer; processing the buffer layer so as to form a good-contact hetero junction between the ZnO micro bar and the p-type GaN; preparing a layer of insulation film on the surface of the hetero junction; etching out the surface of the ZnO micro bar by utilizing a reactive ion etching or photetching technology; transferring graphene onto the ZnO micro bar so as to enable the graphene to be in good contact with the ZnO micro bar; and finally preparing a metal electrode on the surface of the p-type GaN so as to constitute a complete graphene / n-type ZnO micro bar / p-type GaN hetero junction micro-laser. The micro-laser prepared by the method utilizes the high carrier concentration and high light transmittance of the graphene, so that high-quality ultraviolet laser output can be realized.

Description

technical field [0001] The present invention is designed to prepare high-quality single crystal ZnO microrods by gas phase transport method or hydrothermal method, separate a single ZnO microrod and combine it with p-type GaN with a buffer layer, and form a A pn junction with good contact, then sputtering a layer of inorganic transparent insulating film on its surface, then using reactive ion etching or photolithography to expose the surface of ZnO microrods, and finally transferring graphene to the surface of ZnO microrods as electrodes, and Electrodes are prepared on the surface of p-type GaN to form a complete device. The luminescent pn junction obtained by the above method and process flow can obtain high-quality electrically pumped ultraviolet whispering gallery mode laser light. Background technique [0002] Since Japanese scientists and American scientists successively discovered the ultraviolet radiation in ZnO films and nanowires, ZnO has become an ideal material f...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): H01S5/32H01S5/327H01S5/02
Inventor 徐春祥朱刚毅理记涛田正山石增良
Owner SOUTHEAST UNIV
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