Energy-saving evaporation treatment process of high-salinity wastewater

A high-salt wastewater treatment technology, applied in the direction of heating water/sewage treatment, adsorption water/sewage treatment, water/sewage multi-stage treatment, etc., can solve the problems of high production cost, difficult to meet the waste water standard, difficult to effectively use, etc. Achieve the effects of small footprint, short processing flow and remarkable energy saving effect

Active Publication Date: 2013-11-13
山东大明消毒科技有限公司
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  • Application Information

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Problems solved by technology

[0003] At present, the commonly used treatment methods are multi-effect evaporation followed by flaking with a flaker or spray granulation followed by drying in a fluidized bed. However, these methods often consume a large amount of energy such as steam, electricity or coal, and the production cost is high. , and the final evaporated inorganic salts often contain crystal water, which has high impurity content and is difficult to effectively use, and the final discharged wastewater is also difficult to meet the standard

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  • Energy-saving evaporation treatment process of high-salinity wastewater
  • Energy-saving evaporation treatment process of high-salinity wastewater

Examples

Experimental program
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Effect test

Embodiment 1

[0045] Example 1 Taking the wastewater containing ammonium chloride produced in the production process of potassium dihydrogen phosphate as an example, the specific treatment process is as follows:

[0046] ① Evaporation system: 500kg of ammonium chloride wastewater with a concentration of 10% ammonium chloride treated by the sewage treatment system is passed into the raw material tank, and then sent to the primary preheater and secondary preheater in turn for graded preheating , after graded preheating, it is transported to the evaporator, and heated and evaporated at 30°C to obtain an ammonium chloride evaporation liquid with a concentration of 25%;

[0047] ② Concentration system: The ammonium chloride evaporation liquid enters the first storage tank and is stored after being removed by the adsorption layer. The adsorption layer is supported by the upper and lower grid plates. The activated coal gangue in the adsorption layer weighs 5kg. The stored ammonium chloride evaporat...

Embodiment 2

[0053] Embodiment 2 Taking the wastewater containing sodium chloride produced in the epoxy resin production process as an example, the specific treatment process is as follows:

[0054] ① Evaporation system: 1 ton of sodium chloride wastewater with a sodium chloride concentration of 18% treated by the sewage treatment system is passed into the raw material tank, and then sent to the primary preheater and secondary preheater in turn for graded preheating , after graded preheating, it is transported to the evaporator, and heated and evaporated at 100°C to obtain a sodium chloride evaporation liquid with a concentration of 35%;

[0055] ② Concentration system: The sodium chloride evaporation liquid enters the first storage tank and is stored after being removed by the adsorption layer. The adsorption layer is supported by upper and lower grid plates. The activated coal gangue in the adsorption layer weighs 20kg. The stored sodium chloride evaporates The liquid is transported to t...

Embodiment 3

[0061] Embodiment 3 Taking the waste water containing calcium chloride produced in the sodium dichloroisocyanurate production process as an example, the specific treatment process is as follows:

[0062] ① Evaporation system: 2 tons of calcium chloride wastewater with a calcium chloride concentration of 14% treated by the sewage treatment system is passed into the raw material tank, and then sent to the primary preheater and secondary preheater in turn for graded preheating , after graded preheating, it is transported to the evaporator, and heated and evaporated at 65°C to obtain a calcium chloride evaporation liquid with a concentration of 30%;

[0063] ②Concentration system: Calcium chloride evaporation liquid enters the first storage tank and is stored after being removed by the adsorption layer. The adsorption layer is supported by upper and lower grid plates. The activated coal gangue in the adsorption layer weighs 30kg. The stored calcium chloride evaporates The liquid i...

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Abstract

The invention provides an energy-saving evaporation treatment process of high-salinity wastewater. The energy-saving evaporation treatment process comprises an evaporating system, a concentrating system, a drying system and a heat circulating system. Grading preheating, heating evaporation, adsorption purification, concentration, adsorption purification and high-temperature drying are successively carried out on the high-salinity wastewater treated by a wastewater treatment system to obtain the finished product of inorganic salt, heat exhausted in the evaporation, concentration and drying processes is recycled, and wastewater is discharged. By adopting the technical scheme, wastewater discharged finally meets the national industrial wastewater discharge standard, the purity of the obtained inorganic salt is as high as 99.3%, and the energy-saving effect is remarkable.

Description

technical field [0001] The invention belongs to the technical field of industrial wastewater treatment, and in particular relates to an energy-saving evaporation treatment process for high-salt wastewater. Background technique [0002] The wastewater discharged during industrial production often contains high concentrations of inorganic salts, especially the by-products of inorganic salts in the chemical production process or the large amount of inorganic salts produced by neutralizing the pH of the solution, which will lead to higher concentrations of inorganic salts in the final discharged wastewater. High-salt wastewater has the characteristics of large discharge, strong toxicity and high difficulty in treatment. [0003] At present, the commonly used treatment methods are multi-effect evaporation followed by flaking with a flaker or spray granulation followed by drying in a fluidized bed. However, these methods often consume a large amount of energy such as steam, electr...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C02F9/10C01F11/30C01C1/16C01D3/06C01D5/18C02F1/28C02F1/04
Inventor 邵长银李成顺侯贺义程明峰
Owner 山东大明消毒科技有限公司
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