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Textile anti-pilling polyurethane finishing agent and preparation method thereof

A polyurethane finishing agent and anti-pilling technology, which is applied in the fields of textiles and papermaking, fiber treatment, animal fibers, etc., can solve the problems such as polypropylene carbonate polyol type anti-pilling polyurethane, etc., and achieve good Effects of hand feeling, improvement of wet rubbing fastness, and improvement of durability

Active Publication Date: 2013-06-12
库尔勒汇同泰印染科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, there are no research reports and application examples of polypropylene carbonate polyol type anti-pilling polyurethane finishing.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0056] The anti-pilling polyurethane finishing agent for textiles of the present invention is composed of the following raw materials by mass percentage: 13.4% of polypropylene carbonate polyol, 4.5% of isophorone diisocyanate, 0.023% of dibutyltin dilaurate, and dihydroxypropyl Acid 0.9%, acetone 2.727%, amino silicone oil 8.15%, triethylamine 0.7%, deionized water 69.6%, the total content of the above components is 100%;

[0057] Add the weighed polypropylene carbonate polyol into a reaction vessel connected with a stirring device, raise the temperature of the polypropylene carbonate polyol in the reaction vessel to 100°C, and then vacuumize the polypropylene carbonate polyol Dehydration treatment, the treatment time is 40min. After the vacuum dehydration treatment is completed, the polypropylene carbonate polyol is cooled to 30°C to obtain the dehydrated polypropylene carbonate polyol; then the weighed isophorone di Isocyanate IPDI and dibutyltin dilaurate were added to the...

Embodiment 2

[0061] The anti-pilling polyurethane finishing agent for textiles of the present invention consists of the following raw materials by mass percentage: 21.3% of polypropylene carbonate polyol, 0.036% of dibutyltin dilaurate, 10.2% of isophorone diisocyanate, and dihydroxypropyl Acid 1.864%, isopropanol 2.1%, amino silicone oil 3.7%, triethylamine 1.2%, deionized water 59.6%, the total content of the above components is 100%;

[0062] Add the weighed polypropylene carbonate polyol into a reaction vessel connected with a stirring device, raise the temperature of the polypropylene carbonate polyol in the reaction vessel to 110°C, and then vacuumize the polypropylene carbonate polyol Dehydration treatment, the treatment time is 30min. After the vacuum dehydration treatment is completed, the polypropylene carbonate polyol is cooled to 40°C to obtain the dehydrated polypropylene carbonate polyol; then the weighed isophorone di Isocyanate IPDI and dibutyltin dilaurate were added to th...

Embodiment 3

[0066] The anti-pilling polyurethane finishing agent for textiles of the present invention is composed of the following raw materials by mass percentage: 13.9% of polypropylene carbonate polyol, 0.014% of dibutyltin dilaurate, and 5.786% of 4,4-diphenylmethane diisocyanate , dihydroxypropionic acid 1.56%, N-methylpyrrolidone 2.78%, amino silicone oil 5.32%, triethylamine 1.04%, deionized water 69.6%, the total content of the above components is 100%;

[0067] Add the weighed polypropylene carbonate polyol into a reaction vessel connected with a stirring device, raise the temperature of the polypropylene carbonate polyol in the reaction vessel to 120°C, and then vacuumize the polypropylene carbonate polyol Dehydration treatment, the treatment time is 20min. After the vacuum dehydration treatment is completed, the polypropylene carbonate polyol is cooled to 50°C to obtain the dehydrated polypropylene carbonate polyol; then the weighed isophorone di Isocyanate IPDI and dibutyltin...

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PUM

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Abstract

The invention discloses textile anti-pilling polyurethane finishing agent. The textile anti-pilling polyurethane finishing agent is made by the reaction of the following raw materials on a mass percent basis: 11.74-21.3% of polypropylene carbonate polyhydric alcohol, 3.81-10.2% of diisocyanate, 0.014-0.036% of catalyst, 0.9-1.864% of chain extender, 2.1-2.78% of organic solvent, 3.7-8.2% of amino silicon oil, 0.7-1.19% of neutralizer and 59.6-70.5% of deionized water, and the total content of the components is 100%. The invention further relates to a preparation method of the finishing agent, and the preparation method includes the steps of weighing the raw materials, preparing polyurethane prepolymers, preparing amino silicon oil grafting modification polyurethane, and finally adding the deionized water and the neutralizer into the amino silicon oil grafting modification polyurethane to obtain the finishing agent. The finishing agent can improve the anti-pilling property of textile and enable the textile to be soft.

Description

technical field [0001] The invention belongs to the technical field of polymer material synthesis and application, and specifically relates to an anti-pilling polyurethane finishing agent for textiles, and also relates to a preparation method of the polyurethane finishing agent. Background technique [0002] Knitted textiles have low yarn twist and loose tissue structure, and the surface of the fabric tends to have free fiber fluff. Knitted textiles are subject to friction during wearing and washing, and fibers tend to slip from the yarn and free on the surface of the fabric, and the fibers further collude and entangle with each other, resulting in pilling. The pilling of knitted textiles seriously affects the wearability and aesthetics. [0003] At present, many researchers have done more research and reports on the anti-pilling finishing of polyurethane and silicone-modified polyurethane on knitted fabrics. The publication number is: CN102505490A, the title of the invent...

Claims

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Application Information

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IPC IPC(8): D06M15/653C08G18/66C08G18/44C08G18/61C08G18/10D06M101/12
Inventor 徐成书邢建伟任燕
Owner 库尔勒汇同泰印染科技有限公司
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