Blue-phase liquid crystal composite material and liquid crystal display comprising same
A technology of blue-phase liquid crystal and composite materials, applied in liquid crystal materials, instruments, chemical instruments and methods, etc., can solve the problems of electro-optical hysteresis, low driving voltage, and high driving voltage, and achieve the reduction of electro-optical hysteresis, low driving voltage, and low driving voltage. Effect of driving voltage
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Embodiment 1
[0077] This embodiment provides a blue-phase liquid crystal composite material, the composition of which is: 68.5% by weight of the parent blue-phase liquid crystal; 30.0% by weight of a photopolymerizable monomer; 1.0% by weight of a photoinitiator; 0.5% by weight % of inorganic nanoparticles ZnS.
[0078] The above-mentioned blue phase liquid crystal composite material is prepared by the following method:
[0079] Step 1, preparation of inorganic nanoparticles ZnS
[0080] Add surfactant Triton X-100 (TritonX-100) into cyclohexane; add thioacetamide solution into cyclohexane dissolved in surfactant, slowly add positive butanol until the solution is clarified, that is, a thioacetamide microemulsion is formed; measure zinc acetate solution equivalent to thioacetamide, and prepare a zinc acetate microemulsion using the same method as that used to prepare the thioacetamide microemulsion.
[0081] The prepared thioacetamide microemulsion and zinc acetate microemulsion were mixe...
Embodiment 2
[0118] This embodiment provides a blue-phase liquid crystal composite material, the composition of which is calculated by mass percentage: 88.95wt% of the parent blue-phase liquid crystal; 10.0wt% of the photopolymerizable monomer; 1.0% of the photoinitiator; 0.05wt% of the inorganic Nanoparticle BaTiO 3 .
[0119] Step 1, preparation of inorganic nanoparticles BaTiO 3
[0120] By grinding large particles of BaTiO 3 powder (approximately 1 micron in diameter) to produce ferroelectric nanoparticles BaTiO 3 , BaTiO 3 The particles are mixed with oleic acid (surfactant) and heptane (carrier liquid) at a weight ratio of 1:2:10, and after ultrasonic dispersion, they are ground for 15 hours by a planetary high-energy ball mill. The ball-milled dispersion was transferred to a beaker, and left to stand for 3 days, and then filtered through a screen window to remove large-size particles, and the obtained dispersion was a dispersion containing ferroelectric nanoparticles with a spe...
Embodiment 3
[0138] This embodiment provides a blue-phase liquid crystal composite material, the composition of which is: 68.0wt% of the parent blue-phase liquid crystal; 27.0wt% of the photopolymerizable monomer; 3.0wt% of the photoinitiator; 2.0wt% Inorganic ZnO nanoparticles.
[0139] The above-mentioned blue phase liquid crystal composite material is prepared by the following method:
[0140] Step 1, preparation of inorganic nanoparticles ZnO
[0141] The polytetrafluoroethylene lining of the hydrothermal reactor was peeled and weighed, and the oleic acid was sucked into the lining with a dropper. Weigh 0.353g (1.25mmol) oleic acid into the lining by this method, put it into a 50mL hydrothermal reaction kettle, then dissolve sodium hydroxide and zinc acetate dihydrate (ratio of substance 2:1) in water, Add it into the hydrothermal reaction kettle, and keep stirring, then seal the kettle, put it in a dry box, raise the temperature to 130°C, and react for 4 hours; The solid is washed ...
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