LED (light-emitting diode) fluorescent powder with broadband gradient and preparation method thereof
A phosphor, broadband technology, applied in the field of LED solid-state lighting system
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Embodiment 1
[0092] Example 1 Preparation of YAG series broadband gradient phosphor powder
[0093] 1. Raw materials and reagents:
[0094] Yttrium oxide (Y 2 o 3 ≥99.99%) or yttrium nitrate (Y(NO 3 ) 3 ·6H 2 O≥99.99%); cerium nitrate (Ce(NO) 3 ·6H 2 O, analytically pure); aluminum nitrate (Al(NO 3 ) 3 9H 2 O, analytically pure); gallium nitrate (Ga(NO 3 ) 3 9H 2 O, analytically pure), gadolinium nitrate (Gd(NO 3 ) 3 ·6H 2 O, analytically pure), concentrated nitric acid HNO 3 , analytically pure; absolute ethanol, C 2 h 5 OH, analytically pure; distilled water H 2 O; ammonium bicarbonate (NH 4 HCO 3 , analytically pure); ammonia water (NH 3 ·H 2 O, analytically pure); polyethylene glycol (PEG1000)
[0095] 2. Experimental equipment
[0096] Conventional glass apparatus; dryer; pure water system; fully automatic electronic analytical balance; constant temperature magnetic stirrer; electric heating constant temperature water tank; pH acidity meter; Drying box; agate ...
Embodiment 2
[0142] BSS–A, BSS-B series broadband gradient phosphor preparation process such as Figure 7 and Figure 8 Shown:
[0143] 1 Raw materials and reagents:
[0144] Barium oxide (BaO≥99.99%) or barium nitrate (Ba(NO 3 ) 2 ≥99.99%); strontium oxide (SrO≥99.99%) or strontium nitrate (Sr(NO 3 ) 2 ≥99.99%); europium nitrate (Eu(NO 3 ) 3 6H2O, analytically pure); ethyl orthosilicate (Si(OC 2 h 5 ) 4 , analytically pure); concentrated nitric acid HNO 3 , analytically pure; absolute ethanol, C 2 h 5 OH, analytically pure; distilled water H 2 O; ammonium bicarbonate (NH 4 HCO 3 , analytically pure); ammonia water (NH 3 ·H 2 O, analytically pure); polyethylene glycol (PEG1000)
[0145] 2 experimental equipment
[0146] Conventional glass apparatus; dryer; pure water system; fully automatic electronic analytical balance; constant temperature magnetic stirrer; electric heating constant temperature water tank; pH acidity meter; Drying box; agate mortar; high-temperature g...
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