Cured resin, black photoresist, optical filter and their preparation method, display device
A black photoresist, curing resin technology, applied in the direction of filter, optical components, opto-mechanical equipment, etc., can solve the problems of high energy consumption, high curing temperature, increased cost, etc., to save energy, low curing temperature, high The effect of heat resistance
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
preparation example Construction
[0087] The embodiment of the present invention provides a method for preparing cured resin. In the preparation method, the raw materials of dibasic anhydrides and diamines used to prepare polyimide resins have a wide range of sources and a simple synthesis process. The cured resin finally obtained by the addition reaction overcomes the problem of high temperature curing caused by the curing resin in the traditional process, and realizes the low temperature curing of the cured resin. The cured resin prepared by the preparation method can not only reduce the energy consumption required in the production process of the optical filter.
[0088] Corresponding to the above-mentioned black photoresist, the embodiment of the present invention also provides a method for preparing a black photoresist, comprising figure 2 As shown, the method includes,
[0089] Step N1: Weigh the raw cured resin, colorant, solvent, starter and additives and mix them evenly.
[0090] In this step, the ...
Embodiment 1
[0109] Preparation of Cured Resin
[0110] First, take 1 part of 3,3,4,4-biphenyldianhydride and 1 part of 2,2-bis(3-aminophenyl)hexafluoropropane by weight, and dissolve them in 15 parts of ethylene glycol di in methyl ether, fully mixed, and injected into a four-necked bottle equipped with a heating device, a reflux device, a stirring device and a dropping device; after that, 2 parts of methacrylate were weighed by weight, and dissolved in 4 parts of ring fully dissolved in hexane, and injected into the reaction vessel; finally, weigh 0.3 parts of 4-hydroxyphthalic anhydride and 0.03 parts of azobisisovaleronitrile by weight, and dissolve them in 1 part of ethylene glycol dimethyl ether , fully dissolved, added dropwise into a four-necked flask, protected by nitrogen, and reacted for 2.5 hours at a temperature of 80°C to obtain a cured resin.
[0111] The cured resin was analyzed by gel permeation chromatography to obtain: the measured value of the molecular weight of the c...
Embodiment 2
[0117] Preparation of Cured Resin
[0118] First, take 1 part of pyromellitic dianhydride and 1.2 parts of 1,4-bis(aminomethyl)cyclohexane by weight, and dissolve the two in 20 parts of 1,1,1-trichloroethane, Mix well and inject into a four-necked bottle equipped with a heating device, a reflux device, a stirring device and a dropping device; after that, weigh 3 parts of styrene by weight, dissolve it in 7 parts of cyclohexane, and fully dissolve , also injected into the reaction vessel; finally, weigh 0.5 parts of 4-hydroxyphthalic anhydride and 0.06 parts of azobisisovaleronitrile by weight, and dissolve the two in 2 parts of 1,1,1-trichloroethane, fully Dissolve it, add it dropwise into a four-necked bottle, pass through nitrogen protection, and react at a temperature of 120° C. for 2 hours to obtain a cured resin.
[0119] The cured resin was analyzed by gel permeation chromatography to obtain: the measured value of the molecular weight of the cured resin was 43448.96; th...
PUM
| Property | Measurement | Unit |
|---|---|---|
| boiling point | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
Login to View More