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Preparation method of high-hardness water-resistant modified potassium fulvic acid powder

A technology of potassium fulvic acid and high-hard water resistance, which is applied in the fields of botanical equipment and methods, chemicals for biological control, organic fertilizers, etc. Convenience, inconvenient storage and transportation, etc., to achieve the effect of strong resistance to hard water, high production efficiency, and easy transportation and storage

Active Publication Date: 2013-10-09
SHANDONG CHUANGXIN HUMIC ACID TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Biochemical fulvic acid has high biological activity, but it is easy to decarboxylate and lose its activity during the concentration process, so it is only suitable for liquid form, and it is very inconvenient to transport and use
Mineral-derived fulvic acid has a complete chemical structure, many holes, and a large exchange capacity, but it is not resistant to hard water, which brings many problems to field use
Although the newly developed high-water-soluble potassium fulvic acid dry powder solves the problems of inconvenient storage and transportation, the coagulation limit is still not up to the use requirements of high hard water environment, and the content of fulvic acid and water solubility need to be further improved.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0009] Embodiment 1: the sulfonation process is: the potassium fulvic acid dry powder is sent into the multi-section vertical vulcanized bed sulfonation tower with a screw quantitative feeder, and after the selected sulfonating agent sulfur trioxide is atomized, blower is used to Sent into the sulfonation tower, the amount of sulfur trioxide is 2% of the amount of potassium fulvate dry powder, and after 2 seconds of sulfonation treatment in the sulfonation tower, the finished product of modified potassium fulvate powder resistant to high hard water is made. Enter the packaging machine for bagging and packaging. The quality indicators of the finished product are: the content of fulvic acid is 53%, the water solubility is 96%, the potassium content is 10%, and the coagulation limit is 18.

Embodiment 2

[0010] Embodiment 2: the sulfonation process, the potassium fulvate dry powder is sent into the multi-section vertical fluidized bed sulfonation tower by a screw quantitative feeder, and then the sulfur trioxide that accounts for 2.5% of the potassium fulvate dry powder total amount is carried out Atomized, used as a sulfonating agent, sent into the sulfonation tower by a blower, and after 3 seconds of sulfonation treatment, the finished product of anti-high hard water modified potassium fulvic acid powder is obtained, which is input into a packaging machine for bagging and packaging. The finished product is a black powder that is easily soluble in water. The content of fulvic acid is 55%, the water solubility is 98%, and the aggregation limit is 20. It can be used as foliar fertilizer, drip irrigation fertilizer, plant growth regulator, feed additive, and Humic acid micro-fertilizer can be made.

[0011] The finished product of the invention has good water solubility, high co...

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Abstract

The invention discloses a preparation method of high-hardness water-resistant modified potassium fulvic acid powder. The preparation method comprises the following steps of: with potassium fulvic acid dry powder as a main raw material, feeding the potassium fulvic acid dry powder into a sulfonating tower by a feeder through a sulfonating process, wherein the feeder, an air blower, the sulfonating tower and a bag packing machine are connected to form a production line; atomizing a sulfonating agent and feeding the atomized sulfonating agent into the sulfonating tower by the air blower; and carrying out sulfonating treatment for 2-5 seconds in the tower to prepare the high-hardness water-resistant modified potassium fulvic acid finished product, and conveying the finished product into the bag packing machine for bagging and packing, wherein the proportion of the sulfonating agent to the potassium fulvic acid dry powder is (1%-3%):100%, the sulfonating agent is sulfur trioxide, the fulvic acid content of the finished product is 46%-55%, the water solubility is 96%-98% and the condensation limit is 18-20. The finished product can be used as a leaf fertilizer, a drip fertilizer, a humic acid micro fertilizer, a plant biological regulator or a feed additive. Besides, the finished product prepared by the preparation method disclosed by the invention is high in physiological activity, good in water solubility and stability, extremely high in condensation limit, wide in application range, and easy to transport and store.

Description

technical field [0001] The invention relates to a potassium fertilizer production process, in particular to a production process of ore-derived potassium fulvic acid. Background technique [0002] Potassium fulvic acid powder is an excellent potassium fertilizer with multiple functions, which is made by extracting fulvic acid. There are two main sources of fulvic acid, one is extracted from straw and other crops through biological fermentation, called biochemical fulvic acid; the other is extracted from minerals rich in fulvic acid, called mineral-derived fulvic acid . Biochemical fulvic acid has high biological activity, but it is easy to decarboxylate and lose its activity during the concentration process, so it is only suitable for liquid form, and it is very inconvenient to transport and use. Mineral-derived fulvic acid has a complete chemical structure, many cavities, and a large exchange capacity, but it is not resistant to hard water, which brings many problems to ...

Claims

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Application Information

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IPC IPC(8): C05F11/00A23K1/16A01N61/00A01P21/00
Inventor 孙明广田原宇杜茂福樊庆鲁朱升美甄卫军
Owner SHANDONG CHUANGXIN HUMIC ACID TECH
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