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Method for preparing bio-adsorbent by taking rice bran as raw material

A biosorbent and rice bran technology, which is applied in chemical instruments and methods, and other chemical processes, can solve the problems of low added value of products and environmental pollution, and achieve the effects of superior adsorption performance, reduced environmental risks, and small investment

Inactive Publication Date: 2015-04-22
SICHUAN AGRI UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Rice bran is a by-product in the agricultural production process. At present, it is mainly used for animal feed, incineration, composting, etc. The added value of the product is low, and some utilization methods such as incineration will pollute the environment.

Method used

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  • Method for preparing bio-adsorbent by taking rice bran as raw material
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  • Method for preparing bio-adsorbent by taking rice bran as raw material

Examples

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Effect test

Embodiment 1

[0028] A method for preparing a biosorbent by using rice bran. Firstly, rice bran, an agricultural by-product, is selected as a raw material, and the specific preparation steps are as follows:

[0029] 1. Pretreatment: The rice bran is taken from a rural rice processing factory. First, it is manually screened to remove a small amount of large particle size impurities. The rice bran is washed repeatedly with tap water, and then washed repeatedly with distilled water and deionized water. Dry down to constant weight, then pulverize and sieve, and keep the samples between 40-60 mesh.

[0030] 2. Alkali treatment: Weigh 100 g of the original rice bran prepared in step 1, place it in a 1000 mL conical flask, add 1000 ml of NaOH solution with a mass concentration of 2% (solid-to-liquid ratio is 1:10), shake well and soak at room temperature for 24 hours, shaking once every 2 hours.

[0031] The alkali-treated rice bran was vacuum-filtered, washed repeatedly with deionized water unti...

Embodiment 2

[0036] A method for preparing a biosorbent by using rice bran. Firstly, rice bran, an agricultural by-product, is selected as a raw material, and the specific preparation steps are as follows:

[0037] 1. Pretreatment: The rice bran is taken from a rural rice processing factory. First, it is manually screened to remove a small amount of large particle size impurities. The rice bran is washed repeatedly with tap water, and then washed repeatedly with distilled water and deionized water. Dry down to constant weight, then pulverize and sieve, and keep the samples between 40-60 mesh.

[0038] 2. Alkali treatment: Weigh 100 g of the original rice bran prepared in step 1, place it in a 1000 mL conical flask, add 1000 ml of NaOH solution with a mass concentration of 8% (solid-to-liquid ratio is 1:10), shake well and soak at room temperature for 24 hours, shaking once every 2 hours.

[0039] The alkali-treated rice bran was vacuum-filtered, washed repeatedly with deionized water unti...

Embodiment 3

[0044] A method for preparing a biosorbent by using rice bran. Firstly, rice bran, an agricultural by-product, is selected as a raw material, and the specific preparation steps are as follows:

[0045] 1. Pretreatment: The rice bran is taken from a rural rice processing factory. First, it is manually screened to remove a small amount of large particle size impurities. The rice bran is washed repeatedly with tap water, and then washed repeatedly with distilled water and deionized water. Dry down to constant weight, then pulverize and sieve, and keep the samples between 40-60 mesh.

[0046] 2. Alkali treatment: Weigh 100 g of the original rice bran prepared in step 1, place it in a 1000 mL conical flask, add 1000 ml of NaOH solution with a mass concentration of 2% (solid-to-liquid ratio is 1:10), shake well and soak at room temperature for 24 hours, shaking once every 2 hours.

[0047] The alkali-treated rice bran was vacuum-filtered, washed repeatedly with deionized water until ...

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Abstract

The invention discloses a method for preparing a bio-adsorbent by taking rice bran as a raw material. The method comprises the following steps: pre-treating original rice bran and immersing the pretreated rice bran by using an NaOH alkaline solution; washing filtering dreg until the filtering dreg is close to be neutral; after drying at a constant temperature, carrying out oxidization treatment by using a potassium permanganate solution; and carrying out a plurality of times of washing, filtering and constant-temperature drying on the obtained material to obtain the product. The raw materials are agricultural byproducts and are cheap and easily available; chemical agents for modifying the raw materials are common medicines; the operation steps are simple and feasible; a few of sets of equipment are needed, the investment is small and the process is simple; industrial production is easy to realize; the obtained product has good adsorption performance, the environmental risks caused by shell type organic agricultural byproducts are reduced effectively and the resource re-utilization of the agricultural byproducts is realized.

Description

technical field [0001] The invention relates to a method for preparing a biosorbent by using rice bran as a raw material, specifically a method for preparing a high-quality and high-efficiency biosorbent by using rice bran as a raw material for pretreatment, alkali treatment and oxidation treatment combined modification, belonging to Resource utilization of agricultural by-products is used in the technical field of adsorption and removal of heavy metals in water. Background technique [0002] Heavy metal pollution and its hazards in the environment have become one of the global problems. The heavy metal cadmium is highly toxic, widely distributed, and has serious hazards to human, animal and plant health. Cadmium can be toxic to animal and plant life tissues at low concentrations. Cadmium-containing wastewater mainly comes from industries such as mining and metallurgy, battery production, tanning, electroplating, film and automobile manufacturing. In recent years, the prob...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01J20/24B01J20/30
Inventor 邓仕槐梁东旭杨新瑶罗春燕王成明肖鸿王莉淋沈飞李黎李远伟张延宗白林
Owner SICHUAN AGRI UNIV