Reduced graphene oxide/ZnIn2S4 photocatalyst and preparation method and application thereof
A photocatalyst, znin2s4 technology, applied in physical/chemical process catalysts, chemical instruments and methods, chemical/physical processes, etc., can solve problems such as limited application, achieve high reaction efficiency, be beneficial to large-scale industrial production, and simple to operate Effect
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Embodiment 1
[0025] Composite photocatalyst RGO / ZnIn with efficient and stable photocatalytic hydrogen production 2 S 4 preparation of
[0026] First, graphene oxide (GO) was prepared: 5 g graphite and 2.5 g NaNO 3 Stir in 120 mL of concentrated sulfuric acid for 1 h. Slowly add 15 g KMnO 4 , stirred for 5 days. 700 mL H 2 O was added to the reaction system, and then 65 mL of 30% H 2 o 2 . After dilute HCl, H 2 O washing, followed by ultrasonic dispersion in H 2 O, the brown-yellow GO was obtained. Then a certain amount of GO was dispersed in a mixed solvent of ethylene glycol (30ml EG) and N,N-dimethylformamide (30ml DMF), sonicated for 1h, and then ZnCl was added 2 (0.136g), InCl 3 4H 2 O (0.586g) was dissolved, sonicated for 2h, and finally thioacetamide (TAA 0.3g) was added, stirred for 1h, the solution was transferred to a 100mL hydrothermal kettle, reacted at 200°C for 24h, and washed by centrifugation with ethanol and water. Drying, that is, the dark green RGO / ZnIn wit...
Embodiment 2
[0032] Zn 2 S 4 and RGO / ZnIn loaded with different contents of RGO 2 S 4 Comparison of the photocatalytic hydrogen production performance of the composites in the presence of sacrificial agents.
[0033] The resulting composite photocatalyst RGO / ZnIn 2 S 4 The complex is used for photolysis of water to produce hydrogen. Weigh 50mg of the sample and add it to 100ml of aqueous solution containing 2.0ml of lactic acid. After vacuuming the photocatalytic hydrogen production system, turn on the light source for photocatalytic hydrogen production. The amount of photocatalytic hydrogen production was detected by chromatography (Fuli, China, TCD, argon as the carrier gas, and the chromatographic column was 5? molecular sieve). ZnIn of the present invention 2 S 4 and RGO / ZnIn loaded with different contents of RGO 2 S 4 The comparison of the photocatalytic hydrogen production performance of the composite under visible light is as follows: Figure 5 . It can be seen from the f...
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