Gel double-solution plugging regulating agent of steam injection well for thermal recovery and plugging regulating method using gel double-solution plugging regulating agent
A technology of steam injection well and plugging agent, which is applied in chemical instruments and methods, production fluids, earthwork drilling, etc., can solve problems such as uneven steam absorption, and achieves extended gel strength, good thermal stability, and simple preparation process. Effect
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Embodiment 1
[0022] To prepare high-temperature-resistant main agent sodium nitrohumate, mix industrial grade sodium humate and 65% concentrated nitric acid (by weight) in a ratio of 1:6, pass through a condensing reflux device at 90°C, and undergo nitrification modification reaction, After stirring for 3 hours, it was evaporated to dryness, and sodium nitrohumate was finally obtained as dark brown powder, which was acidic.
Embodiment 2
[0024] Preparation of thermal recovery steam injection well gel two-liquid plugging agent,
[0025] 1. the 6wt% sodium nitro humate prepared by Example 1 is dissolved in water by weight, and the pH is adjusted to neutrality. After fully dissolving, it is dissolved into 1.2wt% formaldehyde by weight, and the first solution is obtained after fully dissolving. Working solution, the solution is dark brown;
[0026] ② Dissolve 0.015wt% polyacrylamide by weight in water, and after fully swelling at a speed of less than 100r / min, add 2.2wt% resorcinol by weight and stir until completely dissolved. color viscous;
[0027] ③ Add the second working fluid to the first working fluid, stir for 40 minutes until fully mixed, and obtain the thermal recovery steam injection well gel double-liquid plugging regulator, which is a dark brown solution.
[0028] The above-mentioned weight fractions are the percentages of each component in the total weight of the prepared thermal recovery and injec...
Embodiment 3
[0036] Preparation of thermal recovery steam channeling control gel-type two-liquid plugging agent,
[0037] In this example, sodium nitrohumate by weight is 6wt%, formaldehyde is 1.2wt%, resorcinol is 2.2wt%, HPAM (polyacrylamide) is 0.03wt%, and others are the same as in Example 2 . In this embodiment, it is measured through experiments: the gelling time of the system is 8-9 hours, the gelling viscosity is 37592 mPa·s, and the plugging rate is greater than 97%.
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