Preparation technology of water-based PU (Polyurethane) glue substituting solvent type printing ink TPU (Thermoplastic Polyurethane)
A preparation process, solvent-based technology, applied in the field of water-based PU adhesive preparation process, can solve the problems of many residual solvents, single color, limited flexibility, etc.
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Embodiment 1
[0016] Slowly stir 26.4kg of acrylic resin in a dispersion tank at normal temperature and pressure, and adjust its pH value to 8 by adding ammonia water.
[0017] Put 30kg of polyurethane aqueous dispersion (Impranit DL1537XP), 25kg of polyurethane aqueous dispersion (ADEKA HUX-280), 2kg of propylene glycol methyl ether acetate, 2kg of ethylene glycol butyl ether, and wetting defoamer (Surfynol 104E) into the dispersion tank in turn. ) 1kg, silicon defoamer (Dehydran 12930) 4kg, leveling wetting agent (BYK346) 0.3kg, slip agent (BYK333) 0.25kg, matte powder 2kg, elastomer 2kg, wear agent 3kg, thickener (PTF) 0.2kg, thickener (Viscdam Ps166) 0.4kg, deionized water 2.45kg, continue to disperse for 1 hour.
[0018] After dispersing, heat it to 80°C, and at the same time, use a vacuum pump to continuously evacuate the inside of the tank, and keep the air pressure in the tank at 0.8 negative pressure for 0.5 hours.
[0019] Then inject cooling circulating water into the outer wall...
Embodiment 2
[0021] Slowly stir 30kg of acrylic resin in a dispersion tank at normal temperature and pressure, and add ammonia water to adjust its pH value to 8.
[0022] Put 25kg of polyurethane aqueous dispersion (Impranit DL1537XP), 26kg of polyurethane aqueous dispersion (ADEKA HUX-280), 2kg of propylene glycol methyl ether acetate, 1kg of ethylene glycol butyl ether, and wetting defoamer (Surfynol 104E) into the dispersion tank in turn. ) 3kg, silicon defoamer (Dehydran 12930) 6kg, leveling wetting agent (BYK346) 0.3kg, slip agent (BYK333) 0.2kg, matte powder 1kg, elastomer 1kg, wear agent 2kg, thickener (PTF) 0.2kg, thickener (Viscdam Ps166) 0.1kg, deionized water 2.2kg, continuous dispersion for 1 hour.
[0023] After dispersing, heat it to 80°C, and at the same time, use a vacuum pump to continuously evacuate the inside of the tank, and keep the air pressure in the tank at 0.8 negative pressure for 0.5 hours.
[0024] Then inject cooling circulating water into the outer wall of th...
Embodiment 3
[0026] Slowly stir 24kg of acrylic resin in a dispersion tank at normal temperature and pressure, and add ammonia water to adjust its pH value to 8.
[0027] Put 31kg of polyurethane aqueous dispersion (Impranit DL1537XP), 23kg of polyurethane aqueous dispersion (ADEKA HUX-280), 1kg of propylene glycol methyl ether acetate, 2kg of ethylene glycol butyl ether, and wetting defoamer (Surfynol 104E) into the dispersion tank in turn. ) 1kg, silicon defoamer (Dehydran 12930) 2kg, leveling wetting agent (BYK346) 1kg, slip agent (BYK333) 1kg, matting powder 2kg, elastomer 2kg, wear agent 3kg, thickener (PTF ) 1kg, thickener (Viscdam Ps166) 1kg, deionized water 3kg, continue to disperse for 1 hour.
[0028] After dispersing, heat it to 80°C, and at the same time, use a vacuum pump to continuously evacuate the inside of the tank, and keep the air pressure in the tank at 0.8 negative pressure for 0.5 hours.
[0029] Then inject cooling circulating water into the outer wall of the disper...
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