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A kind of NdFeB permanent magnet material and its preparation method and magnetic field assisted direct casting device

A permanent magnet material, neodymium iron boron technology, applied in the direction of magnetic materials, magnets, magnetic objects, etc., can solve the problems of restricting the application of copper mold casting methods, uneven overall structure of castings, and easy nucleation and growth of grains, etc., to achieve Enhanced corrosion resistance and service life, good mechanical properties, less metallurgical defects

Active Publication Date: 2016-10-05
SOUTH CHINA UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] However, due to the difference in the cooling rate between the core and the surface of the casting during the casting process, the outer surface of the copper mold that first contacts the copper mold has a faster cooling rate, and the greater degree of undercooling makes it skip the crystallization process and obtain an amorphous phase or grain Smaller nanocrystals, while in the core of the casting, due to the existence of the temperature gradient, the cooling rate is much lower than that of the surface, and the grains are easy to nucleate and grow
This leads to uneven overall structure of the casting, which has a great impact on the improvement of the comprehensive magnetic properties of the magnet and the design of subsequent heat treatment, and limits the application of the copper mold casting method in actual production.

Method used

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  • A kind of NdFeB permanent magnet material and its preparation method and magnetic field assisted direct casting device
  • A kind of NdFeB permanent magnet material and its preparation method and magnetic field assisted direct casting device
  • A kind of NdFeB permanent magnet material and its preparation method and magnetic field assisted direct casting device

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Effect test

Embodiment 1

[0036] figure 1 It is a schematic structural diagram of a magnetic field-assisted direct casting device for NdFeB permanent magnet materials, and the arrow in the figure indicates the direction of magnetization. Such as figure 1 , 2As shown, the magnetic field assisted direct casting device of NdFeB permanent magnet materials includes a first repelling magnet 1, a second repelling magnet 2, a magnet guiding magnet 3, a main magnet 4, a control magnet 5, a first soft iron 6 and a second Soft iron 7; Main magnet 4 is the ring-shaped magnet of radial magnetization; Main magnet 4 center is provided with a piece of magnetic field direction and is the second repelling magnet 2 of axially upward disc shape, and the second repelling magnet 2 periphery is provided with There is the circular first repelling magnet 1 of radial magnetization; The first repelling magnet 1 and the second repelling magnet 2 are preferably equal thickness cooperation; The first repelling magnet 1 and the se...

Embodiment 2

[0050] Step 1: Add Nd 35 co 20 Fe 30 al 10 B 5 According to the proportion of (atomic ratio); the total weight of the sample is 10g, of which Nd, Co, Fe, Al, and B are 6.1369g, 1.4327g, 2.0367g, 0.3280, and 0.0657, respectively.

[0051] Step 2: Put the raw materials prepared in Step 1 into the electric arc furnace, and evacuate to 10 ‐3 Pa, after cleaning the furnace with high-purity argon, fill it with high-purity argon at a pressure slightly lower than 1 atmosphere (about 0.1MPa), and repeatedly smelt 5-8 times under the protection of high-purity argon. The melting temperature is 1300-1500°C. The time is 2-3 minutes, and a button-shaped alloy ingot with uniform composition is obtained after cooling.

[0052] Step 3: After simple mechanical crushing of the alloy ingot prepared in Step 2, put it into a quartz tube with a small hole at the lower end, heat it with high-frequency induction, and evacuate to 10 -4 Pa, after cleaning the furnace with high-purity argon, fill i...

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Abstract

The invention discloses a neodymium-iron-boron permanent magnet material, a preparation method and a magnetic field auxiliary direct casting device. A main magnet of the device is a circular-ring-shaped magnet which is magnetized in a radial mode. A first disc-shaped repulsion magnet with the magnetic field direction being axially upward is arranged below the center of the main magnet, and a second disc-shaped repulsion magnet which is magnetized in a radial mode is arranged on the periphery of the first repulsion magnet. A regulating magnet is arranged at the upper end of the main magnet, second soft iron is arranged on the upper portion of the regulating magnet, first soft iron is arranged outside the regulating magnet, and a circular-ring-shaped magnet guide magnet which is magnetized downwards in the axial direction is arranged outside the main magnet. The chemical general formula of the neodymium-iron-boron permanent magnet material is [Nd (85-x-y) CoxFeyAlzB (15-z)] (100-a) Ma, wherein in the formula, x+y is larger than or equal to 30 and smaller than or equal to 70, z is larger than or equal to 0 and smaller than or equal to 10, and a is smaller than and equal to 4. Compared with a material prepared without adding magnetic fields, the performance of the neodymium-iron-boron permanent magnet material is greatly improved, the preparation process is simple, cost is low, products are dense, and the neodymium-iron-boron permanent magnet material is suitable for industrial production.

Description

technical field [0001] The invention relates to an NdFeB magnetic field assisted direct casting device, in particular to a preparation method for directly casting NdFeB under the auxiliary magnetic field system. Background technique [0002] Neodymium-iron-boron (NdFeB)-based alloys (including rare earth-iron / cobalt-boron alloys of different compositions), as rare earth permanent magnet materials with the best comprehensive magnetic properties at room temperature, are widely used in various electromechanical products, and their market value is close to that of permanent magnets. One-half of magnetic materials and rising year by year. At present, the preparation of NdFeB magnets mainly adopts powder metallurgy route. Firstly, magnetic powder is obtained by different methods, and then sintered magnets, bonded magnets and thermally deformed magnets are obtained by sintering, bonding or thermal deformation (die forging). The preparation process of magnets is complicated and the...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B22D27/02H01F7/00H01F1/057
Inventor 刘仲武赵利忠郑志刚李伟王刚钟喜春余红雅曾德长
Owner SOUTH CHINA UNIV OF TECH
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