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41results about How to "Less metallurgical defects" patented technology

Electrodeposition-laser remelting strengthening process of Ni-nanometer TiN composite layer on surface of nickel base superalloy

The invention relates to an electrodeposition-laser remelting strengthening process of a Ni-nanometer TiN composite layer on a surface of a nickel base superalloy. The process comprises the following steps: (1) preparation of plating solution: the plating solution comprises such components as nickel aminosulfonate, nickel chloride and water solution of boric acid; (2) preparation of electrodes: the area ratio of an anode to a cathode is 1.5: 1; and the anode and the cathode are arranged in parallel by a distance of 30 mm; (3) composite electrodeposition: a power supply adopts a two-way high-frequency pulse power supply; and (4) laser remelting: a solid pulse laser processor is adopted to perform the one-way laser remelting; and applied power ultrasonic waves, high-intensity magnetic fields and high-frequency pulse current parameters assist the electrodeposition process. The process organically combines the electrodeposition Ni-nanometer TiN composite layer technology with the laser cladding technology, is a new composite processing technology of physics and electrochemistry, and has the advantages of high processing efficiency and quality and wider application range. The process can satisfy the use requirements of nickel base alloy parts under the working conditions of high speed, high temperature, high impact load and corrosion.
Owner:DALIAN UNIV

Aluminum alloy evaporator inner wall thin plate and continuous casting rolling production process thereof

The present invention discloses an aluminum alloy evaporator inner wall thin plate and a continuous casting rolling production process thereof. The thin plate adopts an aluminum manganese alloy as a base, contains silicon, iron, copper, manganese, magnesium, zinc and titanium, and is prepared by adopting a continuous casting rolling production process. The process comprises the following steps: adding raw materials to a smelting furnace to carry out melting, refining, and residue removing; discharging the resulting material to a cast rolling machine from the furnace to carry out cast rolling; carrying out a first annealing treatment on the cast-rolled plate material to reduce needle-like FeAl3 and influence on mechanical property by a phase composition, wherein the phase composition and the Al-Mn solid solution achieve phase equilibrium; carrying out cold rolling on the first-annealed plate material 5-6 times; carrying out a second annealing treatment on the cold-rolled plate material; and carrying out foil rolling 1-2 times to prepare the aluminum alloy evaporator inner wall thin plate. The technical scheme of the present invention has the following characteristics that: good moldability, good weldability, and good corrosion resistance are provided, structure and performances are uniform, metallurgical defects are less, anisotropy is low, strength is high strength, elasticity is good, and the like.
Owner:江阴新仁铝业科技有限公司

Preparation method of rare earth magnesium alloy and sheet thereof

The invention provides a rare earth magnesium alloy. The rare earth magnesium alloy is characterized by comprising the following components by mass percent: 0.5 to 4.0% of Zn, 0.1 to 2% of Gd, 0.3 to 0.9% of Zr, and the balance of Mg. The preparation method of the rare earth magnesium alloy sheet comprises the following steps of: treating a rare earth magnesium alloy ingot casting by uniform annealing; cooling with water; milling the surface; preheating a milled blank; rolling for four to eight times; melting down and heating once every two to three times after rolling; continuously rolling, wherein the total rolling reduction is 70 to 95%; annealing the sheet subjected to hot rolling; performing cold rolling for a moderate-thickness sheet subjected to hot rolling for two to four times; and then annealing the sheet subjected to cold rolling to obtain the rare earth magnesium alloy sheet. The invention also provides a preparation method of the rare earth magnesium alloy and the sheet thereof. The rare earth magnesium alloy sheet is high in plasticity and high in heat stability. Compared with hot rolling, cold rolling has the advantage that the magnesium alloy can be prevented from being oxidized into a film during heating; in addition, the prepared sheet is accurate in dimension and uniform in thickness; a thin belt which cannot be produced by hot rolling can be obtained; and mass production and application can be realized.
Owner:GUANGDONG INST OF NEW MATERIALS

Powder metallurgy preparation method of graphene reinforced aluminum-based composite material

The invention provides a powder metallurgy preparation method of a graphene reinforced aluminum-based composite material, which comprises the following steps: preparing graphene-aluminum composite powder by long-time low-energy ball milling in advance, annealing, and carrying out short-time high-energy ball milling, densification processing and heat treatment to finally obtain the composite material. Uniform compounding of matrix powder and graphene is achieved through long-time low-energy ball milling, meanwhile, interface reaction can be avoided, and the structural integrity of graphene is protected; the annealed composite powder can improve the plastic deformation capacity of the composite powder while improving the quality of the graphene; short-time high-energy ball milling is performed, so that composite powder is welded into particles, and the quality of graphene is not damaged; and in addition, for the composite material of a aluminum alloy matrix, the uniformly dispersed graphene promotes the precipitation of fine dispersed precipitated phases in the matrix, and the mechanical properties of the composite material are further improved. The method is beneficial to protecting the integrity of the graphene structure to the maximum extent, exerts the graphene strengthening potential, saves energy and time, and is suitable for batch preparation and production.
Owner:SHANGHAI JIAO TONG UNIV

Preparation process of nickel-based high temperature alloy with high-content refractory elements

The invention discloses a preparation process of a nickel-based high temperature alloy with high-content refractory elements, and belongs to the technical field of alloy preparation. According to theprocess, a vacuum induction melting (VIM) and electroslag remelting (ESR) process is adopted for preparing the alloy containing the high-content refractory elements. During the vacuum induction melting stage, by controlling the feeding mode, increasing the refining temperature, prolonging the refining time, accelerating the solidification rate and the like, the segregation phenomena of refractorymetal and low-density alloy elements are effectively suppressed, and the composition uniformity of upper and lower parts of a parent alloy ingot is improved. Through electroslag remelting, secondary shrinkage in the alloy ingot is eliminated, the impurity content is reduced, and the metallurgical quality is improved. The preparation process can significantly reduce the microsegregation and macrosegregation phenomena of the high-content refractory elements and can effectively reduce the content of harmful gas elements such as O and N in the high-temperature alloy, the purity of the alloy is improved, the degree of segregation of the high-specific gravity elements is reduced, the heredity of alloy anomalous tissues is improved, and the overall mechanical properties of the alloy are improved.
Owner:INST OF METAL RESEARCH - CHINESE ACAD OF SCI

Claw assembly with long service life and production process thereof

The invention discloses a claw assembly with long service life and a production process thereof, which are used for manufacturing parts with mutual friction in an operation process of the claw assembly of a nuclear reactor control rod driving mechanism. The process comprises the following steps which are carried out in sequence: discharging, roughly machining and machining a wear-resisting layer on the surface. The step of discharging is to machine blanks of all parts according to design requirements; the step of machining the wear-resisting layer on the surface is to spray and weld the wear-resisting layer on the surface of each blank; and the step of spraying and welding the wear-resisting layer comprises the following steps which are carried out in sequence: pre-heating, spraying powder and re-melting, and cooling. In the claw assembly disclosed by the invention, the sprayed and welded wear-resisting layer or the surfaced wear-resisting layer is arranged on the surface of each part with the friction in the operation process. The invention provides the claw assembly with the long service life and a corresponding manufacturing process, and the obtained claw assembly meets the requirements on the wear resistance under a high-frequency working condition within a 60-year service period.
Owner:SICHUAN HUADU NUCLEAR EQUIP MFR

Hot-isostatic-pressing forming method for in-situ generation of continuous spatial net structure

The invention discloses a hot-isostatic-pressing forming method for in-situ generation of a continuous spatial net structure. According to the hot-isostatic-pressure forming method for in-situ generation of the continuous spatial net structure, the surface of a powder base material is covered with a layer of reinforcing materials before hot-isostatic pressing according to the reinforcing requirement of the base material during actual application, and the base material and the reinforcing material are subjected to an in-situ reaction under the effect of high temperature and high pressure of hot-isostatic pressing, so that a new compound with a reinforcing effect is generated, and the compound exists on the boundary of an original powder particle in the form of the continuous spatial net structure. Metallurgical defects caused by an oxide layer on the surface of the original powder particle are effectively reduced through the spatial net structure, and the metallurgical bonding strength between different kinds of powder is improved; and in addition, through a newly-generated reinforcing phase, relevant performance of the base material can be improved, the service life of a hot-isostatic-pressed workpiece is prolonged, and the safety of the hot-isostatic-pressed workpiece is improved.
Owner:HUAZHONG UNIV OF SCI & TECH

Technical method for manufacturing aero-engine cyclone through special processing technology

ActiveCN108500574AImproves metal stabilityExtended service lifeAviationCyclone
The invention relates to the field of aero-engines and gas turbines, and particularly relates to a technical method for manufacturing an aero-engine cyclone through a special processing technology. The method comprises the step of manufacturing a cyclone blank, wherein the cyclone bank is manufactured through a cylindrical forging piece. The method further comprises the step of manufacturing semi-finished cyclone and the step of finishing through pincers; the step of manufacturing the semi-finished cyclone is that the cyclone blank is sequentially subjected to turning processing and electric spark processing to obtain the semi-finished cyclone; the step of finishing through the pincers is that the semi-finished cyclone is finished based on the requirement on a finished cyclone so as to obtain the finished cyclone. According to the method, the forging piece is outstanding in mechanical property, and two processing modes are provided, so that the manufactured cyclone product is high in strength and toughness; the yield is increased; and the processing cost and the processing period are reduced; the manufactured cyclone product can stably run for a long time in an aero-engine combustion chamber; and the service life of the aero-engine combustion chamber cannot be influenced by the quality of the cyclone.
Owner:广汉天空动力机械有限责任公司

Aluminum alloy evaporator inner wall thin plate and continuous casting rolling production process thereof

The present invention discloses an aluminum alloy evaporator inner wall thin plate and a continuous casting rolling production process thereof. The thin plate adopts an aluminum manganese alloy as a base, contains silicon, iron, copper, manganese, magnesium, zinc and titanium, and is prepared by adopting a continuous casting rolling production process. The process comprises the following steps: adding raw materials to a smelting furnace to carry out melting, refining, and residue removing; discharging the resulting material to a cast rolling machine from the furnace to carry out cast rolling; carrying out a first annealing treatment on the cast-rolled plate material to reduce needle-like FeAl3 and influence on mechanical property by a phase composition, wherein the phase composition and the Al-Mn solid solution achieve phase equilibrium; carrying out cold rolling on the first-annealed plate material 5-6 times; carrying out a second annealing treatment on the cold-rolled plate material; and carrying out foil rolling 1-2 times to prepare the aluminum alloy evaporator inner wall thin plate. The technical scheme of the present invention has the following characteristics that: good moldability, good weldability, and good corrosion resistance are provided, structure and performances are uniform, metallurgical defects are less, anisotropy is low, strength is high strength, elasticity is good, and the like.
Owner:江阴新仁铝箔科技有限公司

A high-efficiency processing method for aeroengine swirlers

The invention relates to the field of aeroengines and gasoline turbines, in particular to a technological method of a high-efficient machining swirler for an aeroengine. The method comprises a step ofpreparing a swirler blank, wherein the swirler blank is manufactured by columnar forging pieces, and the columnar forging pieces are manufactured by aviation materials; the method also comprises a step of preparing a swirler semi-finished product and a step of gripping and repairing; the step of preparing a swirler semi-finished product comprises the following steps: turning the swirler semi-finished product at least one time and milling the swirler semi-finished product at least one time so as to prepare the swirler semi-finished product; and the step of gripping and repairing comprises thefollowing steps: trimming a profile surface of the swirler semi-finished product according to a finished product requirement of the aeroengine so as to prepare a swirler finished product. By adoptinga matched machining way of turning and milling, a machining period is shortened; and by matching with a gripping and repairing operation, a finished product ratio is increased, so that the manufactured swirler finished product has the advantages of stable metal quality and longer service life, and the manufactured swirler finished product meets a high-standard requirement on the aeroengine.
Owner:广汉天空动力机械有限责任公司

Preparation process of a nickel-based superalloy with high content of refractory elements

The invention discloses a preparation process of a nickel-based superalloy with high content of refractory elements, and belongs to the technical field of alloy preparation. The process adopts vacuum induction melting (VIM) + electroslag remelting (ESR) process to prepare alloys with high content of refractory elements. During vacuum induction melting, by controlling the feeding method, increasing the refining temperature and prolonging the refining time, and accelerating the solidification rate, etc., the segregation of refractory metals and low-density alloy elements can be effectively suppressed, and the composition uniformity of the upper and lower parts of the master alloy ingot can be improved. Electroslag remelting eliminates secondary shrinkage cavities in alloy ingots and reduces impurity content to improve metallurgical quality. The invention can not only significantly reduce the micro-segregation and macro-segregation of high-content refractory elements, but also effectively reduce the content of harmful gas elements such as O and N in superalloys, thereby improving the purity of the alloy and reducing the degree of segregation of high-density elements. Improve the heredity of the abnormal structure of the alloy and improve the comprehensive mechanical properties of the alloy.
Owner:INST OF METAL RESEARCH - CHINESE ACAD OF SCI

Technique for producing precision castings of zirconium and zirconium alloy pumps/valves

The invention provides a technique for producing precision castings of zirconium pump and valves. The technique is characterized in that the precision castings of zirconium pumps and valves are produced by adopting the methods of lost-wax ceramic-shell precision casting and hot isostatic pressing, wherein the lost-wax ceramic-shell precision casting refers to near-net-shape casting adopting a lost-wax ceramic shell for casting in a vacuum self-consuming skull furnace; the lost-wax ceramic shell is formed through reproduction according to a wax pattern consistent with the geometric shape and size of a pump and valve component; the first two layers of the shell of the inner surface of the lost-wax ceramic shell is made from special oxide; the whole shell is manufactured through the process links of wax pressing, painting, shell hanging, dewaxing, roasting and the like; and the hot isostatic pressing is to place a to-be-treated casting in a container which ishermetic and resistant to high pressure and can be heated to high temperature, vacuumize the container, fill the container with high-pressure inert gas and heat the container to a preset temperature. The technique has the advantage of solving the problem of low material utilization rate and hidden trouble caused by no welding seams at high temperature and high isostatic pressure in all directions, high surface finish of the casting, few internal defects of the casting, pure composition and stable performance.
Owner:SHENYANG NORTH TITANIUM IND

A kind of preparation method of high-purity titanium-nickel-copper shape memory alloy casting ingot

The invention discloses a preparation method for high-purity titanium nickel copper shape memory alloy ingots, and relates to the technical field of shape memory alloy preparation. Raw materials are screened, cleaned and dried; the raw materials comprise sponge titanium particles, electrolytic nickel particles, high-purity copper particles and phosphorus copper intermediate alloys; after the driedraw materials are weighed, the materials are paved in a smelting furnace in sequence according to a first preset condition; the materials are smelted according to a vacuum induction smelting technology, wherein the smelting process comprises power supply, degassing, refining and casting; the aftertreatment is performed on ingots after casting according to a second preset condition by adopting a hot isostatic pressing method; and then, the flaw detection, the riser cutting and the bottom cushioning are performed on the ingots after aftertreatment in sequence to obtain high-purity titanium nickel copper ingots. The preparation method achieves the technical effects of convenience to prepare the ingots, controllable and lower content of impurity element O, high content stability of the O element, fine grain structure and great reduction of metallurgy defects.
Owner:西安斯塔克材料科技有限公司

A kind of NdFeB permanent magnet material and its preparation method and magnetic field assisted direct casting device

The invention discloses a neodymium-iron-boron permanent magnet material, a preparation method and a magnetic field auxiliary direct casting device. A main magnet of the device is a circular-ring-shaped magnet which is magnetized in a radial mode. A first disc-shaped repulsion magnet with the magnetic field direction being axially upward is arranged below the center of the main magnet, and a second disc-shaped repulsion magnet which is magnetized in a radial mode is arranged on the periphery of the first repulsion magnet. A regulating magnet is arranged at the upper end of the main magnet, second soft iron is arranged on the upper portion of the regulating magnet, first soft iron is arranged outside the regulating magnet, and a circular-ring-shaped magnet guide magnet which is magnetized downwards in the axial direction is arranged outside the main magnet. The chemical general formula of the neodymium-iron-boron permanent magnet material is [Nd (85-x-y) CoxFeyAlzB (15-z)] (100-a) Ma, wherein in the formula, x+y is larger than or equal to 30 and smaller than or equal to 70, z is larger than or equal to 0 and smaller than or equal to 10, and a is smaller than and equal to 4. Compared with a material prepared without adding magnetic fields, the performance of the neodymium-iron-boron permanent magnet material is greatly improved, the preparation process is simple, cost is low, products are dense, and the neodymium-iron-boron permanent magnet material is suitable for industrial production.
Owner:SOUTH CHINA UNIV OF TECH
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