Fly maggot antimicrobial peptide adjuvant, preparation method thereof, vaccine preparation and application containing the adjuvant
A technology of antimicrobial peptide and peptide adjuvant, which is applied in the field of fly maggot antimicrobial peptide, and achieves the effects of convenient use, simple preparation process and simple method
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Embodiment 1
[0040] Embodiment 1: Preparation of fly maggot antimicrobial peptide
[0041] Take 1 kg of fly maggots, homogenize them with 3% acetic acid aqueous solution in a high-speed tissue masher for 5 minutes, place them in a refrigerator at 4°C overnight, centrifuge, and collect the supernatant; the precipitate is treated with 3% acetic acid aqueous solution in the same way. The two supernatants were combined, heated at 100°C for 1 h, left to stand in a refrigerator at 4°C, and filtered under reduced pressure. The filtrate was concentrated under reduced pressure and freeze-dried to obtain the fly maggot extract. Put the fly maggot extract on D101 macroporous adsorption resin chromatography column, elute with water and 55% ethanol in sequence, collect the 55% ethanol eluate, recover ethanol under reduced pressure, concentrate, and freeze-dry to obtain the fly maggot antimicrobial peptide. Fly maggot antimicrobial peptide is light yellow white powder; ninhydrin reaction is positive; p...
Embodiment 2
[0042] Embodiment 2 contains the hepatitis B vaccine preparation of fly maggot antimicrobial peptide adjuvant
[0043]Weigh 500 μg of fly maggot antimicrobial peptide and 100 μg of recombinant hepatitis B virus surface antigen (rHBsAg), dissolve in 10 ml of normal saline, filter with 0.22 μm microporous membrane, and aseptically dispense, 1 ml each. Each ml contains 50 μg of antimicrobial peptides and 10 μg of rHBsAg.
Embodiment 3
[0044] Example 3 Hepatitis B vaccine preparation containing aluminum glue and fly maggot antimicrobial peptide adjuvant
[0045] Weigh an appropriate amount of fly maggot antimicrobial peptide, dissolve it with physiological saline to make a solution with a concentration of 100 μg / ml, and filter it with a 0.22 μm microporous membrane. The antimicrobial peptide solution was mixed with an equal volume of aluminum-containing adjuvanted hepatitis B surface antigen vaccine stock solution (each ml containing 20 μg of rHBsAg and 500 μg of aluminum hydroxide), mixed evenly, and aseptically dispensed, each 1 ml. Each ml contains 50 μg of maggot antimicrobial peptide, 10 μg of rHBsAg and 250 μg of aluminum hydroxide.
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