WS2 nanowatt/graphene electrochemical lithium storage composite electrode and preparation method
A composite electrode, ene electrochemical technology, applied in the direction of battery electrodes, non-aqueous electrolyte battery electrodes, circuits, etc., to achieve the effect of strong hydrophobicity and strong electrostatic interaction
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[0023] 1) Disperse 2.5mmol of graphene oxide ultrasonically in 60mL of deionized water, then add 0.8mmol of gemini surfactant N-dodecyl propylene diamine bis bromide, and stir well, then add 0.76g ( 6.25mmol) L-cysteine and 1.25mmol ammonium thiotungstate, with constant stirring to completely dissolve L-cysteine and ammonium thiotungstate, adjust the volume to about 80 mL with deionized water;
[0024] 2) Transfer the obtained mixture to a 100 mL hydrothermal reaction kettle, put the reaction kettle in a constant temperature oven, and after hydrothermal reaction at 230°C for 24 hours, let it cool to room temperature naturally, and collect the solid product by centrifugation. And fully wash with deionized water, vacuum drying at 100 ℃, the obtained solid product is heat treated in a nitrogen / hydrogen mixed atmosphere at 800 ℃ for 2h, the volume fraction of hydrogen in the mixed gas is 10%, to prepare WS 2 Nano-watt / graphene composite nano-material, composite nano-material WS 2 ...
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