High-capacity and stable-circulation electrochemical lithium storage composite electrode and preparation method
A composite electrode and electrochemical technology, applied in the direction of battery electrodes, electrode manufacturing, non-aqueous electrolyte battery electrodes, etc., to achieve the effect of strong hydrophobicity and strong electrostatic interaction
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[0025] 1) Disperse 2.5 mmol of graphene oxide ultrasonically in 60 mL of deionized water, then add 0.8 mmol of gemini surfactant N-dodecyl propylene diamine bis bromide, and stir well, then add 0.76 g in turn (6.25 mmol) L-cysteine and 0.3 g (1.25 mmol) sodium molybdate (Na 2 MoO 4 ·2H 2 O), and keep stirring to completely dissolve L-cysteine and sodium molybdate, adjust the volume to about 80 mL with deionized water;
[0026] 2) Transfer the obtained mixture to a 100 mL hydrothermal reactor, put the reactor in a constant temperature oven, and after hydrothermal reaction at 230℃ for 24 h, let it cool to room temperature naturally, and collect the solid by centrifugation The product was thoroughly washed with deionized water, dried in vacuum at 100°C, and the obtained solid product was heat-treated in a nitrogen / hydrogen mixed atmosphere at 800°C for 2h, and the volume fraction of hydrogen in the mixed gas was 10%. MoS was prepared 2 Nano-watt / graphene composite nano-materials,...
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