Method for preparing anti-aging agent 4010NA through modification-catalytic hydrogenation
A technology for catalytic hydrogenation and anti-aging agent, which is applied in the directions of reductive alkylation preparation, organic chemistry, and bulk chemical production, etc. The effect of polyalkyl reduction and alkylation side reactions, suppression of side reactions, and saving of operating costs
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Embodiment 1
[0027] Add RT base, acetone and [Bmim]BF to the ingredients tank 4 , stirred evenly to form a raw material solution, wherein the molar ratio of RT base to acetone is 1:5.5, acetone and [Bmim]BF 4 The volume ratio is 1000:2.5.
[0028] Install the granular C?207 copper-based catalyst in the fixed bed, pass in hydrogen, and adjust the pressure in the fixed bed to 4MPa, and then input acetone solvent at a speed of 50ml / hour. After the solvent is mixed with hydrogen, after pre- The heater then enters the fixed bed reactor. Slowly increase the temperature of the preheater and the fixed bed, and when the temperature reaches 180°C, keep it for several hours until the solvent fills the fixed bed reactor. At this temperature, the system pressure was adjusted to 2.0MPa, the material was replaced with raw material solution, the feed rate was adjusted to 20ml / hour, and the reducing solution after the catalytic hydrogenation reaction overflowed from the top of the fixed-bed reactor. Mov...
Embodiment 2
[0034] Concrete operation condition is the same as embodiment 1, just ionic liquid is made of [Bmim] BF 4 Change to [Bmim]BF 4 With [Bzmim] BF 4 Mixed solution (volume ratio 1:1), the copper-based catalyst was changed from C?207 to F04. The test results are shown in the comparison table 2.
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