Preparation method of bamboo wood anti-mold and preservative

A preservative and wood technology, applied in the fields of botanical equipment and methods, wood impregnation, wood impregnation, etc., can solve the problems of affecting the physical and mechanical properties of the treated wood, the effect of fixation is not obvious, and the effect of anti-mildew and anti-corrosion is not lasting. The effect of improving the anti-bleeding performance, improving the anti-bleeding performance, and improving the anti-mildew and anti-corrosion properties

Active Publication Date: 2016-09-28
CENTRAL SOUTH UNIVERSITY OF FORESTRY AND TECHNOLOGY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, these methods have the disadvantages that the anti-mildew and anti-corrosion effects are not durable, and the physical and mechanical properties of the treated materials are affected.
Some studies have attempted to combine copper with boron compounds and octanoic acid to improve the fixation performance of copper in the treated material. The addition of synergistic additives has reduced the loss of copper anti-mold and preservatives in the treated material, but the effect of improving the fixation of copper is not obvious

Method used

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  • Preparation method of bamboo wood anti-mold and preservative
  • Preparation method of bamboo wood anti-mold and preservative

Examples

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Effect test

Embodiment 1

[0023] A kind of preparation method of bamboo wood antiseptic antifungal agent of the present invention, comprises the following steps:

[0024] 1) Preparation of sol: Weigh 60 parts by weight of tetraethyl orthosilicate at room temperature, slowly drop it into a mixture of 40 parts by weight of absolute ethanol and 30 parts by weight of deionized water, and simultaneously put the mixed solution in a 40°C water bath , stirring; then add an appropriate amount of dilute hydrochloric acid to adjust the pH value to 3-4, and after the reaction is carried out for 30-45min, a uniform sol is obtained;

[0025] 2) Preparation of anti-mildew preservative: under the conditions of bathing and stirring the sol prepared in step 1) at 40°C, slowly add 3 parts by weight of copper sulfate aqueous solution into the sol; then add 5 parts by weight of aminopropyltrimethoxy The base silane is used as a directing agent, fully stirred to make it react, and the required bamboo wood anti-mold preserva...

Embodiment 2

[0029] A kind of preparation method of wood antiseptic antifungal agent of the present invention, comprises the following steps:

[0030] 1) Preparation of sol: Weigh 60 parts by weight of n-butyl titanate at room temperature, slowly drop it into a mixture of 40 parts by weight of absolute ethanol and 30 parts by weight of deionized water, and simultaneously put the mixed solution in a 40°C water bath , stirring; then add an appropriate amount of dilute hydrochloric acid to adjust the pH value to 3-4, and after the reaction is carried out for 30-45min, a uniform sol is obtained;

[0031] 2) Preparation of anti-mildew preservative: Under the conditions of bathing and stirring the sol prepared in step 1) at 40°C, slowly add 3 parts by weight of copper sulfate aqueous solution to the sol, and then add 5 parts by weight of aminopropyl tris Ethoxysilane is used as a guiding agent, and it is fully stirred to make it react, that is, the required bamboo wood anti-mold preservative is ...

Embodiment 3

[0033] A kind of preparation method of wood antiseptic antifungal agent of the present invention, comprises the following steps:

[0034] 1) Preparation of sol: weigh 100 parts by weight of sodium silicate solution with a modulus of 2.8 at room temperature, slowly drop it into a mixture of 55 parts by weight of absolute ethanol and 45 parts by weight of deionized water, and simultaneously Water bath and stir at 60°C; then add an appropriate amount of glacial acetic acid to adjust the pH to 3-4, and react for 30-45 minutes to obtain a uniform sol;

[0035] 2) Preparation of anti-mildew preservative: Under the conditions of bathing and stirring the sol prepared in step 1) at 60°C, slowly add 9 parts by weight of copper chloride aqueous solution to the sol, and then add 10 parts by weight of 3-aminopropane The base triethoxysilane is used as a guiding agent, fully stirred to make it react, and the required bamboo wood anti-mold preservative is prepared.

[0036] Pour the prepare...

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Abstract

The invention discloses a preparation method of a bamboo wood anti-mildew preservative: weighing 60-150 parts by weight of tetraethyl orthosilicate, sodium silicate solution or n-butyl titanate at room temperature, slowly dripping into 40-75 parts by weight Parts of absolute ethanol and 30-60 parts by weight of deionized water in the mixed solution, while the mixed solution is subjected to 40-80 ° C water bath, stirring; then add an appropriate amount of acid to adjust the pH to 3-4, after the reaction is carried out for 30-45min, that is A homogeneous sol is obtained; under the conditions of 40-80°C water bath and stirring of the sol, slowly add 3-12 parts by weight of an aqueous solution of a copper-containing compound into the sol, and then add 5-15 parts by weight of an aminosilane coupling agent as a guide The agent is fully stirred to make it react, and the bamboo wood anti-mildew preservative is prepared. The anti-mildew preservative for bamboo and wood prepared by the invention has excellent anti-loss performance, simple components, simple preparation method, relatively low production cost, friendly environment and little harm to human health.

Description

technical field [0001] The invention belongs to the field of preservatives, and in particular relates to a preparation method of a bamboo and wood anti-mildew preservative. Background technique [0002] There are many kinds of anti-mildew preservatives for bamboo and wood, and copper anti-mold preservatives are the most widely used one. Copper anti-mildew preservatives have been widely used for a century due to their broad-spectrum bactericidal properties, low harm to humans and animals, and environmental friendliness. As we all know, in addition to micronized copper and other nano anti-mold preservatives, copper anti-mold preservatives are a typical type of water-soluble anti-mold preservatives, and their fatal flaw is poor anti-loss performance. [0003] How to improve the loss resistance of copper-containing bamboo wood antifungal preservatives has become a research hotspot and difficulty. Studies have shown that in copper chromium arsenic preservatives (CCA), chromium ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A01N59/20A01N55/10B27K3/52
CPCB27K3/52
Inventor 吴义强杨守禄卿彦
Owner CENTRAL SOUTH UNIVERSITY OF FORESTRY AND TECHNOLOGY
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