Modified titanium dioxide/bamboo charcoal composite environment-friendly aerogel and preparation method thereof
A titanium dioxide and composite technology, which is applied in the field of modified titanium dioxide/bamboo charcoal composite environmental protection airgel and its preparation, can solve the problems of no visible light photocatalysis, small specific surface area of airgel, and uneven pore size distribution. Achieve non-irritating, pore size distribution, strong photocatalysis, and improve the effect of photocatalysis
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Embodiment 1
[0024] Example 1: Dissolve 10 mL of ethyl titanate in 8 mL of absolute ethanol, then add 0.001 g of hexadecyl glucoside and stir evenly to obtain solution A; dissolve 1 mL of 0.004 mol / L silver nitrate solution in water with 0.01 In the mixed solution of mL glacial acetic acid, stir evenly to obtain solution B; drop solution B into solution A, the volume ratio of solution A to solution B is 1:0.06, and then add 2% aluminum borosilicate Potassium 400-mesh bamboo charcoal powder 0.001g, stir evenly, leave still to obtain wet gel, age the wet gel at room temperature for 20h, add absolute ethanol to soak for 5h, remove unreacted liquid in the gel, separate and remove ethanol, Then wash with n-hexane to remove the modified solution; put the washed product in a microwave oven and heat it up to 110°C for 5 hours, and then cool it to room temperature to obtain the modified titanium dioxide / bamboo charcoal composite environmentally friendly airgel; the ratio of the airgel The surface a...
Embodiment 2
[0025] Example 2: Dissolve 10 mL of ethyl titanate in 2 mL of absolute ethanol, then add 0.003 g of cetyl glucoside and stir evenly to obtain solution A; dissolve 2 mL of 0.005 mol / L silver nitrate solution in deionized water and 0.02mL glacial acetic acid mixture, stir evenly to obtain solution B; drop solution B into solution A drop by drop, the volume ratio of solution A to solution B is 1:2, and then add borosilicate mixed with 6% 0.02g of 400-mesh bamboo charcoal powder of Potassium Aluminate, stirred evenly, left to stand to obtain a wet gel, aged the wet gel at room temperature for 20h, added absolute ethanol and soaked for 5h, removed the unreacted liquid in the gel, separated and removed ethanol, and then washed with n-hexane to remove the modified solution; the washed product was placed in a microwave oven and heated to 115°C for 3.5 hours, and then cooled to room temperature to obtain the modified titanium dioxide / bamboo charcoal composite environmentally friendly ai...
Embodiment 3
[0026] Example 3: Dissolve 10 mL of ethyl titanate in 5 mL of absolute ethanol, then add 0.005 g of octadecyl glucoside and stir evenly to obtain solution A; dissolve 3 mL of 0.004 mol / L silver nitrate solution in deionized water and 0.05mL glacial acetic acid mixture, stir evenly to obtain solution B; drop solution B into solution A drop by drop, the volume ratio of solution A to solution B is 1:0.5, and then add borosilicate mixed with 3% 0.003g of 350-mesh bamboo charcoal powder of potassium aluminum acid, stir evenly, and let stand to obtain wet gel, age the wet gel at room temperature for 20h, add absolute ethanol to soak for 5h, remove unreacted liquid in the gel, separate and remove ethanol, and then washed with n-hexane to remove the modified solution; the washed product was placed in a microwave oven and heated to 120°C for 3 hours, and cooled to room temperature to obtain the modified titanium dioxide / bamboo charcoal composite environmentally friendly airgel; the airg...
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