Carbon-coated nickel oxide/metallic nickel and simple synthesis method thereof
A synthesis method and carbon coating technology, applied in the field of new materials and new energy, can solve the problems of expensive instruments, long reaction time, etc., achieve the effect of improving crystal quality, improving conductivity, and overcoming poor conductivity
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Embodiment 1
[0025] Weigh 4 g of ferric nitrate, 1 g of citric acid, and 0.03 g of ammonium nitrate, respectively, to prepare an aqueous solution, stir and dissolve until a transparent solution is obtained. The solution was heated to 60 °C, and the water was continuously evaporated to a viscous gel state. The gel was heated in an environment of 130 °C, and the gel self-propagatingly burned within a few minutes to obtain a black loose powder. The resulting powder was washed in deionized water and dried.
Embodiment 2
[0027] Weigh 4 g of ferric nitrate, 2 g of citric acid and 0.1 g of ammonium nitrate, respectively, to prepare an aqueous solution, stir and dissolve until a transparent solution is obtained. The solution was heated to 100 °C, and the water was continuously evaporated to a viscous gel state. The gel was heated in an environment of 200 °C, and the gel self-propagatingly burned within a few minutes to obtain a black loose powder. The resulting powder was added to ethanol for washing and dried.
Embodiment 3
[0029] Weigh 1.6 g of ferric chloride, 0.2 g of glycine, and 0.5 g of ammonium nitrate, respectively, to prepare an aqueous solution, stir and dissolve to a transparent solution. The solution was heated to 50 °C, and the water was continuously evaporated to a viscous gel state. The gel was heated in an environment of 290 °C, and the gel self-propagatingly burned within a few minutes to obtain a black loose powder. The resulting powder was washed in deionized water and dried.
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