Fire resistant material and preparation method thereof
A technology for refractory materials and raw materials, applied in the field of silica-containing refractory materials and their preparation, can solve the problems of high energy consumption and complex process, and achieve the effects of good formability, wide source of raw materials and excellent application potential.
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Embodiment 1
[0043] Pour the silicone resin and kaolin into the beaker according to the mixture, wherein the silicone resin content is 50%-75%, and the kaolin content is 25%-50%. Stir with a glass rod for 10 minutes to mix evenly. After mixing, a viscous and fluid mixture is obtained. The mixture was precured at 100° C. for 5 h, and stirred with a glass rod every 20 minutes during the precuring process. The purpose of pre-curing is to initially evaporate the solvent in the silicone resin, and the purpose of regular stirring is because the kaolin will condense and form a precipitate during the process, making the two mixed unevenly. Then put the mixture into a specific mold for curing and molding. The curing process is 100°C for 24 hours, and then apply pressure for molding. For kaolin content of 25%, 33% and 50%, the pressure is 5MPa, 7MPa and 10MPa respectively. Then keep it at 200°C for 5 hours, and at 300°C for 5 hours. At this stage, the solvent component xylene in the silicone resin w...
Embodiment 2
[0048] The difference between this example and Example 1 is that the mass ratio of kaolin and silicone resin is 1:3, and the temperature during the heating and oxidation process is 1°C / min, 5°C / min and 10°C / min, after 100°C heat preservation The molding pressure is 5MPa. Other steps are identical with embodiment 1. The performance parameters of the prepared refractories are listed in Table 2.
[0049] Intensity (MPa) and density (g / cm3) of refractories prepared under different heating rates in Table 2 3 )
[0050]
Embodiment 3
[0052] The difference between this example and Example 1 is that the mass ratio of kaolin and silicone resin is 1:2, and the maximum heat treatment temperature is 800°C, 1300°C and 1500°C. Other steps are identical with embodiment 1. The performance parameters of the prepared refractories are shown in Table 3.
[0053] The strength (MPa) and density (g / cm3) of refractory materials prepared under different maximum treatment temperatures in Table 3 3 )
[0054]
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