Preparation method for graphene
A graphene and graphite technology, applied in the field of graphene preparation, can solve the problems of small output and incapable of large-scale production, and achieve the effects of low cost, large industrial application potential, and increased application range
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[0025] Example 1
[0026] The first step is to disperse 10g of natural graphite into 500ml of organic solvent 1-methyl-2-pyrrolidone (NMP) according to the ratio in Table 1, to obtain a graphite suspension with a concentration of 20g / l. The carbon content of natural graphite It is more than 98% graphite powder.
[0027] In the second step, the obtained graphite suspension was sheared in a colloid mill for 5 min. The colloid mill was a JM-5 emulsified asphalt tester with a pressure of 0.1 MPa, and then the sheared graphite suspension was taken out.
[0028] In the third step, the prepared graphite suspension is centrifuged, the centrifuge speed is 500 rpm, and the centrifugation time is 10 min. The supernatant is collected, and then the supernatant is vacuum filtered and dried to obtain graphene. The quality, concentration, yield and efficiency of the prepared graphene are shown in Table 2, as figure 2 The graphene monolayer structure prepared by the present invention is obvious, th...
Example Embodiment
[0029] Example 2
[0030] In the first step, according to the proportional relationship in Table 1, 30 g of natural graphite was dispersed in 500 ml of organic solvent 1-methyl-2-pyrrolidone (NMP) to obtain a graphite suspension with a concentration of 60 g / l.
[0031] The second step is the same as the second step in Example 1.
[0032] The third step is the same as the third step in Example 1. The quality, concentration, yield and efficiency of the graphene prepared are shown in Table 2.
Example Embodiment
[0033] Example 3
[0034] The first step is to disperse 1.8g of natural graphite into 600ml of water in the surfactant sodium dodecylbenzene sulfonate solution according to the ratio in Table 1, to obtain a graphite suspension with a concentration of 3g / l, of which 12 The ratio of the concentration of sodium alkylbenzene sulfonate to the concentration of initial graphite is 1 / 8.
[0035] In the second step, the obtained graphite suspension was poured into a colloid mill and mechanically sheared for 5 minutes at a pressure of 0.1 MPa, and then the graphite suspension after the shearing was taken out.
[0036] In the third step, the prepared graphite suspension is centrifuged (centrifugation speed is 1000 rpm, centrifugation time is 10 min) and the supernatant is collected, and then the supernatant is vacuum filtered, washed, and dried to obtain graphene . The quality, concentration, yield and efficiency of the graphene prepared are shown in Table 2.
[0037] Such as image 3 As shown...
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