High-melting-point heat-conducting electronic material and preparation method thereof
An electronic material with a high melting point technology, which is applied in the field of high melting point thermally conductive electronic materials and its preparation to achieve high melting point and good thermal conductivity
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Embodiment 1
[0016] S1: Add 30 parts of ACS resin, 1 part of titanium dioxide, 2 parts of zinc carbonate and 10 parts of ethyl 9-fluorenylidene acetate into the reactor and stir for 20 minutes at a temperature of 100°C to obtain a mixed solution A;
[0017] S2: Add 15 parts of fumaric acid resin, 0.5 part of sulfazone, 0.5 part of zinc 1-butanethiol and 9 parts of sorbitan trioleate into the reactor and stir for 10 minutes at a temperature of 60°C to obtain a mixed solution B;
[0018] S3: Add 1 part of copper-beryllium alloy rod, 1 part of magnesium thiocyanate and 3 parts of siltianil to 15 parts of leaf alcohol acetal, ultrasonically vibrate for 3 minutes, and then mix it with mixed solution A and mixed solution B at a temperature of 120 Stir the reaction at °C for 1 h; then lower the temperature to room temperature at a rate of 4 °C / min to obtain the high-melting thermally conductive electronic material.
Embodiment 2
[0024] S1: Add 40 parts of ACS resin, 3 parts of titanium dioxide, 5 parts of zinc carbonate and 13 parts of ethyl 9-fluorenylidene acetate into the reactor and stir for 30 minutes at a temperature of 110°C to obtain a mixed solution A;
[0025] S2: Add 25 parts of fumaric acid resin, 3 parts of sulfazone, 2.5 parts of zinc 1-butanethiol and 15 parts of sorbitan trioleate into the reactor and stir for 20 minutes at a temperature of 80°C to obtain a mixed solution B;
[0026] S3: Add 3 parts of copper-beryllium alloy rods, 4 parts of magnesium thiocyanate and 7 parts of siltianil to 20 parts of leaf alcohol acetal, ultrasonically vibrate for 5 minutes, and then mix it with mixed solution A and mixed solution B at a temperature of 140 Stir the reaction at °C for 3 h; then lower the temperature to room temperature at a rate of 8 °C / min to obtain the high-melting thermally conductive electronic material.
Embodiment 3
[0032] S1: Add 32 parts of ACS resin, 2 parts of titanium dioxide, 3 parts of zinc carbonate and 11 parts of ethyl 9-fluorenylidene acetate into the reactor and stir for 20 minutes at a temperature of 100°C to obtain a mixed solution A;
[0033] S2: Add 18 parts of fumaric acid resin, 1 part of sulfazone, 1 part of zinc 1-butanethiol and 11 parts of sorbitan trioleate into the reactor and stir for 20 minutes at a temperature of 60°C to obtain a mixed solution B;
[0034] S3: Add 2 parts of copper-beryllium alloy rods, 2 parts of magnesium thiocyanate and 4 parts of siltianil to 17 parts of leaf alcohol acetal, ultrasonically vibrate for 3 minutes, and then mix it with mixed solution A and mixed solution B at a temperature of 120 Stir the reaction at °C for 1 h; then lower the temperature to room temperature at a rate of 6 °C / min to obtain the high-melting thermally conductive electronic material.
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