Non-stick pan and preparation method thereof
A non-stick pan and buffer layer technology, applied in metal material coating process, superimposed layer plating, coating and other directions, can solve problems such as health hazards, polyvinyl alcohol is not resistant to high temperature, prone to cracking, etc.
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[0029] A kind of preparation method of non-stick pan, it comprises steps:
[0030] S100 coating the buffer layer on the surface of the pot base;
[0031] S200 sequentially washing the surface of the buffer layer with alkali, acid and water; and
[0032] S300 coating a composite cermet layer on the buffer layer through a laser cladding process.
[0033] Wherein, the step S200 includes the step of: first using 5wt% Na on the surface of the buffer layer 2 CO 3 It was cleaned for 5-15 minutes with the assistance of ultrasound, and then washed with 2 wt % dilute acetic acid solution for 5-15 minutes with the assistance of ultrasound, and then washed with deionized water and dried.
[0034] Wherein, alkali washing can remove oil stains and other dirt on the surface of the buffer layer, pickling can remove the oxide layer on the surface of the buffer layer while activating the surface, and washing with water can remove the residual liquid on the surface of the buffer layer.
[00...
Embodiment 1
[0053] First, coat the inner surface of the pot base with a 15-20 μm TiAl layer; 2 CO 3 and 2wt% dilute acetic acid solution were cleaned for 15 minutes under the condition of ultrasonic assistance, then washed with deionized water and dried; finally, a composite cermet layer was coated on the outer surface of the pot base by laser cladding process, the thickness of 50-60 μm.
[0054] Wherein the preparation process of TiAl is as follows: after Ti powder and Al powder are proportioned according to weight ratio 3: 1, add deionized water wherein, make the volume of deionized water and powder raw material be 50% of ball mill tank, use planetary ball mill, The rotational speed was 400rpm, and the ball milling was performed for 20 hours. After the ball milling, the mixed powder was dried at 120°C for 2 hours, and finally the sample was calcined at 1200°C for 4 hours in a vacuum sintering furnace.
[0055] The preparation process of the composite cermet layer: Zr powder, W powder,...
Embodiment 2
[0058] First, coat the inner surface of the pot base with a 15-20 μm TiAl layer; 2 CO 3 and 2wt% dilute acetic acid solution were cleaned for 15 minutes under the condition of ultrasonic assistance, then washed with deionized water and dried; finally, a composite cermet layer was coated on the outer surface of the pot base by laser cladding process, the thickness of 50-60 μm.
[0059] Wherein the preparation process of TiAl is the same as that in Example 1.
[0060] The preparation process of the composite cermet layer: Zr powder, W powder, Mo powder, Ta powder and graphene are mixed according to the weight ratio of 7:1:0.8:0.5:30, and a certain amount of deionized water is added thereto, Make the volume of deionized water and powder raw materials 50% of the ball mill tank, use a planetary ball mill with a rotation speed of 500 rpm, mill for 3 hours, and dry the mixed powder at 120° C. for 2 hours after ball milling. Mix the obtained mixed powder with silica sol to form a p...
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