Systems and methods for continuous separation and conversion of carbonate-rich heavy oil deposits
A heavy oil ore and carbonate technology, which is applied in the petroleum industry and the preparation of liquid hydrocarbon mixtures, etc., can solve the problems of solvent leakage and high energy consumption, and achieve the effects of accelerating the reaction process, simple operation, and reducing environmental pollution
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Embodiment 1
[0037] A method for continuous separation and conversion of carbonate-rich heavy oil ore, the steps are as follows:
[0038] The oil sludge crushed by the crusher A (the carbonate content in the mineral is 33%, the maximum particle size is 5cm) is fed into the mixing-reactor B1 at a speed of 5kg / min, 50kg of oil sand ore, and the concentration of 2mol / L of hydrogen fluoride The mixture of acid and hydrochloric acid (mixed at a volume ratio of 1:1) is fully mixed at 35°C with a solid-to-liquid ratio of 1:3 (mass ratio), ultrasonicated, and reacted for a total of 40 minutes. Let stand for 5 minutes to take out the upper asphalt foam. Discharge the middle solution phase and the solid material at the bottom respectively; when the feeding of B1 is finished, feed to B2, B2 and B1 perform the same operation, switch in turn, such as figure 1 Shown. The recovery rate of the obtained asphalt foam is 99.7%, the residual solid sand and clay in the foam are less than 40% of the total mass of...
Embodiment 2
[0040] A method for continuous separation and conversion of carbonate-rich heavy oil ore, the steps are as follows:
[0041] The oil sand (the carbonate content in the mineral 10.2%, the maximum particle size is 0.5cm) crushed by the crusher A is fed into the mixing-reactor B1 at a speed of 15kg / min. 50kg of oil sand ore, and the concentration of 2mol / L The mixture of hydrofluoric acid and hydrochloric acid (mixed at a volume ratio of 1:1) is fully mixed at 35°C according to a solid-to-liquid ratio of 1:4 (mass ratio), ultrasonicated, reacted for a total of 40 minutes, and left for 5 minutes to take out the upper asphalt foam , And simultaneously discharge the middle solution phase and the solid substance at the bottom; when the feeding of B1 is finished, feed to B2, B2 and B1 perform the same operation, and so on, switch to B3, B4, B5 respectively, such as figure 1 Shown.
[0042] The recovery rate of the obtained asphalt foam is 99.5%, the metal ion concentration in the discharg...
Embodiment 3
[0044] A method for continuous separation and conversion of carbonate-rich heavy oil ore, the steps are as follows:
[0045] The sludge crushed by the crusher A (the carbonate content in the mineral is 83.4%, the maximum particle size is 0.5cm) is fed into the mixing-reactor B1 at a speed of 15kg / min, 50kg of oil sand ore, and formic acid with a concentration of 5 mol / L According to the solid-to-liquid ratio of 1:4 (mass ratio), mix thoroughly at 5℃, microwave, react for a total of 40 minutes, let stand for 5 minutes to take out the upper asphalt foam, and simultaneously discharge the middle solution phase and the bottom solid matter; when B1 After the end of the feeding, feed to B2, B2 and B1 perform the same operation, and so on, switch to B3, B4, B5 respectively, such as figure 1 Shown.
[0046] The recovery rate of the obtained asphalt foam is 99.5%, the metal ion concentration in the discharged solution exceeds 56g / kg, the residual solid sand and clay in the foam are less tha...
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