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Biodiesel

A technology of biodiesel and rice bran oil, which is applied in the fields of biofuel, petroleum industry, fatty acid production, etc. It can solve the problems of complex preparation process, high requirements, and difficulty in industrialization, and achieve simple post-processing, mild reaction conditions, and low cost. low effect

Inactive Publication Date: 2016-09-21
梁红
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, most of the biodiesel formulations are complicated, resulting in complicated subsequent preparation processes and high requirements, making it difficult to realize industrialization

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0008] Material preparation: including the following components by weight: 30 parts of rice bran oil, 30 parts of soybean oil, 5 parts of methanol, 5 parts of ethanol, 1 part of sodium hydroxide, 1 part of potassium hydroxide, 1 part of sodium silicate, and 1 part of zinc acetate , 0.5 part of naphthenic acid, 0.4 part of tallow fatty acid.

[0009] Preparation:

[0010] S1. Add rice bran oil and soybean oil into a reaction kettle with stirring equipment at a stirring speed of 350r / min, then add naphthenic acid, tallow fatty acid, part of methanol and ethanol, and stir at high speed for 1.5 hours at room temperature to form a uniform mixture Emulsion;

[0011] S2, adding zinc acetate to the above emulsion, stirring at high speed for 2 hours;

[0012] S3, dissolving potassium hydroxide and sodium hydroxide in the remaining methanol and ethanol as catalysts, adding them to the emulsion of S2, and reacting under reflux at 60° C. for 1 hour;

[0013] S4. After the reaction is c...

Embodiment 2

[0016] Preparation of materials: including the following components by weight: 40 parts of rice bran oil, 40 parts of soybean oil, 7 parts of methanol, 8 parts of ethanol, 3 parts of sodium hydroxide, 2 parts of potassium hydroxide, 2 parts of sodium silicate, and 2 parts of zinc acetate , 1.2 parts of naphthenic acid, 1.2 parts of tallow fatty acid.

[0017] Preparation:

[0018] S1. Add rice bran oil and soybean oil to a reaction kettle with stirring equipment at a stirring speed of 350r / min, then add naphthenic acid, tallow fatty acid, part of methanol and ethanol, and stir at high speed for 1.5 hours at room temperature to form a uniform mixture Emulsion;

[0019] S2, adding zinc acetate to the above emulsion, stirring at high speed for 2 hours;

[0020] S3, dissolving potassium hydroxide and sodium hydroxide in the remaining methanol and ethanol as catalysts, adding them to the emulsion of S2, and reacting under reflux at 60° C. for 1 hour;

[0021] S4. After the react...

Embodiment 3

[0024] Preparation of raw materials: including the following components by weight: 50 parts of rice bran oil, 50 parts of soybean oil, 10 parts of methanol, 10 parts of ethanol, 5 parts of sodium hydroxide, 3 parts of potassium hydroxide, 3 parts of sodium silicate, and 3 parts of zinc acetate , 2 parts of naphthenic acid, 2 parts of tallow fatty acid.

[0025] Preparation:

[0026] S1. Add rice bran oil and soybean oil to a reaction kettle with stirring equipment at a stirring speed of 350r / min, then add naphthenic acid, tallow fatty acid, part of methanol and ethanol, and stir at high speed for 1.5 hours at room temperature to form a uniform mixture Emulsion;

[0027] S2, adding zinc acetate to the above emulsion, stirring at high speed for 2 hours;

[0028] S3, dissolving potassium hydroxide and sodium hydroxide in the remaining methanol and ethanol as catalysts, adding them to the emulsion of S2, and reacting under reflux at 60° C. for 1 hour;

[0029] S4. After the rea...

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PUM

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Abstract

The invention provides a biodiesel, which comprises the following components in parts by weight: 30 to 50 parts of rice bran oil, 30 to 50 parts of soybean oil, 5 to 10 parts of methanol, 5 to 10 parts of ethanol, 1 to 5 parts of sodium hydroxide, 1 to 3 parts of potassium hydroxide, 1 to 3 parts of sodium silicate, 1 to 3 parts of zinc acetate, 0.5 to 2 parts of naphthenic acid and 0.4 to 2 parts of fany acid. The biodiesel is reasonable in formula, extensive in raw material source, simple in post-treatment, mild in reaction condition, low in energy consumption, high in product yield, low in cost and easy for industrialization.

Description

technical field [0001] The invention relates to the technical field of fuel oil, in particular to biodiesel. Background technique [0002] Diesel is the main power fuel for many large vehicles such as trucks, diesel locomotives and generators. It has the advantages of high power and low price. The demand for diesel in China is very large. The main problem of diesel application is "black smoke". We often Saw a smoky truck on the road. The main cause of black smoke is incomplete combustion, which seriously pollutes the air, such as producing a large amount of particle dust and high CO2 emissions. In order to solve this problem, biodiesel, a substitute for diesel, has been developed. Biodiesel is a high-quality clean diesel that can be extracted from various biomass, so it can be said to be an inexhaustible source of energy. In today's increasingly depleted resources, it is expected to replace petroleum as an alternative fuel. However, most biodiesel formulations are complex...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11C3/00C10L1/02
CPCC10L1/02C11C3/00Y02E50/10
Inventor 梁红
Owner 梁红