Pentadecyl (pentadecenyl) resorcinol polyoxyethylene ether glucoside and its preparation method and use

A technology of m-phenol polyoxyethylene ether-based glucoside and m-phenol polyoxyethylene ether, which is applied in the field of pentadecyl m-phenol polyoxyethylene ether-based glucoside and its preparation, and can solve unmentioned problems

Inactive Publication Date: 2016-11-09
常熟耐素生物材料科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Tyman reacted cardanol and cardol with ethylene oxide respectively to prepare cardanol polyoxyethylene ether surfactants, and investigated the surface activity and biodegradability of these compounds, but did not mention pentadecane (ene ) based meta-diphenol (cardiac alcohol) polyoxyethylene ether-based glucoside surfactant

Method used

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  • Pentadecyl (pentadecenyl) resorcinol polyoxyethylene ether glucoside and its preparation method and use
  • Pentadecyl (pentadecenyl) resorcinol polyoxyethylene ether glucoside and its preparation method and use

Examples

Experimental program
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Effect test

Embodiment 1

[0032] Take 300g of refined cardanol and put it into a high-pressure reactor, add 0.6g of 50% potassium hydroxide solution, and carry out nitrogen replacement. ℃~130℃ for dehydration. After the dehydration is completed, raise the temperature to 135°C-160°C, add 44g of ethylene oxide to carry out the epoxidation reaction, control the temperature of the addition reaction at 130°C-190°C, and control the pressure below 0.3MPa. After the addition reaction is completed, Lower the temperature to 65°C-75°C, add 0.33g of acetic acid to neutralize until the pH value reaches 5.0-8.0, and obtain cardanol polyoxyethylene ether. A certain amount of pentadecyl (en) base metaphenol (cardanol) polyoxyethylene ether, glucose 180g, solid acid TiO 2 / SO 2 -4 and TiO 2 -ZrO 2 / SO 2 -4 Put 3.44g of mixed catalyst into the reactor, stir evenly, reduce the pressure to 4kPa, rapidly raise the temperature to 90-120°C, keep the temperature for 2.5-4.0h, and continuously pump out the generated water...

Embodiment 2

[0034]Take 300g of refined cardanol and put it into a high-pressure reactor, add 0.6g of 50% potassium hydroxide solution, and carry out nitrogen replacement. ℃~130℃ for dehydration. After the dehydration is completed, raise the temperature to 135°C-160°C, add 88g of ethylene oxide to carry out the epoxidation reaction, control the temperature of the addition reaction at 130°C-190°C, and control the pressure below 0.3MPa. After the addition reaction is completed, Lower the temperature to 65°C-75°C, add 0.33g of acetic acid to neutralize until the pH value reaches 5.0-8.0, and obtain cardanol polyoxyethylene ether. A certain amount of pentadecyl (en) base metaphenol (cardanol) polyoxyethylene ether, glucose 180g, solid acid TiO2 / SO2-4 and TiO2-ZrO2 / SO2-4 mixed catalyst 3.88g is dropped into the reactor, Stir evenly, depressurize to 4kPa, rapidly heat up to 90-120°C, keep warm for 2.5-4.0 hours, continuously pump out the generated water until the mixture in the reactor changes ...

Embodiment 3

[0036] Take 300g of refined cardanol and put it into a high-pressure reactor, add 0.6g of 50% potassium hydroxide solution, and carry out nitrogen replacement. ℃~130℃ for dehydration. After the dehydration is completed, raise the temperature to 135°C-160°C, add 132g of ethylene oxide to carry out the epoxidation reaction, control the temperature of the addition reaction at 130°C-190°C, and control the pressure below 0.3MPa. After the addition reaction is completed, Lower the temperature to 65°C-75°C, add 0.33g of acetic acid to neutralize until the pH value reaches 5.0-8.0, and obtain cardanol polyoxyethylene ether. A certain amount of pentadecyl (en) base metaphenol (cardanol) polyoxyethylene ether, glucose 180g, solid acid TiO2 / SO2-4 and TiO2-ZrO2 / SO2-4 mixed catalyst 4.3g is dropped into the reactor, Stir evenly, depressurize to 4kPa, rapidly heat up to 90-120°C, keep warm for 2.5-4.0 hours, continuously pump out the generated water until the mixture in the reactor changes...

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Abstract

The invention discloses pentadecyl (pentadecenyl) resorcinol polyoxyethylene ether glucoside. The pentadecyl (pentadecenyl) resorcinol polyoxyethylene ether glucoside at least comprises components shown in the structural formula (1) and in the structural formula (1), -R1 represents a -C15H25, -C15H27, -C15H29 or -C15H31 straight chain alkane structure, -m represents 0-10 and -n represents 1-3. The invention discloses a preparation method and use of pentadecyl (pentadecenyl) resorcinol polyoxyethylene ether glucoside.

Description

technical field [0001] The invention relates to the technical field of surfactants, in particular to a pentadecyl m-phenol polyoxyethylene ether-based glucoside and a preparation method and application thereof. Background technique [0002] Surfactants can change the properties of gas-liquid, liquid-liquid and liquid-solid interfaces, so that they have various performances such as foaming, defoaming, emulsification, dispersion, penetration, and solubilization. Therefore, surfactants are widely used in various fields of human activities, such as daily chemicals and cosmetics, food and feed processing, leather product processing, chemical fiber processing, textile printing and finishing, pharmaceutical processing, mineral flotation, oil exploration, oil products, etc. Processing, industrial washing and other industrial sectors, known as "the most efficient industrial monosodium glutamate". Although the amount of surfactant is small, it has a great effect. Mainly divided into...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C07H15/08C07H1/00B01F17/56B01F17/42C09K23/42C09K23/56
CPCC07H1/00C07H15/08C09K23/00
Inventor 戴志成刘骥顾斌
Owner 常熟耐素生物材料科技有限公司
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