Polyurethane-compounded cement-based expanded-perlite heat preservation plate and preparing method thereof
A technology of expanded perlite and composite cement, which is applied in the field of preparation of roofing and wall insulation materials. It can solve the problems of expanded perlite's high water absorption, low concrete strength, and large volume shrinkage, and achieve good sound insulation and stable dimensions. Good performance and low thermal conductivity
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Embodiment 1
[0033] This embodiment first prepares A component and B component with two-component polyurethane:
[0034] To prepare component A:
[0035] Put butyl acetate into a reaction kettle equipped with a thermometer, agitator, and reflux condenser, start stirring, add polyethylene adipate diol, heat to 60°C, and then add polymethylene polyphenyl poly Isocyanate, when the temperature rises to 90-100°C, the polymerization reaction begins to occur, keep warm for 2-3 hours, dissolve the ethyl acetate, let the polymer dissolve, finally add acetone, and mix and stir to form a uniform solution, that is, the solid content is 25-35%. Component A in polyurethane adhesives.
[0036] To prepare Component B:
[0037]Put polymethylene polyphenyl polyisocyanate and ethyl acetate into the reaction kettle, start stirring, add small molecule polyol dropwise, control the drop rate, keep the temperature in the range of 60-80°C, after the dropwise addition, keep warm After cooling to room temperature...
Embodiment 2
[0049] This embodiment prepares polyurethane composite cement-based expanded perlite insulation board, including the following steps:
[0050] (1) Take 100 parts of expanded perlite and 1.0 parts of silane coupling agent KH-550 and mix and stir evenly;
[0051] (2) Add 80 parts of cement and 2.0 parts of fiber mesh cloth to the mixture of step (1) and mix and stir evenly;
[0052] (3) Add 0.3 part of redispersible latex powder to the mixture of step (2) and dissolve in 80 parts of water to form a water solution, mix and stir evenly;
[0053] (4) Add 10 parts of component A to the mixture in step (3), then add 0.1 part of nitric acid and 0.1 part of sulfonated melamine-formaldehyde condensate, mix and stir evenly;
[0054] (5) Add 1 part of component B to the mixture in step (4), mix and stir evenly;
[0055] (6) Inject the mixture obtained in step (5) into the mold and level it out, press it with a press according to the compression ratio of 2.0, and hold the pressure for 30...
Embodiment 3
[0061] This embodiment prepares polyurethane composite cement-based expanded perlite insulation board, including the following steps:
[0062] (1) Take 60 parts of expanded perlite and 0.5 parts of silane coupling agent KH-5700 and mix and stir evenly;
[0063] (2) Add 50 parts of cement and 0.15 part of chopped fiber to the mixture of step (1) and mix and stir evenly;
[0064] (3) Add 0.2 parts of redispersible latex powder to the mixture of step (2) and dissolve in 50 parts of water to form a water solution, mix and stir evenly;
[0065] (4) Add 5 parts of component A to the mixture of step (3), then add 0.1 part of chlorine salt, 0.1 part of sulfonated melamine formaldehyde condensate, mix and stir evenly;
[0066] (5) Add 2 parts of component B to the mixture in step (4), mix and stir evenly;
[0067] (6) Inject the mixture obtained in step (5) into the mold and level it out, press it with a press according to the compression ratio of 2.0, and hold the pressure for 30s t...
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