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Method for preparing active carbon from agricultural-forestry residues Chinese chestnut thorn shells

A technology for preparing activated carbon, agricultural and forestry wastes, applied in chemical instruments and methods, other chemical processes, deodorization, etc. The effect of particle strength

Inactive Publication Date: 2016-12-07
旌德县龙强净化材料厂
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

The chemical activation method is to add chemicals to the raw materials, and then heat them in an inert gas medium to activate them; the most representative chemical activation methods are zinc chloride method, phosphate method, calcium chloride method and alkali method; but due to The use of chemicals will bring the following problems: highly corrosive to equipment; pollute the environment; chemicals remain in the activated carbon; a large amount of chemicals are consumed and the cost is high; an external heat source is required and the activation temperature is strictly controlled
[0004] my country is a big producer of chestnuts, and the by-products of the chestnuts produced are chestnut thorn shells (those with thorns on the outside of chestnuts), which are not widely used at present, and are mainly piled up as garbage, which seriously affects environmental sanitation

Method used

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  • Method for preparing active carbon from agricultural-forestry residues Chinese chestnut thorn shells

Examples

Experimental program
Comparison scheme
Effect test

example 1

[0025] 1000 kg of chestnut thorn shells with a drying moisture of 16% are manually sent to the chopping device, and the chopped into short pieces with a length of 0.3 cm, the crushed material is transported to the feed bin of the forming device through a belt conveyor; the feeding speed is controlled, Squeeze the crushed material into blocks (it is enough to form a block, the size is not limited); the block material is transported to the carbonization furnace silo by the belt conveyor; the formed block material enters the carbonization furnace intermittently, and 50kg of ammonium polyphosphate is added to the carbonization furnace , 80kg of melamine and 10kg of sodium silicate are carbonized at 320°C for 5 hours to form carbon blocks; the carbon blocks are cooled to room temperature by a water cooling system and then transported to the feed port of the crusher by a belt conveyor, and the carbon blocks are crushed and screened into 1.5cm*1cm * Unshaped particles with a size of 1...

example 2

[0027] 1000 kg of chestnut thorn shells with a dry moisture content of 22% are manually sent to the chopping device, chopped into short pieces with a length of 0.6 cm, and the crushed materials are transported to the silo of the forming device through a belt conveyor; the feeding is controlled speed, so that the crushed material is extruded into a block; the block material is transported to the carbonization furnace silo by the belt conveyor; the formed block material enters the carbonization furnace intermittently, and 50 kg of potassium pyrophosphate, 80 kg of guanidine and sodium metasilicate are added to the carbonization furnace 10kg is carbonized at 350°C for 8 hours to form carbon blocks; the carbon blocks are cooled to room temperature by a water cooling system and then transported to the feed port of the crusher by a belt conveyor, and the carbon blocks are crushed and screened into amorphous particles with a size of 1.5cm*1cm*1cm ;The unshaped particles are lifted fro...

example 3

[0029] 1000 kg of chestnut thorn shells with a drying moisture of 19% are manually sent into the chopping device, and chopped into short pieces with a length of 0.5 cm, and the crushed material is transported to the feed bin of the forming device through a belt conveyor; the feeding speed is controlled, Squeeze the broken materials into blocks; the block materials are transported to the carbonization furnace silo by the belt conveyor; the formed block materials enter the carbonization furnace intermittently, and 50kg of tartaric acid, 80kg of dicyandiamide and 10kg of sodium silicate are added to the carbonization furnace through 335 Carbonize at ℃ for 6.5 hours to form carbon blocks; the carbon blocks are cooled to room temperature by the water cooling system and then transported to the feed port of the crusher by the belt conveyor. The unshaped particles are lifted to the silo of the activation furnace by the bucket elevator, and then transported into the physical method acti...

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Abstract

A method for preparing activated carbon by utilizing agricultural and forestry waste chestnut thorn shells, the method comprising the following steps: sending the air-dried chestnut thorn shells to a chopping device, and the crushed materials are transported to a silo through a belt conveyor; controlling the feeding speed so that The crushed materials are extruded into blocks and then sent to the carbonization furnace silo; the formed block materials enter the carbonization furnace intermittently, and then add acid source, gas source and inorganic silicon and carbonize at 320-350 °C for 5-8 hours to form carbon blocks; After cooling to normal temperature, it is transported to the crusher for crushing and screening into unshaped particles; the unshaped particles are lifted to the silo of the activation furnace, and transported to the physical method activation converter through a screw conveyor, and activated with water at a temperature of 700-850 ° C to become crude activated carbon; Transport the crude activated carbon to the pickling device for pickling; then wash the activated carbon to neutral through the water washing device; transport the wet activated carbon washed to neutral to the drying device, add nano-zinc oxide to the dried activated carbon, and mix well Activated carbon is obtained, and the activated carbon has high adsorption efficiency.

Description

technical field [0001] The invention relates to a method for preparing activated carbon, in particular to a method for preparing activated carbon by utilizing agricultural and forestry waste chestnut thorn shells. Background technique [0002] Activated carbon is a kind of porous carbon material, which has the advantages of large specific surface area, wide source of raw materials, high mechanical strength, easy regeneration and good stability. Activated carbon is usually obtained by carbonizing and activating raw materials under certain conditions. The main purpose of carbonization is to obtain a carbonized material with initial pores suitable for activation and a certain mechanical strength. The essence of carbonization is that the organic matter in the raw material undergoes pyrolysis reactions, including thermal decomposition reactions and polycondensation reactions. The main purpose of activation is to prepare activated carbon with high specific surface area; activatio...

Claims

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Application Information

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IPC IPC(8): B01J20/20B01J20/30C01B31/12A61L9/00A61L101/30
CPCB01J20/20A61L9/00A61L2209/21B01J20/06B01J2220/4881C01P2006/12C01P2006/90
Inventor 强昌余
Owner 旌德县龙强净化材料厂
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