A catalyst for producing divinylbenzene, its preparation method and use
A divinylbenzene and catalyst technology, which is applied in the field of catalysts for producing divinylbenzene, can solve the problems of low catalyst activity, low conversion rate of raw materials, and high reaction energy consumption, and achieves high catalyst activity, high ethylbenzene conversion rate, and high selectivity. good effect
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0023] A catalyst for the production of divinylbenzene, its composition is the following components in parts by weight:
[0024] 12 parts of single-layer graphene;
[0025] 25 parts of aluminum trichloride;
[0026] 60 parts ferric chloride;
[0027] 3 parts copper chloride.
[0028] The catalyst is a graphene-supported aluminum-iron-copper catalyst, and its preparation method is carried out as follows:
[0029] Weigh 12 parts by weight of single-layer graphene, 25 parts of aluminum trichloride, 60 parts of ferric chloride and 3 parts of copper chloride, mash, mix well, add deionized water, make the mixture humidified to kneadable, and then Carry out wet material kneading, extrude into spherical particles, the diameter of spherical particles is 7~10mm. Then aged at room temperature for 12 hours, dried at 120°C for 6 hours, and calcined at 500°C for 3 hours to obtain catalyst 1.
[0030] The graphene-supported aluminum-iron-copper catalyst prepared by the present invention...
Embodiment 2
[0034] A catalyst for the production of divinylbenzene, its composition is the following components in parts by weight:
[0035] 11 parts of bilayer graphene;
[0036] 25 parts aluminum silicate;
[0037] 62 parts iron acetate
[0038] 2 parts copper acetate.
[0039] The catalyst is a graphene-supported aluminum-iron-copper catalyst, and its preparation method is carried out as follows:
[0040] Weigh 11 parts by weight of double-layer graphene, 25 parts of aluminum silicate, 62 parts of iron acetate and 2 parts of copper acetate, mash, mix well, add deionized water to make the mixture humidified enough to be kneaded, and then carry out wet material Knead and extrude into spherical particles (ball diameter 7~10mm). Aged at room temperature for 10 hours, dried at 130°C for 4 hours, and calcined at 520°C for 2.5 hours to obtain catalyst 2.
[0041] The graphene-loaded aluminum-iron-copper catalyst prepared by the present invention can be used to produce divinylbenzene, the...
Embodiment 3
[0043] The catalyst for producing divinylbenzene, its composition is the following components in parts by weight:
[0044] 5 parts multilayer graphene;
[0045] 14 parts aluminum sulfate;
[0046] 80 parts iron sulfate;
[0047] 1 part copper sulfate.
[0048] The catalyst is a graphene-supported aluminum-iron-copper catalyst, and its preparation method is carried out as follows:
[0049] Weigh 5 parts by weight of multi-layer graphene, 14 parts of aluminum sulfate, 80 parts of iron sulfate and 1 part of copper sulfate, mash them, mix them evenly, add deionized water, make the mixture humidified enough to be kneaded, and then carry out wet material kneading , extruded into spherical particles (ball diameter 7 ~ 10mm). Aged at room temperature for 14 hours, dried at 100°C for 8 hours, and calcined at 480°C for 3.5 hours to obtain catalyst 3.
[0050] The graphene-loaded aluminum-iron-copper catalyst prepared by the present invention can be used to produce divinylbenzene, t...
PUM
| Property | Measurement | Unit |
|---|---|---|
| diameter | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
Login to View More 
PatSnap Eureka turns technology decisions into work you can execute. Powered by our Innovation Knowledge Graph, it runs expert workflows across engineering, life sciences, materials and intellectual property. Get your review-ready output in minutes.
