Preparation method of hydroxyl-ferric oxide/graphene oxide composite material and application of hydroxyl-ferric oxide/graphene oxide composite material
A technology of iron oxyhydroxide and composite materials, applied in chemical instruments and methods, other chemical processes, water/sewage treatment, etc., can solve the problems of high operating cost, easy to be blocked, high toxicity, etc., and achieve rich oxygen-containing groups , efficient adsorption, and large specific surface area
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Embodiment 1
[0025] Graphite powder and potassium permanganate are in a mass ratio of 1:1, add sulfuric acid and phosphoric acid with a volume ratio of 8:1 mixed acid, and heat in a water bath at 50°C for 2 hours. The oxidized graphite is filtered, dried and ground into powder for later use.
[0026] The mass of graphite oxide and the volume of deionized water are 1g:50ml, mixed and dispersed for 5-10min to prepare a 0.02g / ml graphene oxide suspension.
[0027] Fe(NO 3 ) 3` 2H 2 O and NaOH were mixed in 100ml deionized water for 30min according to the mass ratio of 1.2:1, and kept in an oven at 150°C for 24 hours.
[0028] Mix the obtained iron oxyhydroxide mass with deionized water volume according to 0.5g:50ml, and disperse for 5 minutes to prepare 0.1g / ml iron oxyhydroxide suspension. The uniformly dispersed iron oxyhydroxide suspension was added to the dispersed graphene oxide suspension, and the mixed solution was dispersed for 5-10 minutes, and kept in an oven at 120° C. for 24 h...
Embodiment 2
[0031] Graphite powder and potassium permanganate are in a mass ratio of 1:2, add sulfuric acid and phosphoric acid with a volume ratio of 7:1 mixed acid, and heat in a water bath at 50°C for 2 hours. The oxidized graphite is filtered, dried and ground into powder for later use.
[0032] The mass of graphite oxide and the volume of deionized water were mixed according to 1g:50ml, and dispersed for 5-10min to prepare a 0.02g / ml graphene oxide suspension.
[0033] Fe(NO 3 ) 3` 2H 2 O and NaOH were added into 100ml deionized water according to the mass ratio of 1:1, mixed for 30min, and kept in an oven at 120°C for 24 hours.
[0034] The mass of the obtained iron oxyhydroxide and the volume of deionized water were mixed according to 1g:50ml, and dispersed for 5 minutes to prepare a 0.2g / ml iron oxyhydroxide suspension. The uniformly dispersed iron oxyhydroxide suspension was added to the dispersed graphene oxide suspension, and the mixed solution was dispersed for 5-10 minute...
Embodiment 3
[0037] Graphite powder and potassium permanganate are in a mass ratio of 1:3, add sulfuric acid and phosphoric acid with a volume ratio of 6:1 mixed acid, and bathe in water at 50°C for 2 hours. The oxidized graphite is filtered, dried and ground into powder for later use.
[0038] The mass of graphite oxide and the volume of deionized water are 1g:50ml, mixed and dispersed for 5-10min to prepare a 0.02g / ml graphene oxide suspension.
[0039] Fe(NO 3 ) 3` 2H 2 O and NaOH were added into 100ml deionized water according to the mass ratio of 0.5:1, mixed for 30min, and kept in an oven at 120°C for 24 hours.
[0040] The mass of the obtained iron oxyhydroxide and the volume of deionized water were mixed according to 1g:50ml, and dispersed for 5 minutes to prepare a 0.2g / ml iron oxyhydroxide suspension. The uniformly dispersed iron oxyhydroxide suspension was added to the dispersed graphene oxide suspension, and the mixed solution was dispersed for 5-10 minutes, and kept in an ov...
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