Production method of high-strength AGM partition plate
A production method and high-strength technology, applied in electrochemical generators, nanotechnology, electrical components, etc., can solve the problem that the thickness of the separator cannot be well controlled, the consistency of the pore size of the separator is affected, and the pore size distribution of the separator is not uniform. problems such as uniformity, to avoid chronic short circuits, low production costs, and good mechanical strength
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Embodiment 1
[0029] (1) Preparation of modified nano-silicon nitride: Add nano-silicon nitride to the modified liquid and ultrasonically disperse, filter and dry to obtain modified nano-silicon nitride. The modified liquid consists of the following components by mass percentage Composition: 50% polytetrafluoroethylene dispersion emulsion, 0.2% quaternary ammonium salt, 0.5% polyoxyethylene stearate, 0.3% silane coupling agent KH-550, and the balance is water;
[0030] (2) Preparation of modified basalt mineral fibers: Add basalt mineral fibers with a diameter of 3 μm and a length of 3 mm into chlorosulfonic acid, heat to 100°C to swell for 3 hours, cool, filter, wash the filtrate with water until the pH is neutral, and dry in vacuum , and then added to the sizing agent for soaking for 60 minutes and then dried at 105°C to obtain the modified basalt mineral fiber. The sizing agent is composed of the following components by mass percentage: 5% epoxy resin emulsion, 0.5% polyurethane emulsion,...
Embodiment 2
[0038] (1) Preparation of modified nano-silicon nitride: Add nano-silicon nitride to the modified liquid and ultrasonically disperse, filter and dry to obtain modified nano-silicon nitride. The modified liquid consists of the following components by mass percentage Composition: 40% polytetrafluoroethylene dispersion emulsion, 0.1% quaternary ammonium salt, 0.3~0.5% polyoxyethylene stearate, 0.1% silane coupling agent KH-550, and the balance is water;
[0039] (2) Preparation of modified basalt mineral fibers: add basalt mineral fibers with a diameter of 1 μm and a length of 1 mm into chlorosulfonic acid, heat to 80°C to swell for 1 hour, cool, filter, wash the filtrate with water until the pH is neutral, and dry in vacuum , and then added to the sizing agent for soaking for 30 minutes and then dried at 95°C to obtain modified basalt mineral fiber. The sizing agent is composed of the following components by mass percentage: 3% epoxy resin emulsion, 0.3% polyurethane emulsion, 0....
Embodiment 3
[0047] (1) Preparation of modified nano-silicon nitride: Add nano-silicon nitride to the modified liquid and ultrasonically disperse, filter and dry to obtain modified nano-silicon nitride. The modified liquid consists of the following components by mass percentage Composition: 45% polytetrafluoroethylene dispersion emulsion, 0.15% quaternary ammonium salt, 0.4% polyoxyethylene stearate, 0.2% silane coupling agent KH-550, and the balance is water;
[0048] (2) Preparation of modified basalt mineral fibers: Add basalt mineral fibers with a diameter of 2 μm and a length of 2 mm into chlorosulfonic acid, heat to 90°C to swell for 2 hours, cool, filter, wash the filtrate with water until the pH is neutral, and vacuum After drying, soak in the sizing agent for 40 minutes and then dry at 100°C to obtain the modified basalt mineral fiber. The sizing agent is composed of the following components by mass percentage: 4% epoxy resin emulsion, 0.4% polyurethane emulsion, 0.4 % silane coup...
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