A kind of ev71-vp1 hand, foot and mouth disease polypeptide vaccine and its preparation method and application
A technology of EV71-VP1, hand, foot and mouth disease, applied in the field of immune biomedicine, can solve problems such as harmful effects on the human body
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Embodiment 1
[0026] Example 1 Detection of Serum Antibodies in Rehabilitated Children
[0027] Collect serum sample information of clinical children: Liu Zhehan, Liu Yueyue, Wu Linman, Gao Junhao, Chen Yixuan, Zhou Yutong. Use human enterovirus EV71 IgG ELISA kit to detect serum antibody concentration, the specific operation method is as follows:
[0028] Steps:
[0029] 1. Dilution and sample addition of the standard: Set 10 wells of the standard on the enzyme-labeled plate, add 100ul of the standard to the first and second wells, and then add the standard to the first and second wells Dilute 50ul, mix well; then take 100ul from the first well and the second well, add to the third well and the fourth hole respectively, then add 50ul standard diluent to the third and fourth well, mix well; Then take 50ul from the third hole and the fourth hole and discard, then add 50ul to the fifth and sixth holes respectively, then add 50ul of the standard dilution solution to the fifth and sixth holes...
Embodiment 2
[0041] Example 2 Synthetic polypeptide coated ELISA plate and evaluation and screening of polypeptide immune effect
[0042] 1. The buffer solution is prepared as follows:
[0043] ①Coating solution: 0.05mol / L carbonate buffer solution (pH9.6)
[0044] 0.75g sodium carbonate, 1.46g sodium bicarbonate, add deionized water to make the volume to 500ml.
[0045] ②0.02mol / L phosphate buffer (pH7.4)
[0046] 0.2g potassium dihydrogen phosphate, 2.90g disodium hydrogen phosphate, 8g sodium chloride, add deionized water to make up to 1000ml.
[0047] ③Antibody diluent: 0.02mol / LPBS(pH7.4)+0.2%BSA
[0048] Add 0.2gBSA to the prepared 0.02mol / L phosphate buffer solution to dissolve and quantify to 100g.
[0049] ④Blocking solution: 0.05mol / L carbonate buffer (pH9.6)+2.0%BSA
[0050] Add 2.0g of BSA to the prepared 0.05mol / L carbonate buffer solution to dissolve and quantify to 100g.
[0051] ⑤Washing solution: 0.02mol / LPBS(pH7.4)+0.05%Tween-20
[0052] Dissolve 50ul of Tween-20 i...
Embodiment 3
[0078] Example 3 In vivo experiments to further verify and evaluate the immune effect of polypeptides
[0079] 1. Model construction of immune mice (Shanghai Experimental Animal Center, Chinese Academy of Sciences)
[0080] Dissolve the obtained No. 2 polypeptide, No. 4 polypeptide, and No. 8 polypeptide in 0.9% sodium chloride solution to make the final concentration 1 mg / ml, and mix with the same volume of Freund's complete adjuvant (purchased from Roche Pharmaceuticals) , to make a polypeptide vaccine. Balb / c mice (purchased from Shanghai Experimental Animal Center, Chinese Academy of Sciences) used 12 6-8 week old female Balb / c healthy mice, divided into 4 groups (No. 2 polypeptide group, No. 4 polypeptide group, and No. 8 polypeptide group) Group) Inject 0.1ml of the above polypeptide solution into the abdominal cavity, and repeat the immunization one week later. The heat-inactivated virus is used as a positive control, and the hepatitis B virus surface antigen is used a...
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