Zr/chitosan composite adsorbent for adsorbing Pb<2+> in water body and preparation method thereof
A composite adsorption and chitosan technology, applied in the fields of adsorption water/sewage treatment, water/sludge/sewage treatment, chemical instruments and methods, etc. The effect of chemical promotion and simple preparation process
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[0024] The first aspect of the present invention provides a method for adsorbing Pb in water 2+ The preparation method of Zr / chitosan composite adsorbent, comprises the following steps:
[0025] (1) Preparation of chitosan colloid: dissolving chitosan in acetic acid solution, stirring and sonicating to prepare chitosan colloid;
[0026] (2) Preparation of zirconium oxychloride solution: dissolving zirconium oxychloride octahydrate in deionized water to prepare zirconium oxychloride solution;
[0027] (3) Mix the chitosan colloid described in step (1) with the zirconium oxychloride solution described in step (2), stir and sonicate to obtain a uniformly dispersed mixed solution;
[0028] (4) Cross-linking reaction: adding aldehyde to the mixed solution described in step (3), stirring, drying and grinding to obtain the Zr / chitosan composite adsorbent.
[0029] In the step (1) of the embodiment of the present invention, the stirring time for preparing the chitosan colloid is 2-4...
Embodiment 1
[0048]Weigh 1.0 g of chitosan, dissolve it in 36 mL of 2% acetic acid solution, stir at room temperature for 3 h, and then sonicate for 30 min to obtain chitosan colloid; weigh 0.8 g of zirconium oxychloride octahydrate and disperse it in 10 mL of deionized water , stirred at room temperature for 3 hours, and ultrasonicated for 30 minutes to obtain a zirconium oxychloride solution; pour the zirconium oxychloride solution into the chitosan colloid, stirred at room temperature for 24 hours, and then ultrasonicated for 1 hour to make it fully mixed to obtain a uniformly dispersed mixed solution; 4.6 mL of glutaraldehyde solution with a volume ratio of 1% was added dropwise to the mixed solution of zirconium oxychloride and chitosan colloid, stirred for 1 h to cause a cross-linking reaction, and then dried in an oven at 55 °C for 36 h to obtain dry The Zr / chitosan composite material is ground, and the Zr / chitosan composite material is ground to obtain a powdery Zr / chitosan composit...
Embodiment 2
[0051] Weigh 1.0g of chitosan, dissolve it in 36mL of 2% acetic acid solution, stir at room temperature for 3h, and then sonicate for 30min to obtain chitosan colloid; weigh 1.6g of zirconium oxychloride octahydrate and disperse it in 10mL of deionized water, Stir at room temperature for 3 hours, and sonicate for 30 minutes to obtain a zirconium oxychloride solution; pour the zirconium oxychloride solution into chitosan colloid, stir at room temperature for 24 hours, and then sonicate for 1 hour to make it fully mixed to obtain a uniformly dispersed mixed solution; 4.6 mL of glutaraldehyde solution with a ratio of 1% was added dropwise to the mixed solution of zirconium oxychloride and chitosan colloid, stirred for 1 h to cause a cross-linking reaction, and then dried in an oven at 55 °C for 36 h to obtain dry Zr / chitosan composite material, grinding the above Zr / chitosan composite material to obtain powdered Zr / chitosan composite adsorbent.
[0052] Use Pb with an initial con...
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