Yttrium-ferrous alloy and preparation method thereof
A ferroalloy, yttrium-iron technology, applied in the field of yttrium-iron alloy and its preparation, can solve problems such as high local concentration of rare earth metals, high requirements for smelting temperature, and influence on product consistency, and achieve broad development and market prospects, high product quality, and low cost. low effect
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[0036] The preparation technology of the yttrium-iron alloy used for producing rare earth steel comprises the following steps:
[0037] Step 1: Graphite is used as the electrolytic cell, the graphite plate is used as the anode, the iron rod is used as the self-consumable cathode, and there is a receiver containing the alloy under the cathode;
[0038] The material of the receiver can be one of iron, rare earth oxide, and boron nitride.
[0039] Step 2: In the fluoride molten salt electrolyte system of yttrium fluoride and lithium fluoride, yttrium oxide is used as the electrolytic raw material, and direct current is applied to electrolyze to obtain the yttrium-iron master alloy;
[0040] Step 3: Using the yttrium-iron master alloy and iron as raw materials, the yttrium-iron alloy is prepared by a melting method.
[0041] The equipment for melting yttrium-iron master alloy into yttrium-iron alloy is an intermediate frequency induction furnace. The melting process is carried o...
Embodiment 1
[0047] A Φ650mm circular graphite electrolytic cell is used, the anode is composed of four graphite plates, the electrolyte contains 85wt% yttrium fluoride and 15wt% lithium fluoride, the cathode is a Φ70mm pure iron rod, the average current intensity is 6000A, and the anode current density is 0.5- 1.0A / cm 2 , cathode current density 7-11A / cm 2, the electrolysis temperature is maintained at 950-1050°C, continuous electrolysis for 720 hours, 5.35 tons of yttrium oxide is consumed, and 5.43 tons of yttrium-iron alloy is produced, the average yttrium content is 76%, the current efficiency is 85%, the rare earth yield is 95%, and the alloy composition The results are shown in Table 1.
[0048] Table 1 yttrium-iron master alloy composition analysis results / wt%
[0049] Y Fe C O P S Si mn 76.00 23.75 0.0085 0.0094 <0.01 <0.005 <0.01 <0.005
[0050] Using the yttrium-iron master alloy prepared in this example as a raw material, take 3 kg of yttriu...
Embodiment 2
[0054] A Φ400mm circular graphite electrolytic cell is used. The anode is composed of four graphite plates. The electrolyte contains 85wt% yttrium fluoride and 15wt% lithium fluoride. The cathode is a Φ50mm pure iron rod. The average current intensity is 2800A, and the anode current density is 0.5- 1.5A / cm 2 , cathode current density 6-10A / cm 2 , the electrolysis temperature was maintained at 950-1050°C, continuous electrolysis for 360 hours, 1342kg of yttrium oxide was consumed, and 1339kg of yttrium-iron alloy was obtained, with an average yttrium content of 75%, a current efficiency of 90%, and a rare earth yield of 95%. The alloy composition results are shown in the table 3.
[0055] Table 3 yttrium-iron master alloy composition analysis results / wt%
[0056] Y Fe C O P S Si mn 75.0 24.86 0.0085 0.0094 <0.01 <0.005 0.011 <0.005
[0057] Using the yttrium-iron master alloy prepared in this example as a raw material, take 5 kg of the yttri...
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