Magnetic photocatalysis nanometer composite material using bismuth oxide and nickel ferrite and preparation method thereof
A technology of nanocomposite materials and photocatalytic materials, which is applied in the field of magnetic photocatalytic nanocomposite materials and their preparation, can solve the problems of limited application and large energy gap, and achieve the effects of recycling, expanding the scope of application and reducing costs
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Embodiment 1
[0016] In Example 1 of the present invention, a method for preparing a magnetic photocatalytic nanocomposite material using bismuth oxide and nickel ferrite comprises the following steps:
[0017] 1) For the preparation of ferroferric oxide, iron salt, stabilizer and reducing agent are added to the alcohol solvent according to the mass ratio of 1:0.2:1, and after complete dissolution, a solution with an iron ion concentration of 0.04M is obtained; the obtained solution is transferred to In the high-pressure reactor, after reacting at a temperature of 180°C for 8 hours, a black product was obtained, and the black product was fully washed with deionized water and absolute ethanol respectively, and after drying, finally obtained ferric oxide nanoparticles ;
[0018] 2) To prepare nickel ferrite, fully dissolve nickel nitrate and ferric nitrate in deionized water in proportion, adjust the pH to 13 with alkaline solution a to obtain mixed solution A; transfer mixed solution A to th...
Embodiment 2
[0022] In Example 2 of the present invention, a method for preparing a magnetic photocatalytic nano-composite material using bismuth oxide and nickel ferrite comprises the following steps:
[0023] 1) For the preparation of ferric oxide, iron salt, stabilizer and reducing agent are added to the alcohol solvent according to the mass ratio of 1:0.55:2, and after complete dissolution, a solution with an iron ion concentration of 0.12M is obtained; the obtained solution is transferred to In the high-pressure reactor, after reacting at a temperature of 200°C for 9 hours, a black product was obtained, and the black product was fully washed with deionized water and absolute ethanol respectively, and after drying, finally obtained ferric oxide nanoparticles ;
[0024] 2) To prepare nickel ferrite, fully dissolve nickel nitrate and ferric nitrate in deionized water in proportion, adjust the pH to 13.5 with alkaline solution a to obtain mixed solution A; transfer mixed solution A to the...
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