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230 results about "Nickel ferrite" patented technology

Nickel ferrite, for instance, is NiFe2O4, and manganese ferrite is MnFe2O4; both are spinel minerals. The garnet mineral known as YIG, containing the rare-earth element yttrium, has the formula Y3Fe5O12; it is used in microwave circuitry.

N-doped graphene/nickel ferrite nanometer compound material and preparation thereof

The invention discloses an N-doped graphene/nickel ferrite nanometer compound material and a preparation method thereof. The preparation method comprises the following steps: performing ultrasonic dispersion on graphite oxide in water, thereby acquiring a graphite oxide solution; adding ferric nitrate and nickel nitrate into the graphite oxide solution and continuing to perform ultrasonic dispersion; adding urea into the mixed solution; transferring the mixed solution into a three-neck flask; after oil-bath heating reaction, centrifugally washing and drying a product, thereby acquiring the N-doped graphene/nickel ferrite nanometer compound material. According to the method, the urea is adopted for reducing the graphite oxide; while reducing, nitrogen atoms are doped on the surface of the graphene; the surface chemical property of the graphene is changed and the surface defect of a chemical method for preparing the graphene is overcome by the doping of the nitrogen atoms; alkalinity is supplied through the urea hydrolysis, so that nickel ferrite is formed on the surface of the N-doped graphene; the accumulation and agglomeration of the graphene in layers can be further stopped by the nanometer particles of the nickel ferrite, so that the electrochemical property of the compound material is increased.
Owner:NANJING UNIV OF SCI & TECH +1

Preparation method of heterogeneous Fenton catalyst, and method for visible photocatalytic degradation of organic pollutants

The invention provides a preparation method of a heterogeneous Fenton catalyst. The preparation method comprises the following steps: weighing ferric trichloride or ferric nitrate and nickel sulfate which are raw materials according to a molar ratio of Fe:Ni of 2:1, respectively dissolving the raw materials in ultrapure water to obtain two solutions, and uniformly mixing to obtain a mixed solution; and adding certain masses of NaOH, and graphene or graphite oxide or active carbon to the mixed solution, stirring, transferring to a reaction kettle, heating for 10min, separating in a magnetic field, washing, and drying to obtain the heterogeneous Fenton catalyst. The invention also provides a method for the visible photocatalytic degradation of organic pollutants through using the heterogeneous Fenton catalyst. The heterogeneous Fenton catalyst prepared through the preparation method is mixed with oxalic acid to degrade organic stimulating pollutants under visible lights. The organic pollutant degradation method is simple and is easy to implement, the catalyst can be separated from the solution through the applied magnetic field, and the carbon material-nickel ferrite composite catalyst can be recycled; and the method enables the chroma of polluted water to be rapidly and effectively removed.
Owner:SUZHOU UNIV OF SCI & TECH

Preparation method of nickel ferrite based magnetic loaded type titanium dioxide photo-catalyst

The invention provides a preparation method of nickel ferrite based magnetic loaded type titanium dioxide photo-catalyst with micron grade micron order as carrier; the preparation process includes the following steps: adding green copperas solution and oxalic acid solution into the nickel salt solution for reaction to obtain the mixture precipitate of oxalate of nickel oxalate and iron oxalate; then baking to obtain the micron grade nickel ferrite powder; adding the titanic sulfate solution into the suspension of micron grade nickel ferrite powder so as to crystallize the titanium ions on the suspended particulates in the suspension to form a wrapping layer and obtain the nickel ferrite based magnetic loaded type titanium dioxide photo-catalyst product. The magnetic loaded type titanium dioxide photo-catalyst prepared by the method of the invention has good dispersibility; and the particle diameter of the particles is about 5 mum; the titanium dioxide is obviously wrapping on the surface of the nickel ferrite to form a core/shell structure with large wrapping capacity as well as adjustable and homogenous distribution; the specific surface is 90-110 m/g; and the photo-catalyst has the feature of strong soft magnetism, can be rapidly recycled in aqueous solution and has higher catalytic activity, so that organic wastewater can be completely degraded. The preparation technology is simple, the cost is low, and large-scale production is easily realized.
Owner:GUIZHOU BRANCH CHINA ALUMINUM IND

Preparation method of reduced graphene oxide/multi-walled carbon nanotube/nickel ferrite three-element nano composite wave-absorbing material

The invention discloses a reduced graphene oxide / multi-walled carbon nanotube / nickel ferrite (RGO / MWCNTs / NiFe2O4) three-element nano composite wave-absorbing material and a preparation method thereof.The RGO / MWCNTs / NiFe2O4 three-element nano composite material with a local three-dimensional conducting network structure is prepared by adopting graphene oxide (GO), the multi-walled carbon nanotube,nickel nitrate hexahydrate and iron nitrate nonahydrate as precursors and carrying out one-step hydrothermal reaction. The preparation method is pollution-free and environmentally friendly, has no production of any toxic and harmful side products, and is simple in preparation process and low in cost; the prepared three-element nano composite wave-absorbing material is strong in capability of absorbing electromagnetic waves, wide in absorbing frequency band, small in thickness and low in density, can realize effective absorption of the electromagnetic waves with different wavebands by adjusting the content of MWCNTs in the composite material and the thickness of a coating layer, and has an important application value in the fields of electromagnetic absorption and electromagnetic shielding.
Owner:ANHUI UNIV OF SCI & TECH

Nickel ferrite-copper metal ceramic inert anode material and preparation method

The invention relates to a nickel ferrite-copper metal ceramic inert anode material which comprises a ceramic phase and a metal phase, wherein the ceramic phase is nickel ferrite or nickel ferrite base composite ceramic; and the metal phase consists of metal copper and cuprous oxide, and the cuprous oxide accounts for 1-20% of the total mass of the metal phase. In the preparation process, the content of the cuprous oxide in the metal phase is controlled through controlling the oxygen partial pressure of a nitrogen protection atmosphere so as to improve the wettability of the nickel ferrite and the copper and achieve the sintering infiltration preparation of the ceramic phase and the metal phase. The metal phase and the ceramic phase of the nickel ferrite-copper metal ceramic inert anode material are in a three-dimensional reticular through structure, wherein the sintering density is higher than 98%, the electric conductivity of the metal ceramic material is more than 200S/cm at a temperature of 900 DEG C, the heat conductivity is up to 40W/(m.K) at the room temperature, and the metal ceramic material cannot be cracked through temperature difference thermal shock at the temperature of 400 DEG C. The problems of difficult sintering densification of the nickel ferrite and the copper, sintering overflow of the metal phase and material thermal shock and cracks are effectively solved, and compared with a material prepared by a conventional mixed powder sintering process, the electric conductivity and the thermal shock resistance of the nickel ferrite-copper metal ceramic material are greatly improved.
Owner:CENT SOUTH UNIV

Method for preparing graphene/ferrite composite nanometer microspheres having high magnetic-electric performances

The invention belongs to the field of novel material preparation and provides a method for preparing graphene/ferrite composite nanometer microspheres having high magnetic-electric performances. Ferrites are manganous ferrite and nickel ferrite. According to the method, first graphene oxide is prepared, and then graphene/manganous ferrite or graphene/nickel ferrite composite nanometer microspheres are synthesized in one step through a hydrothermal method (a solvothermal method). The synthesizing method is simple. The obtained graphene/manganous ferrite or graphene/nickel ferrite composite nanometer microspheres are high in specific surface area and have high magnetism; and by controlling the ratio of graphene oxide to manganous ferrite or the ratio of graphene oxide to nickel ferrite, it is guaranteed that the composite nanometer microspheres can achieve very good wave-absorbing properties. Prepared graphene/manganous ferrite and graphene/nickel ferrite nanocomposite materials not only have excellent electromagnetic loss performances, but also can serve as a light and high-strength wave-absorbing material to be applied to the fields of sewage treatment, energy, stealth and electronics.
Owner:UNIV OF ELECTRONICS SCI & TECH OF CHINA

Preparation method of ultrathin paper-base wave-absorbing material

The invention relates to a preparation method of an ultrathin paper-base wave-absorbing material, belonging to the technical field of electromagnetic shielding. The preparation method comprises the following steps: acidifying a multi-walled carbon nanotube which serves as a carrier by virtue of concentrated nitric acid to generate oxygen-containing groups on the surface of the carbon nanotube so as to provide depositing sites for cobalt-nickel-iron ions; carrying out hydrothermal reaction to uniformly embed cobalt-nickel ferrite nano-particles into the carbon nanotube by virtue of an electrostatic attraction effect between the metal ions and the oxygen-containing groups so as to effectively improve electromagnetic performance and generate a cobalt-nickel ferrite / carbon nanotube with a good wave-absorbing effect; and finally, dispersing the cobalt-nickel ferrite / carbon nanotube and regenerated paper fibers into a turbid liquid in a high-speed shearing dispersion machine, manufacturing wet paper with pulp, carrying out compaction to remove moisture, flatting a paper web, drying, and carrying out press polishing to increase the smoothness of the paper so as to obtain the ultrathin paper-base wave-absorbing material. The ultrathin paper-base wave-absorbing material has good electromagnetic matching property, is capable of effectively absorbing and inhibiting secondarily-emitted noise waves and has high high-frequency electromagnetic wave shielding performance.
Owner:赵顺全

Magnetic reduction graphene oxide nano composite material and preparation method and application thereof

The invention relates to a magnetic reduction graphene oxide nano composite material and a preparation method and application thereof. The nano composite material comprises reduced graphene oxide andmagnetic nickel ferrite nanocrystalline with the average particle diameter of 6-12 nm uniformly deposited on the surface of the reduced graphene oxide. The method comprises the following steps: uniformly dispersing graphene oxide with deionized water to obtain graphene oxide dispersion liquid; adding divalent nickel salt and trivalent iron salt into the graphene oxide dispersion liquid, and uniformly stirring to obtain a first mixed solution; adding ammonia water into the first mixed solution to adjust the first mixed solution to be alkaline to obtain a second mixed solution; and carrying outhydrothermal treatment on the second mixed solution to obtain the nano composite material. The nano composite material has strong absorption strength, wide absorption bandwidth and double-band microwave absorption performance. The process is simple and convenient, the agglomeration problem of reduced graphene oxide and magnetic small-size nanocrystals can be avoided, and the microwave absorption performance and the effective absorption bandwidth of the composite material are improved.
Owner:BEIJING INST OF ENVIRONMENTAL FEATURES

Nitrogen-doped graphene nickel ferrite composite wave-absorbing material and preparation method thereof

The invention discloses a nitrogen-doped graphene nickel ferrite composite wave-absorbing material and a preparation method thereof. A nitrogen-doped reduced graphene oxide / hexagonal nickel ferrite nano composite material is prepared by taking graphene oxide (GO) as a template, taking ferric nitrate nonahydrate and nickel nitrate hexahydrate as precursors and taking hydrazine hydrate as a nitrogen-doped reagent through a simple one-step hydrothermal method. The nano composite material prepared by the invention is formed by entangling a large number of hexagonal nickel ferrite particles in nanosize by two-dimensional folded graphene, has strong electromagnetic wave absorption capability, wide absorption frequency band and small matching thickness, and can generate double absorption peaks at low frequency (3-6GHz) and high frequency (12-18GHz); and the nitrogen doping amount of graphene in the composite material can be changed by controlling the adding volume of hydrazine hydrate, meanwhile, effective attenuation of the composite material to electromagnetic waves under different wave bands can be achieved by changing the matching thickness, and the composite material has important application value in the fields of electromagnetic wave absorption and electromagnetic shielding.
Owner:安徽理工大学环境友好材料与职业健康研究院(芜湖)

High ductility nickel-free ferrite stainless steel and manufacturing method thereof

The invention relates to a high tenacity non-nickel ferrite stainless steel. The components has the mass percentage that: C occupies 0.03 to 0.08 percent, Si is lower than or equal to 1.0 percent, Mn is lower than or equal to 1.0 percent , S is lower than or equal to 0.030 percent , P is lower than or equal to 0.035 percent, Cr occupies 16 to 21 percent, N occupies 0.01 to 0.03 percent, is lower than or equal to 0.0050 percent, rear earth RE occupies 0.02 to 0.1 percent, and the residual is Fe and inevitable foreign impurities. The utility model provides a manufacture method that: firstly, smelting and casting are performed, the time between the adding of rear earth metal and the steel casting is strictly controlled to be lower than or equal to 25 seconds; the casting temperature is controlled at 1550 plus or minus 5 DEG C; secondly, casting ingot or casting blank cogging is performed, the casting ingot or the casting blank can adopt forging cogging or continuous casting continuous rolling, the heating temperature of the casting ingot or the casting blank is 1150 plus or minus 10 DEG C, and the final forging temperature is not lower than 900 DEG C, and the casting ingot or the casting blank is performed with water cooling. thirdly, steel material rolling is performed, the heating temperature is 1160 plus or minus 10 DEG C, the rolling starting temperature is controlled between 1100 to 1150 DEG C, and the final rolling temperature is controlled to be lower than or equal to 800 DEG C, and the casting ingot or the casting blank is performed air cooling; finally, heat treatment is performed. The invention can obviously lengthen the service life under the low temperature condition, and compared with ultra low carbon and nitrogen and nickel-bearing ferrite stainless steel, the performance-price ratio is high.
Owner:BAOSHAN IRON & STEEL CO LTD
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