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224results about How to "Reduce interfacial energy" patented technology

Preparation method of polycrystalline silicon

The invention discloses a preparation method of polycrystalline silicon. The preparation method of the polycrystalline silicon comprises the following steps: firstly carrying out pre-treatment on a quartz crucible, then paving a crystalline silicon chip material layer at the bottom of the quartz crucible, then placing silicon and mother alloy into the quartz crucible, charging, vacuumizing, and heating to melt silicon; after melting is finished, controlling the temperature of a heater to be 1540-1570 DEG C, lifting a thermal insulation cage until aperture a is 5-20mm, and controlling temperature TC2 to be no more than 1425 DEG C until broken polycrystals at the bottom are just molten, performing a temperature-fall period, and slowly opening the thermal insulation cage while slowly cooling in gradient; finally growing crystals, so that the polycrystalline silicon containing massive twin crystals is formed. A polycrystalline silicon slice prepared by adopting the preparation method is uniform in grain size, the battery efficiency is 0.2-0.3% higher than that of common polycrystalline silicon, the average battery efficiency of the whole silicon slice is more than 17.5%, and ratio of the silicon slice with the efficiency more than 17.4% is more than 65.0%.
Owner:HUNAN RED SUN PHOTOELECTRICITY SCI & TECH

Finishing method of fiber product free of cleaning by detergent

The invention provides a finishing method of a fiber product free of cleaning by a detergent. The technical process comprises singeing, desizing, mercerizing, tentering and preshrinking. The finishing method is characterized in that enzyme piling is added between the singeing and the desizing; a high-efficiency desizing technique is adopted in desizing; liquid ammonia finish and pretreatment are added between the mercerizing and tentering; baking finish is added between the tentering and preshrinking so as to lead the whole technical process to be singeing, enzyme piling, desizing, mercerizing, liquid ammonia finish, pretreatment, tentering, baking and preshrinking. Textiles manufactured by adopting the technique is not cleaned by using the detergent for cleaning, has basically the same cleaning effect with that of cleaning during which the detergent is added, also can not generate secondary dirt in cleaning; and simultaneously, the textile manufactured by using the method has the functions of fouling resistance and easy decontamination, proper oil-proof function, excellent multiple functions of water absorption, air permeability, washing resistance and electrostatic resistance, meets the requirements of people and belongs to an ideal high-grade textile which is energy-saving, environment-friendly and low-carbon.
Owner:LUTAI TEXTILE

Large-proportion methanol gasoline catalyst and preparation method

The invention provides a large-proportion methanol gasoline catalyst and a preparation method thereof. A product mark of the large-proportion methanol gasoline can be expressed by M50 and M85, wherein M represents a first letter of methanol; 50 and 85 respectively represent 50% of methanol and 85% of methanol are added in the gasoline The large-proportion methanol gasoline catalyst is obtained by mixing refined methanol with a purity of 99.9% and national standard gasoline or naphtha and component oil in presence of a special catalyst. A preparation method of the special catalyst is composed of high alcohols (C3-C11), alkanes (C5(C5H12), C6(C6H14), C7(C7H16), C8(C8H18) or CH3NO2), an organic amine, a plurality of esters and auxiliary inhibitors. The large-proportion methanol gasoline produced by the invention passes through a road test longer than 10,000 KM, without changing an engine structure. The large-proportion methanol gasoline is powerful, can be easily started at a low temperature, has no gas block at a high temperature, is not stratified when being contacted with water, can resist rubber swelling, and is low in production cost and flexible in operations. Besides, all project technical indicators are superior to those of national standard gasoline for vehicles. Practice proves that the large-proportion methanol gasoline catalyst has the advantages in a plurality of aspects such as technology, economy, feasibility for large-scale application, and the like, and has obvious competitive advantages as alternative energy.
Owner:杨军

High-damping magnesium alloy containing quasicrystal reinforcing phase and preparation method thereof

InactiveCN101603138ASolute mass decreasedIncrease dampingDislocationAlloy element
The invention discloses a high-damping magnesium alloy containing quasicrystal reinforcing phase and a preparation method thereof. The high-damping magnesium alloy containing quasicrystal reinforcing phase comprises the following alloy components in percentage by weight: 0.9%-1.0% of zinc, 0.15-0.2% of yttrium and 0.6% of zirconium, wherein, zinc and magnesium are industrial pure zinc and industrial pure magnesium; alloy elements, namely, yttrium and zirconium respectively adopt the preliminary alloy form of magnesium-30% of yttrium and magnesium-30% of zirconium to be added in; the high-damping magnesium alloy containing quasicrystal reinforcing phase is prepared by preheating, smelting and shaping. The invention takes zinc, yttrium and zirconium as alloy elements, the atom content ratio of zinc to yttrium in the alloy is controlled to 5-6, so that the formed icosahedron quasicrystal phase has special crystal structure, which ensures the stability of interface combination. The high-damping magnesium alloy containing quasicrystal reinforcing phase of the invention can effectively prevent dislocation slippage and twin crystal expansion, performs favourable strengthening function, effectively overcomes the contradictoriness between the strength and the damping performance in the magnesium base high-damping structure material, has favourable anti-corrosion performance and is a magnesium alloy with comprehensive performance.
Owner:NORTHWESTERN POLYTECHNICAL UNIV

Aluminum-based in-situ composite material formed based on laser 3D printing and preparation method of aluminum-based in-situ composite material

The invention belongs to the technical field of particle-reinforced aluminum-based in-situ composite materials and discloses an aluminum-based in-situ composite material formed based on laser 3D printing and a preparation method of the aluminum-based in-situ composite material. The preparation method includes the steps that a mixture of Al-Si-Mg alloy powder and Al2O3 powder is prepared; the mixture is ball-milled through an intermittent ball-milling process; a three-dimensional CAD model established through a workpiece is subjected to layered slicing treatment; laser beams are adopted for scanning the laid powder line by line to form a two-dimensional section of the workpiece; and the steps are repeated till the workpiece is machined, and the aluminum-based in-situ composite material with an Al2Si4O10 reinforced element scattered on an Al matrix is formed. The operation method is easy and convenient to carry out, Al-Si-Mg alloy and Al2O3 generate the Al2Si4O10 reinforced phase in situ under the effect of high-energy lasers in the laser forming process, the interface wettability is improved, and then the interface strength of the composite material is enhanced.
Owner:NANJING UNIV OF AERONAUTICS & ASTRONAUTICS

Nickel ferrite-copper metal ceramic inert anode material and preparation method

The invention relates to a nickel ferrite-copper metal ceramic inert anode material which comprises a ceramic phase and a metal phase, wherein the ceramic phase is nickel ferrite or nickel ferrite base composite ceramic; and the metal phase consists of metal copper and cuprous oxide, and the cuprous oxide accounts for 1-20% of the total mass of the metal phase. In the preparation process, the content of the cuprous oxide in the metal phase is controlled through controlling the oxygen partial pressure of a nitrogen protection atmosphere so as to improve the wettability of the nickel ferrite and the copper and achieve the sintering infiltration preparation of the ceramic phase and the metal phase. The metal phase and the ceramic phase of the nickel ferrite-copper metal ceramic inert anode material are in a three-dimensional reticular through structure, wherein the sintering density is higher than 98%, the electric conductivity of the metal ceramic material is more than 200S/cm at a temperature of 900 DEG C, the heat conductivity is up to 40W/(m.K) at the room temperature, and the metal ceramic material cannot be cracked through temperature difference thermal shock at the temperature of 400 DEG C. The problems of difficult sintering densification of the nickel ferrite and the copper, sintering overflow of the metal phase and material thermal shock and cracks are effectively solved, and compared with a material prepared by a conventional mixed powder sintering process, the electric conductivity and the thermal shock resistance of the nickel ferrite-copper metal ceramic material are greatly improved.
Owner:CENT SOUTH UNIV

Ingot casting process for high-efficiency polycrystalline silicon

The invention discloses an ingot casting process for high-efficiency polycrystalline silicon. The process comprises the steps of (1) arranged heat-insulating strips below heaters on two sides of an ingot casting furnace; (2) filling a silicon material and an electroactive doping agent into a quartz crucible, and sending the quartz crucible into the ingot casting furnace; (3) heating to completely melt the silicon raw material and the electroactive doping agent; (4) adjusting the temperature of heaters to be in a range of 1425-1440 DEG C at the initial period of crystal growth, quickly opening a heat-insulating bottom plate, and adjusting the opening the heat-insulating bottom plate to be in a range of 1-8cm, wherein a layer of dendritic crystals are grown longitudinally along the bottom of the crucible; and (5) controlling the temperature gradient of a solid-liquid phase at the middle period and the later period of crystal growth, keeping a straight solid-liquid interface with dendritic crystals at the bottom serving as seed crystals, and producing polycrystalline silicon containing a large amount of twin crystals through directional solidification in a vertical upward direction. Polycrystalline silicon chips are produced by the ingot casting process, the battery efficiency is 0.4-0.6% higher than that of ordinary polycrystalline silicon, the average battery efficiency of integrated ingot silicon chips reaches 17.5%, and the maximum efficiency can be up to 18%.
Owner:东海晶澳太阳能科技有限公司 +1

Warm-mixed type water damage resisting asphalt pavement reinforcing agent and preparation method thereof

The invention discloses a warm-mixed type water damage resisting asphalt pavement reinforcing agent which comprises the following components in percentage by mass: 30-60 percent of low molecular weight polyethylene, 30-60 percent of polyethylene oxide, 0-10 percent of an interface compatibilizer and 0-3 percent of an inorganic reinforcing agent. The interface compatibilizer is used for reducing interface energy between the asphalt pavement reinforcing agent and asphalt and aggregate so that the coating capability between an asphalt cementing material and the aggregate is greatly increased and the water damage resistance of an asphalt mixture is improved; when the temperature is reduced below a melting point of the asphalt pavement reinforcing agent, plastic components in the asphalt pavement reinforcing agent are separated out by crystallization; due to a nucleation effect of the inorganic reinforcing agent, the plastic components separated out by crystallization grow radially by taking the inorganic reinforcing agent as center; due to a compatibilization effect of the interface compatibilizer, the plastic components form a good adhered netlike structure with the asphalt and the aggregate, so that the high-temperature stability and high-temperature anti-track performance of the asphalt mixture are greatly improved.
Owner:南京交科瑞路技术有限公司

Carbon dioxide cured prefabricated water-permeable concrete and preparation method thereof

ActiveCN109824321ALow alkalinity requirementLow Pre-Care RequirementsEnvironmental resistanceCellulose
The invention discloses a carbon dioxide cured prefabricated water-permeable concrete and a preparation method thereof. The water-permeable concrete is composed of following components in parts by weight: 55 to 80 parts of regenerated aggregate, 7 to 30 parts of nickel slag sand, 18 to 40 parts of cementing material, 5 to 25 parts of water, 0.01 to 2 parts of naphthalene water reducer, 0 to 0.02 part of cellulose ether, and 0 to 0.01 part of welan gum. The cementing material is composed of following components in parts by weight: 70 to 90 parts of common silicate cement, 5 to 15 parts of fly ash, 10 to 30 parts of steel slag, 5 to 15 parts of lime or lime slag, and 0.02 to 1 part of nano calcium carbonate. The technology is simple, the structure advantage of water-permeable concrete and the properties of industrial byproducts such as nickel slag, steel slag, fly ash, and the like are fully utilized; carbon dioxide curing is utilized to realize rapid, efficient and environmentally friendly production; high strength, durable and water permeable concrete is obtained, the energy consumption is reduced, the industrial tail gas, metallurgy slag, and building waste are effectively utilized, and good economic benefits, social benefits, and environmental benefits are generated.
Owner:SOUTHEAST UNIV

Preparation method for aluminium oxide porous ceramic

InactiveCN103910520AImprove stabilityProlonged collapse timeCeramicwareFreeze-dryingHigh energy
The invention provides a preparation method for aluminium oxide porous ceramic. Freeze drying and direct foaming are combined, a surfactant is utilized for modifying particle surfaces and further for enabling particles to have partial hydrophobicity, and particles with the partial hydrophobicity are utilized for stabilizing foams, so that the porous ceramic with high mechanical strength and relatively more closed pores is obtained. According to the preparation method, propyl gallate is utilized for modifying aluminium oxide particles and further for enabling aluminium oxide particles to have partial hydrophobicity, because solid particles with partial hydrophobicity has extremely high adsorption energy at a gas-liquid interface, the aluminium oxide particles are absorbed at a gas-liquid interface in an almost irreversible form, thus a low-energy-state gas-solid interface replaces the high-energy-state gas-liquid interface, and therefore the interfacial energy is reduced, the foam stability is substantially improved, the foam collapse time is prolonged, the pore structure in a dried blank body is guaranteed to be complete, and also the clear dimension of a sample is guaranteed to be unchanged by utilizing the freeze drying process for drying. The prepared aluminium oxide porous ceramic has the density of 0.35-0.65 g/cm<3>, the porosity of 75-90% and the compressive strength of 1.5-16 MPa.
Owner:ZHENGZHOU UNIV

SiC nanoparticle and SiC whisker hybrid toughened ZrC-based superhigh temperature ceramic composite material and preparation method thereof

The invention discloses a SiC nanoparticle and SiC whisker hybrid toughened ZrC-based superhigh temperature ceramic composite material and a preparation method thereof, relating to a superhigh temperature ceramic composite material and a preparation method thereof. The invention solves the technical problems of low density and high cost of ZrC-based superhigh temperature ceramic in the prior art.The SiC nanoparticle and SiC whisker hybrid toughened ZrC-based superhigh temperature ceramic composite material comprises SiC nanoparticle, SiC whisker and ZrC matrix, wherein, the SiC nanoparticle and SiC whisker as a reinforcing phase exist in the ZrC matrix. The preparation method comprises the following steps: dispersing the SiC whisker through ultrasonic waves, mixing the dispersed SiC whisker with SiC nanoparticle and ZrC powder, then carrying out ball milling and drying, and putting the mixed powder in a graphite die for hot pressed sintering to obtain the SiC nanoparticle and SiC whisker hybrid toughened ZrC-based superhigh temperature ceramic composite material. The prepared SiC nanoparticle and SiC whisker hybrid toughened ZrC-based superhigh temperature ceramic composite material has a density of 96-100 % and low cost, and can be applied in solid rocket engines or superspeed aircrafts.
Owner:HARBIN INST OF TECH

Cleaning agent for treating polymer-containing oil sludge and treatment method thereof

The invention discloses a cleaning agent for treating polymer-containing oil sludge and a treatment method thereof. The cleaning agent is prepared by mixing 0.1-5% of a biological enzyme, 0.1-20% of a polymer digester, 1-5% of a low-density nano material, 1-10% of an alkali, 0.01-2% of an auxiliary agent and water according to the mass ratio. The treatment method comprises the following steps of: (1) putting a certain volume of oil sludge into a stirring and mixing device according to a mud-water ratio set by the water content of the oil sludge; after the biological enzyme, the polymer digester and the low-density nano material are prepared into the cleaning agent, pumping the cleaning agent to the stirring and mixing device; (2) pumping the cleaning agent into the stirring device, and heating the system; (3) starting a stirring and circulating system for stirring, mixing and flushing; (4) allowing flushing liquid to enter an oil-gas-water separation device for oil-gas-water separation, allowing separated oil to enter a collection and transportation system, performing evacuation after escaping gas reaches the standard, allowing the separated cleaning agent to enter a biological nano bubble generation device for recycling; and (5) allowing clean sediment to enter a sediment collection system, or directly discharging after pressure filtration and air drying of the clean sediment.
Owner:菁华绿尔生态环境科技(天津)有限公司

Nitrogen-phosphorus-silicon modified graphene halogen-free flame retardant polymer composite material and preparation method thereof

The invention belongs to the technical field of macromolecular materials, and relates to a nitrogen-phosphorus-silicon modified graphene halogen-free flame retardant polymer composite material and a preparation method thereof, wherein the composite material is prepared from the following substances in parts by weight: 60-90 parts of a polymer, and 10-40 parts of a nitrogen-phosphorus-silicon modified graphene flame retardant. All the components are weighed according to the weight percentage and are mixed uniformly, and then the mixture is added into a twin-screw extruder, melted and mixed andthen subjected to injection molding into corresponding sample strips by an injection moulding machine, or the mixture is melted and blended by an internal mixer and is subjected to compression moulding forming by a mould with a certain size on a plate vulcanizing machine, or a method of solidifying moulding by a curing agent is adopted. The nitrogen-phosphorus-silicon modified graphene halogen-free flame retardant polymer composite material provided by the invention has the advantages of high charring property, and excellent flame retardancy and thermal stability, and can be applied to flame retardancy of materials such as electric cables, automobiles and packages.
Owner:SICHUAN UNIV

SiC-Al3Ti enhanced aluminum-based composite material preparing method

The invention discloses a SiC-Al3Ti enhanced aluminum-based composite material preparing method, and relates to the technical field of aluminum-based composite materials. The problems that in the prior art, SiC particles are prone to being aggregated, the alloy element Mg and the metamorphic element Sr are prone to getting burning losses, and consequently the performance of an aluminum-based composite material is poor are solved. Specifically, high-temperature melt with a SiC-Al3Ti composite powder prefabricated block is prepared, the temperature of the high-temperature melt is 850-900 DEG C,low-temperature melt prepared through pure magnesium, an aluminum copper intermediate alloy and an aluminum strontium intermediate alloy is added in an alloy, the temperature of the low-temperature melt is 580-620 DEG C, then, the low-temperature melt is added in the high-temperature melt, and an aluminum-based composite material is obtained. Due to high-low-temperature mixed treatment, an Al3Ti intermetallic compound can be better formed at the high temperature so that good interface bonding can be kept between SiC and an aluminum base body, and base body grains are refined. According to themethod, the preparing technology is simple in operation, and the comprehensive performance of the aluminum-based composite material can be effectively improved.
Owner:ZHONGBEI UNIV
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