Viscosity-increasable profile control agent and preparation method thereof
A profile control agent and initiator technology, applied in chemical instruments and methods, drilling compositions, etc., can solve the problem that the profile control agent has no viscosity-increasing ability and cannot play a displacing effect, etc., to ensure the strength and expansion performance, The effect of uniform cross-linking structure
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[0036] Example 1:
[0037]
[0038] Dissolve 30.00g of acrylamide in 94.00g of water, add 3.00g of the main crosslinking agent N,N-dimethylacrylamide and 0.52g of lithium magnesium silicate to the acrylamide monomer aqueous solution in turn, stir until it is clear and add 0.12 g of the secondary crosslinking agent polyethylene glycol diacrylate, mixed uniformly to obtain a monomer solution; while uniformly stirring, nitrogen gas was introduced into the polymerization system to remove oxygen for 30 minutes;
[0039] Weigh 0.06g potassium persulfate and dissolve it in 6.00g water to prepare an initiator solution;
[0040] Mix the monomer solution and the initiator solution, and put the mixed reaction solution in a 40°C water bath to react for 10.0 hours, and raise the temperature to 60°C for 8.0 hours to increase the conversion rate;
[0041] The product obtained in the above steps is crushed, and dried in an oven at 60°C to a constant weight;
[0042] The dried product is pulverized wit...
Example Embodiment
[0043] Example 2
[0044]
[0045] Dissolve 30.00g of acrylamide in 94.00g of water, add 1.80g of the main crosslinking agent N,N-dimethylacrylamide and 2.60g of lithium magnesium silicate to the acrylamide monomer aqueous solution in turn, stir until it is clear and add 0.30 g of the secondary crosslinking agent polyethylene glycol diacrylate, mixed uniformly to obtain a monomer solution;
[0046] Weigh 0.06g potassium persulfate and dissolve it in 6.00g water to prepare an initiator solution;
[0047] Mix the monomer solution and initiator solution, and deoxidize with nitrogen for 30 minutes;
[0048] Put the deoxygenated mixed reaction solution into a 40°C water bath to react for 10.0 hours, and raise the temperature to 60°C for 8.0 hours to increase the conversion rate;
[0049] The product obtained in the above steps is crushed, and dried in an oven at 60°C to a constant weight;
[0050] The dried product is pulverized with a 12000r / min universal pulverizer, and the sieving is divi...
Example Embodiment
[0065] Take Example 3 as an example:
[0066] Dissolve 30.00g of acrylamide in 94.00g of water, add 0.90g of the main crosslinking agent N,N-dimethylacrylamide and 1.12g of lithium magnesium silicate to the acrylamide monomer aqueous solution in turn, stir until it is clear and add 0.21 g of the secondary crosslinking agent polyethylene glycol diacrylate, mixed uniformly to obtain a monomer solution;
[0067] Weigh 0.06g potassium persulfate and dissolve it in 6.00g water to prepare an initiator solution;
[0068] Mix the monomer solution and initiator solution, and deoxidize with nitrogen for 30 minutes;
[0069] Put the deoxygenated mixed reaction solution into a 40°C water bath to react for 10.0 hours, and raise the temperature to 60°C for 8.0 hours to increase the conversion rate;
[0070] The product obtained in the above steps is crushed, and dried in an oven at 60°C to a constant weight;
[0071] The dried product is pulverized with a 12000r / min universal pulverizer, and the siev...
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