Feed grade monocalcium phosphate and preparation method thereof
A calcium dihydrogen phosphate, feed-grade technology, applied in chemical instruments and methods, phosphorus compounds, inorganic chemistry, etc., can solve the problems of large equipment, small production capacity, large power consumption, etc., and achieve broad market prospects and production speed. The effect of fast and reduced production time
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Embodiment 1
[0039] A kind of feed grade calcium dihydrogen phosphate, by weight, by 20-30 parts of phosphate rock, 5-15 parts of calcium hydroxide, 5-15 parts of calcium carbonate, 5-15 parts of sulfuric acid, 5-15 parts of industrial waste acid, Activated carbon particles consist of 2-6 parts.
[0040] Described feed grade calcium dihydrogen phosphate and preparation method thereof comprise the following steps:
[0041] (1) Mixing sulfuric acid and waste acid to prepare mixed acid A;
[0042] (2) Mix and react the prepared mixed acid A with phosphate rock, heat and stir for 2-6 hours to obtain phosphoric acid solution B;
[0043] (3) Add activated carbon particles, calcium hydroxide, and 2-4kg of water to the prepared phosphoric acid solution B to defluorinate and remove impurities, and let it stand for 3-5 hours to obtain a clean phosphoric acid solution C;
[0044] (4) Neutralize calcium carbonate with the prepared phosphoric acid solution C, heat to concentrate, filter, wash, and dr...
Embodiment 2
[0046] A feed grade calcium dihydrogen phosphate is composed of 25 parts of phosphate rock, 10 parts of calcium hydroxide, 10 parts of calcium carbonate, 10 parts of sulfuric acid, 10 parts of industrial waste acid and 4 parts of activated carbon particles by weight.
[0047] (1) Mixing sulfuric acid and waste acid to prepare mixed acid A;
[0048] (2) Mix and react the prepared mixed acid A with phosphate rock, heat and stir for 4 hours to obtain phosphoric acid solution B;
[0049] (3) Add activated carbon particles, calcium hydroxide, and 3kg of water to the prepared phosphoric acid solution B to defluorinate and remove impurities, and let it stand for 4 hours to obtain a clean phosphoric acid solution C;
[0050] (4) Neutralize calcium carbonate with the prepared phosphoric acid solution C, heat, concentrate, filter, wash, and dry to obtain the product.
Embodiment 3
[0052] A feed grade calcium dihydrogen phosphate consists of 20 parts by weight of phosphate rock, 5 parts of calcium hydroxide, 5 parts of calcium carbonate, 5 parts of sulfuric acid, 5 parts of industrial waste acid and 2 parts of activated carbon granules.
[0053] (1) Mixing sulfuric acid and waste acid to prepare mixed acid A;
[0054] (2) Mix the prepared mixed acid A with phosphate rock, heat and stir for 2 hours to obtain phosphoric acid solution B;
[0055] (3) Add activated carbon particles, calcium hydroxide, and 2kg of water to the prepared phosphoric acid solution B to defluorinate and remove impurities, and let it stand for 3 hours to obtain a clean phosphoric acid solution C;
[0056] (4) Neutralize calcium carbonate with the prepared phosphoric acid solution C, heat, concentrate, filter, wash, and dry to obtain the product.
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