Flame-retardant degradable antibacterial polylactic acid elastic fiber and preparation method thereof
An elastic fiber, polylactic acid technology, applied in the field of fibers, can solve the problems of the elastic properties to be improved, the hardness is high, the polylactic acid is brittle, etc., and achieves the effects of good flame retardant effect, high elasticity and simple preparation method.
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Embodiment 1
[0018] The flame-retardant and degradable antibacterial polylactic acid elastic fiber provided by the present embodiment comprises 100 parts of polylactic acid, 8 parts of maleic anhydride graft compatibilizer, 2 parts of tert-butyl peroxybenzoate, and 12 parts of antibacterial agent in parts by mass. parts, 6 parts of citric acid, 12 parts of tert-butanol, 5 parts of vinyl polydimethylsilane, 0.3 parts of phosphite, 10 parts of flame retardant; 75 parts of nano zinc oxide, 5 parts of modified activated carbon, wherein said modified activated carbon comprises 80 parts of activated carbon, 5 parts of cerium nitrate, 5 parts of starch, and 10 parts of citric acid solution whose concentration is 3mol / L by mass fraction; The flame retardant includes 20 parts of phosphoric acid ester, 8 parts of cobalt oxide and 25 parts of diammonium phosphate in parts by weight.
[0019] The preparation method of flame-retardant and degradable antibacterial polylactic acid elastic fiber is as fol...
Embodiment 2
[0027] The raw material and preparation method of the flame-retardant and degradable antibacterial polylactic acid elastic fiber provided in this example are roughly the same as those in Example 1, the main difference being that in this example, 14 parts by mass of the flame retardant is used.
[0028] The prepared flame-retardant degradable antibacterial polylactic acid elastic fiber is tested for performance, and the recovery rate under 100% elongation is 96.9%; The inhibition rate of fiber to Escherichia coli and Staphylococcus aureus reaches 99.99%; According to the standard of GB / T5455-1997 "Textile Combustion Performance Test Vertical Method", the flame-retardant and degradable antibacterial polylactic acid provided by this embodiment is measured The LOI of the elastic fiber was 31.0%.
Embodiment 3
[0030] The raw material and preparation method of the flame-retardant and degradable antibacterial polylactic acid elastic fiber provided in this example are roughly the same as those in Example 1, the main difference being that in this example, 18 parts by mass of the flame retardant is used.
[0031] The prepared flame-retardant degradable antibacterial polylactic acid elastic fiber is tested for performance, and the recovery rate under 100% elongation is 96.9%; The inhibition rate of fiber to Escherichia coli and Staphylococcus aureus reaches 99.99%; According to the standard of GB / T5455-1997 "Textile Combustion Performance Test Vertical Method", the flame-retardant and degradable antibacterial polylactic acid provided by this embodiment is measured The LOI of the elastic fiber was 31.9%.
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