Preparation method of transition metal phosphide nano hollow spheres
A transition metal, phosphide technology, applied in the direction of phosphide, can solve the problems of many by-products, expensive raw materials, unsuitable operation, etc., and achieve the effects of large specific surface area, mild reaction conditions and stable structure
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Embodiment 1
[0022] (1) Weigh 20mg of cobalt oxide nanospheres and disperse them in 50mL of ethylene glycol solvent;
[0023] (2) Add 100 mg of sodium hypophosphite to the dispersion obtained in step (1), and react in an oil bath at 100° C. for 12 hours;
[0024] (3) The product obtained in step (2) is washed with water and ethanol by suction filtration for several times, and vacuum-dried at 60° C.;
[0025] (4) Etching the product obtained in step (3) for 12 hours at 20°C in a 1mol / L hydrochloric acid solution;
[0026] (5) The product obtained in step (4) is centrifuged, washed with water, and vacuum-dried at 60° C. to obtain transition metal cobalt phosphide hollow spheres.
Embodiment 2
[0028] (1) Weigh 40mg of nickel oxide nanospheres and disperse them in 50mL of ethylene glycol solvent;
[0029] (2) Add 100 mg of sodium hypophosphite to the dispersion obtained in step (1), and react in an oil bath at 100° C. for 12 hours;
[0030] (3) The product obtained in step (2) is washed with water and ethanol by suction filtration for several times, and vacuum-dried at 60° C.;
[0031] (4) Etching the product obtained in step (3) for 12 hours at 40°C in a 1mol / L sulfuric acid solution;
[0032] (5) The product obtained in step (4) is centrifuged, washed with water, and vacuum-dried at 60° C. to obtain transition metal nickel phosphide hollow spheres.
Embodiment 3
[0034] (1) Weigh 60mg of manganese oxide nanospheres and disperse them in 50mL of ethylene glycol solvent;
[0035] (2) Add 100 mg of sodium hypophosphite to the dispersion obtained in step (1), and react in an oil bath at 100° C. for 12 hours;
[0036] (3) The product obtained in step (2) is washed with water and ethanol by suction filtration for several times, and vacuum-dried at 60° C.;
[0037] (4) Etching the product obtained in step (3) for 12 hours at 20°C in a 1mol / L hydrochloric acid solution;
[0038] (5) The product obtained in step (4) is centrifuged, washed with water, and dried under vacuum at 60° C. to obtain transition metal manganese phosphide hollow spheres.
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