Preparation method for modified organosilicon fabric coating agent

A silicone and coating agent technology, applied in textiles and papermaking, liquid repellent fibers, fiber treatment, etc., can solve the problems of difficulty in meeting the development needs of fabric coatings, low adhesion, poor water resistance, etc. High color fastness, high adhesion, good water resistance

Active Publication Date: 2017-08-11
WEIFANG JIACHENG DIGITAL MATERIAL CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The technical problem to be solved by the present invention is to provide a modified organosilicon fabric coating agent for the problems of low adhesion between the traditional fabric coating agent and the fabric, poor water resistance, and difficulty in meeting the development needs of fabric coating finishing. preparation method

Method used

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Examples

Experimental program
Comparison scheme
Effect test

example 1

[0020] Take 180g of allyl glycidyl ether, 150g of terminal hydrogen-containing silicone oil, and 6g of 0.1% isopropanol solution of chloroplatinic acid by mass fraction, put them into a three-necked flask, stir and mix evenly at 400r / min, and heat to 85°C, keep React at temperature for 5 hours to obtain a modified silicone oil mixture; take 240g of triethanolamine and 100g of glacial acetic acid and mix evenly, add to the modified silicone oil mixture, stir and mix at 400r / min for 20min, then heat to 80°C for 5 hours to obtain a reaction solution , put the reaction solution into a vacuum distillation device and distill under reduced pressure for 5h, then cool to room temperature and discharge to obtain polyether modified silicone oil; mix polyether modified silicone oil with 6g mass fraction of 0.1% isopropyl chloroplatinate The alcohol solution was put into a three-necked flask, stirred at 400r / min for 30min under a nitrogen atmosphere, then heated to 105°C, and at the same ti...

example 2

[0022] Take 120g of allyl glycidyl ether, 100g of terminal hydrogen-containing silicone oil, and 5g of isopropanol solution with a mass fraction of 0.1% chloroplatinic acid, put them into a three-necked flask, stir and mix evenly at 300r / min, and heat to 80°C, keep React at temperature for 4 hours to obtain a modified silicone oil mixture; take 150g of triethanolamine and 80g of glacial acetic acid and mix evenly, add to the modified silicone oil mixture, stir and mix at 300r / min for 15min, then heat to 70°C for 4 hours to obtain a reaction solution , put the reaction liquid into a vacuum distillation device and distill under reduced pressure for 3h, then cool to room temperature and discharge to obtain polyether modified silicone oil; mix polyether modified silicone oil with 5g mass fraction of 0.1% isopropyl chloroplatinate The alcohol solution was put into a three-necked flask, stirred at 300r / min for 20min under a nitrogen atmosphere, then heated to 100°C, and at the same t...

example 3

[0024] Take 160g of allyl glycidyl ether, 120g of terminal hydrogen-containing silicone oil, and 5g of isopropanol solution with a mass fraction of 0.1% chloroplatinic acid, put them into a three-necked flask, stir and mix evenly at 350r / min, and heat to 82°C, keep React at temperature for 4 hours to obtain a modified silicone oil mixture; take 220g of triethanolamine and 90g of glacial acetic acid and mix evenly, add to the modified silicone oil mixture, stir and mix at 350r / min for 17min, then heat to 75°C for 5 hours to obtain a reaction solution , put the reaction liquid into a vacuum distillation device and distill under reduced pressure for 4h, then cool to room temperature and discharge to obtain polyether modified silicone oil; mix polyether modified silicone oil with 5g mass fraction of 0.1% isopropyl chloroplatinate The alcohol solution was put into a three-necked flask, stirred at 350r / min for 25min under a nitrogen atmosphere, then heated to 103°C, and at the same t...

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Abstract

The invention specifically relates to a preparation method for a modified organosilicon fabric coating agent, belonging to the technical field of textile chemicals. The preparation method comprises the following steps: subjecting allyl glycidyl ether and silicone oil containing hydrogen at its terminal to a heating reaction and then carrying out modification with triethanolamine so as to synthesize quaternary ammonium salt-modified polyether organosilicon oil; then subjecting the modified organosilicon oil, butyl acrylate and ethylene glycol dimethacrylate to polymerization to produce an acrylate emulsion so as to obtain self-adhesive organosilicon oil; and subjecting the self-adhesive organosilicon oil, glass microspheres, water and other substances to shearing and dispersion. The modified organosilicon fabric coating agent prepared in the invention has high adhesion on a fabric, high color fastness and good water resistance and meets the development demands of finishing of fabric coatings.

Description

technical field [0001] The invention belongs to the technical field of textile chemical industry, and in particular relates to a preparation method of a modified organosilicon fabric coating agent. Background technique [0002] In recent years, the development of functional textiles has been extremely rapid, mainly in climate adaptation functions (such as temperature maintenance, waterproof and moisture-permeable, windproof and water-repellent, etc.), protective functions (flame retardant, antistatic, heat insulation, radiation protection, etc.), hygienic Health care and medical functions (such as antibacterial, antifouling, health care and skin care, etc.) and sports and leisure functions (such as softness, elasticity, moisture absorption and heat dissipation, etc.), and fabric coating finishing is a newly developed processing technology in textile finishing. It is mainly to uniformly coat a layer of polymer compound that can form a film on the surface of the fabric. Becaus...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06M15/263D06M11/00D06M11/79C08F283/12C08F220/18C08F222/14C08G77/388C08G77/38
CPCD06M11/00D06M11/79D06M15/263C08F283/122C08G77/38C08G77/388D06M2200/12C08F222/102C08F220/1804
Inventor 薛洋杨阳
Owner WEIFANG JIACHENG DIGITAL MATERIAL CO LTD
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