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Method for recycling side product in S-abscisic acid production

A by-product, inducer technology, applied in the field of S-induced resistin production technology, can solve the problems of high cost, high production cost, low purity, etc., to reduce pollution and waste, reduce pollutant discharge, and increase economic benefits Effect

Inactive Publication Date: 2017-08-18
SICHUAN LOMON BIO TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The direct extraction method refers to direct extraction from plants, but due to the low content in the plant body, the production method has a low yield and a small scale; the chemical synthesis method prepares S-antibodies, and its synthetic purity is low, because The products obtained by chemical synthesis are non-natural abscisic acid and natural abscisic acid (S-abscisic acid), only natural abscisic acid (S-abscisic acid) has the above physiological activities, and the production cost of chemical synthesis is extremely high, so the current Only Japan, the United States and other developed countries are used in large-scale agricultural production; the S-abscisin produced by the biological fermentation method has a high yield and will not produce unnatural abscisic acid. It will produce a large number of by-products, which also contain a certain amount of S-inducer, which are all discharged and wasted. The cost is high, the pollution is serious, and it is not suitable for industrial production.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0033] A method for recycling by-products in the production of S-antigen described in this embodiment comprises the following steps:

[0034] (1) The first by-product is obtained by filtering the fermented liquid containing S-antibiotics through a plate frame, which is flash-dried, pulverized, and compounded. The first by-product formed after compounding contains 1.0% of S-antibiotics , its components include the first by-product and auxiliary agent, wherein the ratio of the first by-product and auxiliary agent is 100:3, wherein the auxiliary agent is amino acid, copper, iron, manganese, zinc, boron, molybdenum, titanium, red Mycin, indolebutyric acid, cytokinin.

[0035] (2) The filtrate obtained after plate and frame filtration is subjected to membrane filtration and acid analysis to obtain the second by-product, which is evaporated and concentrated at a temperature of 60°C and then compounded. The second by-product formed after compounding contains 80% S-inducible Its comp...

Embodiment 2

[0038] A method for recycling by-products in the production of S-antigen described in this embodiment comprises the following steps:

[0039] (1) The first by-product is obtained by filtering the fermented liquid containing S-antibiotics through a plate frame, which is flash-dried, pulverized, and compounded, and the first by-product formed after compounding contains 0.2% of S-antibiotics , its components are: the first by-products, additives, wherein the ratio of the first by-products and additives is 100:1, wherein the additives are amino acids, humic acid, copper, iron, manganese, zinc, boron, molybdenum , titanium, brassinolide, naphthaleneacetic acid, 2,4-D, chlormequat.

[0040] (2) The filtrate obtained after plate and frame filtration is subjected to membrane filtration and acid analysis to obtain the second by-product, which is evaporated and concentrated at a temperature of 40°C and then compounded. The second by-product formed after compounding contains 70% of S-ind...

Embodiment 3

[0043] A method for recycling by-products in the production of S-antigen described in this embodiment comprises the following steps:

[0044] (1) The first by-product is obtained by filtering the fermented liquid containing S-antibiotics through plate and frame, and compounded after flash drying and pulverization. The first by-product formed after compounding contains 2.5% of S-antibiotics , its components are: the first by-product, auxiliary agent, wherein the ratio of the first by-product and auxiliary agent is 10:1, wherein the auxiliary agent is biochemical fulvic acid, amino acid, copper, iron, manganese, zinc, boron , molybdenum, titanium, 2,4-D, chlormequat, paclobutrazol.

[0045] (2) The filtrate obtained after plate and frame filtration is subjected to membrane filtration and acid analysis to obtain the second by-product, which is evaporated and concentrated at a temperature of 80°C and then compounded. The second by-product formed after compounding contains 90% of S...

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PUM

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Abstract

The invention discloses a method for recycling a side product in S-abscisic acid production. The recycling method comprises the following steps: (1) filtering a fermentation liquid containing S-abscisic acid with a plate frame to obtain a first side product and filtrate, and drying, smashing and compounding the first accessory substance to obtain a first byproduct; (2) performing film filtration and acid precipitation on the filtrate obtained in the step (1) to obtain a second accessory substance and an acid precipitation substance, and concentrating and compounding the second accessory substance to obtain a second byproduct; (3) performing extraction, concentration crystallization and recrystallization on the acid precipitation product obtained in the step (2) to obtain a third accessory substance and an S-abscisic acid crystal, and performing back extraction, drying and compounding on the third accessory substance to obtain a third byproduct. By adopting the method, a production line is enriched, the economical benefit is increased, emission of relatively expressive S-abscisic acid is avoided, pollution and waste are reduced, energy is saved, and emission is reduced.

Description

technical field [0001] The invention relates to the technical field of S-induced antibiotic production technology, in particular to a method for recycling by-products in the production of S-induced antibiotic. Background technique [0002] S-abscisic acid (natural abscisic acid), together with auxin, ethylene, gibberellin, and cytokinin, is listed as the five natural growth regulators of plants. Reverse gene, induces and activates the anti-stress immune system in plants, improves the plant's own resistance to cold, drought, pests, and salinity, and can reduce the use of chemical pesticides by applying S-absorbin, which can improve the quality of agricultural products, etc. It has important physiological activity and application value in many aspects. [0003] At present, there are three main methods for the preparation of S-antibodies: direct extraction, chemical synthesis, and biological fermentation. The direct extraction method refers to direct extraction from plants, b...

Claims

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Application Information

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IPC IPC(8): A01N25/12A01N37/42A01P21/00C07C51/42C07C59/90C05G3/00
CPCA01N25/12A01N37/42C05C11/00C05G3/00C07C51/42C07C59/90C05D9/02C05F9/04C05F11/02C05F11/10
Inventor 刘健熊仁科谭虎左建英侯永春
Owner SICHUAN LOMON BIO TECH CO LTD