A kind of preparation method of safe and environment-friendly alcohol-free fountain solution
A safe, environmentally friendly, alcohol-free technology, applied in the preparation and printing of printing surfaces, can solve the problems of reducing surface tension, adverse environmental effects, corrosion of metal parts, etc., to prevent microbial contamination, strong microbial killing, and prevent being The effect of corrosion
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example 1
[0017] Weigh 50g of protein powder and add it to a flask containing 400mL of 10% hydrochloric acid, and place the flask in an oil bath, control the temperature at 95℃, stir and hydrolyze for 2h to obtain a protein hydrolysate. Filter, collect the filtrate, and add 15% sodium hydroxide solution to the filtrate to adjust the pH to 6.5 to obtain an amino acid solution for use; weigh 30g of lauric acid and add it to a three-necked flask containing 100mL of dichloromethane, and add Place the flask in a water pot, control the temperature at 20°C, and then add 40 mL of thionyl chloride dropwise. The addition is completed within 10 minutes. After the addition is complete, stir for 2 minutes, and then add 0.3 mL of N,N-dimethylformamide , Heat up to 70℃, continue to stir the reaction for 2h, transfer the product to a rotary evaporator, and rotary evaporate to 1 / 5 of the original volume to obtain a concentrated solution; add the spare amino acid solution to the three ports with thermomete...
example 2
[0020] Weigh 60g of protein powder and add it to a flask containing 500mL of 10% hydrochloric acid, and place the flask in an oil bath, control the temperature at 100℃, stir and hydrolyze for 3 hours to obtain a protein hydrolysate. Filter, collect the filtrate, and add 15% sodium hydroxide solution to the filtrate to adjust the pH to 6.5 to obtain an amino acid solution for use; weigh 40g of lauric acid and add it to a three-necked flask containing 120mL of dichloromethane, and add Place the flask in a water pot, control the temperature at 25°C, and then add 50 mL of thionyl chloride dropwise. The addition is completed within 15 minutes. After the addition is complete, stir for 3 minutes, and then add 0.5 mL of N,N-dimethylformamide , Warm up to 80°C, continue to stir and react for 3h, transfer the product to a rotary evaporator, and rotary evaporate to 1 / 5 of the original volume to obtain a concentrated solution; add the spare amino acid solution to the three ports with thermo...
example 3
[0023] Weigh 55g of protein powder and add it to a flask containing 450mL of 10% hydrochloric acid, and place the flask in an oil bath, control the temperature at 98°C, stir and hydrolyze for 3 hours to obtain a protein hydrolysate. Filter, collect the filtrate, and add 15% sodium hydroxide solution to the filtrate to adjust the pH to 7.0 to obtain an amino acid solution for use; weigh 35g of lauric acid and add it to a three-necked flask containing 110mL of dichloromethane, and add Place the flask in a water pot, control the temperature at 23°C, and then add 45 mL of thionyl chloride dropwise. The addition is completed within 13 minutes. After the addition is complete, stir for 3 minutes, and then add 0.4 mL of N,N-dimethylformamide , Heat up to 75℃, continue to stir and react for 3h, transfer the product to a rotary evaporator, and rotary evaporate to 1 / 5 of the original volume to obtain a concentrated solution; add the spare amino acid solution to the three ports with thermom...
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