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A kind of cold pad batch decolorization method of colored wool

A cold pad-batch and colored technology, which is applied in textiles and papermaking, can solve the problems of reducing the color residue rate of purple velvet, high cost, and difficulty in recycling, so as to improve the solubility of pigments, reduce strong damage, and solve the effects of large water consumption

Active Publication Date: 2020-06-12
WUHAN TEXTILE UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, its disadvantage is that the decolorization time is longer and the decolorization temperature is higher
However, its disadvantage is that this method does not improve the fluff strength
Although it uses organic solvents such as 3-butoxyl-1-propanol to carry out pickling fumigation and decolorization of purple velvet, it does reduce the color residual rate of velvet, but its disadvantage is that its pickling solution and decolorization There are many types of organic solvents and other chemical additives used in the liquid, the preparation is more complicated, the recovery is difficult, and the cost is high
Although it adopts pigment separation and protection, purple velvet protection and stabilization, purple velvet reduction bleaching, and the decolorization method of purple velvet reduction protection have indeed played a role in simplifying the decolorization process and reducing production costs, but its disadvantage is that in the decolorization process it needs Add special T1 pigment separation agent, T2 wool protection agent, T4 complexing agent, T5 oxidation stabilizer, etc., the formula is more complicated
Although it adopts the decolorization method of pickling, pretreatment, oxygen bleaching and reduction bleaching to improve the whiteness of green velvet and reduce the strong damage, its disadvantage is that a certain concentration of sericin and sericin must be added in the decolorization process. Organic phosphonic acid and its sodium salt increase the cost to a certain extent and have certain limitations

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0065] According to the above process steps: select 1g green velvet for cold pad batch decolorization, place ferrous sulfate and penetrating agent in the mixed solution of ethanol and water, stir evenly to prepare the pretreatment solution, the bath ratio of the pretreatment solution is 1:10, The volume ratio of ethanol and water in the pretreatment solution is 95%:5%, the concentration of mordant is 1g / L, and the concentration of penetrant is 0.5g / L. Place the green velvet in the pretreatment solution for pretreatment, the temperature of the pretreatment solution is 35°C, and the treatment time is 10 minutes. Mix ethanol and water evenly to prepare washing liquid, and the volume ratio of ethanol and water in the washing liquid is 50%:50%. The pretreated green velvet is placed in the washing solution for pre-washing. The temperature of the washing solution is 30° C., and the washing time is 1 minute. The liquid-carrying rate of the colored velvet after washing is 70%. Put hyd...

Embodiment 2

[0067] According to the above process steps: select 1g of purple velvet for cold pad-batch decolorization, place copper sulfate and penetrating agent in the mixed solution of n-propanol and water, stir evenly to prepare the pretreatment solution, the bath ratio of the pretreatment solution is 1:100, The volume ratio of alcoholic organic solvent and water in the pretreatment liquid is 50%:50%, the concentration of mordant is 15g / L, and the concentration of penetrant is 5g / L. Put the purple velvet to be pretreated in the pretreatment solution for pretreatment, the temperature of the pretreatment solution is 75°C, and the treatment time is 60 minutes. Mix n-propanol and water evenly to prepare washing liquid, and the volume ratio of n-propanol and water in the washing liquid is 10%:90%. The pretreated purple velvet is placed in the washing solution for pre-washing. The temperature of the washing solution is 50° C., and the washing time is 10 minutes. The liquid-carrying rate of t...

Embodiment 3

[0069] According to the above process steps: select 1g of camel hair for cold pad batch decolorization, place cobaltous sulfate and penetrating agent in the mixed solution of isopropanol and water, stir evenly to prepare the pretreatment solution, the bath ratio of the pretreatment solution is 1:50, The volume ratio of isopropanol and water in the pretreatment liquid is 70%:30%, the concentration of cobaltous sulfate is 5g / L, and the concentration of penetrant is 2g / L. The camel hair to be pretreated is placed in the pretreatment solution for pretreatment, the temperature of the pretreatment solution is 50° C., and the treatment time is 30 minutes. Mix isopropanol and water evenly to prepare a washing liquid, and the volume ratio of isopropanol to water in the washing liquid is 30%:70%. Put the camel hair in the washing solution for pre-washing, the temperature of the washing solution is 40° C., and the washing time is 5 minutes. The liquid-carrying rate of the camel hair afte...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Abstract

The invention relates to a colored velvet cold-pad batch decolorizing method, and belongs to a pretreatment process technology of textile printing and dyeing. By changing a colored velvet decolorizing process route and a preparation method of a decolorizing solution and performing cold-pad batch decolorizing on colored velvet by use of a solution prepared by mixing high-proportion ethanol and a little water with a decolorizing reagent, strength damage to the colored velvet can be effectively reduced in a decolorizing process, the pigment solubility is improved, and the decolorizing difficulty is reduced; meanwhile, the water consumption and sewage discharge are reduced to a great extent, the quality of the colored velvet is improved, and the quality is good and the efficiency is high. The cold-pad bath decolorizing technology provided by the invention is simple and convenient and realizes a good decolorizing effect and high efficiency; through recycling of an alcohol organic solvent, the burden of sewage treatment on an enterprise is remarkably reduced; the cold-pad bath decolorizing technology is a clean production technology conforming to the environmental protection requirement, and has remarkably high social and economic benefits.

Description

technical field [0001] The invention relates to a cold pad-batch decolorization method for colored cashmere, which belongs to the pretreatment technology of textile printing and dyeing. Background technique [0002] Among the animal fibers, quite a few fibers have natural color, especially some special animal fibers with large output in China, such as purple cashmere, green cashmere, yak hair, camel hair and so on. Among them, cashmere is a precious natural protein fiber and a valuable raw material in the textile industry, known as "the crown of fibers", "the king of wool" and "soft gold". In addition, the fineness of cashmere is mostly 13-17 μm, the unevenness of fineness is small, and the length is between 21-40 mm. It has excellent characteristics such as fine fiber fineness, soft hand feeling, lightness, warmth retention and natural luster. Camel hair is also an important textile raw material, which has the characteristics of high elasticity, soft touch and good luster....

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D06L4/13D06L4/12D06L4/30
Inventor 徐卫林张春华朱坤迪徐文昉王运利
Owner WUHAN TEXTILE UNIV
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