Preparation method of dacron fabric compound antistatic agent
A technology of composite antistatic agent and polyester fabric, which is applied in the field of preparation of polyester fabric composite antistatic agent, can solve the problems affecting polyester fabric dyeing, polyester fiber discoloration, friction coefficient increase, etc., to achieve increased smoothness and small foaming , Good antistatic effect
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example 1
[0020] According to the mass ratio of 10:1, add absolute ethanol and phosphorus pentoxide into the four-necked flask, put it in an ice-water bath, stir and mix at 5°C for 20 minutes, and after mixing, move the four-necked flask into a water bath and heat to Seal the four-necked flask after 70°C, stir and react for 3 hours. After the reaction, add 10% deionized water of absolute ethanol quality dropwise to the four-necked flask. After finishing, cool to room temperature and discharge to obtain reaction solution 1; in parts by weight, weigh 15 parts of dimethyl diallyl ammonium chloride, 10 parts of hydroxyethyl acrylate, 4 parts of azobisisobutyl Nitrile and 200 parts of n-butanol, mix and raise the temperature to 85°C, heat and stir for 30 minutes to obtain a mixed solution, add dropwise the reaction solution 1 with 55% of the mixed solution mass in the mixed solution, and control the dripping in 50 minutes. Stir at a speed of 800r / min; continue to stir and react for 5 hours a...
example 2
[0022] According to the mass ratio of 10:1, add absolute ethanol and phosphorus pentoxide into the four-necked flask, put it in an ice-water bath, stir and mix at 0°C for 10 minutes, and after mixing, move the four-necked flask into a water bath and heat to Seal the four-necked flask after 50°C, stir and react for 2 hours. After the reaction, add 5% deionized water of absolute ethanol quality to the four-necked flask dropwise, and control the dropping rate to 1 drop / s. After the addition, stir and react for 60 minutes. After finishing, cool to room temperature and discharge to obtain reaction solution 1; in parts by weight, weigh 10 parts of dimethyl diallyl ammonium chloride, 8 parts of hydroxyethyl acrylate, 2 parts of azobisisobutyl Nitrile and 100 parts of n-butanol, mix and raise the temperature to 80°C, heat and stir for 20 minutes to obtain a mixed solution, add dropwise to the mixed solution 55% of the mixed solution mass reaction solution 1, control the dripping in 40 ...
example 3
[0024]According to the mass ratio of 10:1, add absolute ethanol and phosphorus pentoxide into the four-necked flask, put it in an ice-water bath, stir and mix at 2°C for 15 minutes, and after mixing, move the four-necked flask into a water bath and heat to Seal the four-necked flask after 60°C, stir and react for 2 hours. After the reaction, add 7% deionized water of absolute ethanol quality to the four-necked flask dropwise, control the dropping rate at 1 drop / s, and stir for 70 minutes after the addition. After finishing, cool to room temperature and discharge to obtain reaction solution 1; in parts by weight, weigh 12 parts of dimethyl diallyl ammonium chloride, 9 parts of hydroxyethyl acrylate, 3 parts of azobisisobutyl Nitrile and 150 parts of n-butanol, mix and raise the temperature to 82°C, heat and stir for 25 minutes to obtain a mixed solution, add dropwise to the mixed solution 52% of the mixed solution quality reaction solution 1, control the dripping in 45 minutes, ...
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