A kind of laminated flexible electrode sheet and preparation method thereof
A flexible electrode and pole piece technology, applied in the field of electrochemistry, can solve the problems of low capacity and insufficient cycle of lithium batteries, and achieve the effects of improving flexibility, improving thickness and increasing energy density
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[0034] The preparation method of the laminated flexible electrode sheet in the present invention includes the following steps:
[0035] (1) Dispersion: Use organic solvent or deionized water as the solvent for the conductive agent, and ultrasonically disperse at a dispersion concentration of 0.1-2mg / ml to form a conductive agent slurry; use organic solvent or deionized water as the solvent for the fiber body, high speed Stirring dispersion, the dispersion concentration is 0.5-3mg / ml; among them, the organic solvent is ethanol, ethylene glycol, propanol, N-methylpyrrolidone, isopropanol.
[0036] (2) Stir and homogenize: add the binder to the conductive agent slurry in step (1) and disperse for 2 to 3 minutes, then add the active material, mix thoroughly, and then add the fibers dispersed in step (1) And then mix thoroughly to form a suspension slurry.
[0037] (3) Pour the suspended slurry obtained in step (2) into a suction filter device containing filter paper. The filter paper is...
Embodiment 1
[0042] In this embodiment, the active material is lithium cobalt oxide, the fiber material is nanocellulose, the conductive agent is carbon nanotubes, the mass ratio of the three is 99.7:0.1:0.2, and the area density of the active material is 20 mg / cm. 2 . First, disperse nanocellulose in isopropanol at high speed, disperse carbon nanotubes in isopropanol ultrasonically for 20 minutes, with a volume ratio of 0.6 mg / ml. After dispersion, add lithium cobalt oxide to the conductive agent slurry and disperse at high speed for 10 minutes. After mixing uniformly, add the dispersed nano cellulose, and continue to stir at high speed to form a uniform suspension slurry. Then, pour the suspension slurry into a cellulose filter paper with a pore size of 2 microns for vacuum filtration. Remove the isopropanol to form a film. The sample after the film is baked in a 130 degree oven to remove the remaining isopropanol, and the dried self-supporting pole piece substrate can be easily transferre...
Embodiment 2
[0045] In this embodiment, the active material is lithium manganate, the fibrous material is nanocellulose, the conductive agent is graphene, and the cushion material is nanocellulose. The mass ratio is 89:5:5:1. The surface of the active material is The density is 15mg / cm 2 . First, disperse the fibrous material at high speed in N-methyl-2-pyrrolidone (NMP). The carbon nanotubes are dispersed in NMP ultrasonically for 10 minutes at a volume ratio of 0.5mg / ml. Add lithium manganate to the conductive agent slurry and disperse it at high speed for 6 minutes until uniformly mixed, then add the dispersed fiber material, and continue to stir at high speed to form a uniform suspension slurry; secondly, combine the cushion material and N-methylpyrrolidone at high speed Disperse for 5min, with an areal density of 1mg / cm 2 Prepare the cushion suspension, then pour the cushion suspension into a cellulose filter paper with a pore size of 50 microns for vacuum filtration. When the cushion ...
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