Weak solvent ink absorption flame retardant coating and preparation method thereof
A technology of absorbing coating and flame-retardant coating, which is applied in the field of materials, can solve problems such as unsafe, toxic smoke, and slow volatilization of weak solvents, and achieve the effects of good flame retardancy, enhanced ink absorption ability, and simple preparation methods
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Embodiment 1
[0032] (1) According to the formula, weigh the following components:
[0033]
[0034] The addition ratio of the above-mentioned composite combustion-supporting agent is: melamine modified ammonium polyphosphate, decabromodiphenylethane, and antimony trioxide in a mass ratio of 2:3:1.
[0035] (2) Add 2 / 3 weight of emulsifier, acrylic acid, methacrylic acid, lauryl methacrylate, methyl acrylate, ethyl acrylate, butyl acrylate, methyl methacrylate, butyl methacrylate Ester, 2-hydroxypropyl acrylate and 1 / 3 of the initiator by weight are added to the water at a water-oil ratio of 2-0.6:1, and stirred at high speed for 30 minutes;
[0036] (3) Stir the remaining 1 / 3 weight of the emulsifier and the remaining 2 / 3 weight of the initiator to form a mixed emulsion;
[0037] (4). The reaction system of step (2) is heated to 82°C, the mixed emulsion in step (3) is added dropwise, and the dripping is completed in 3 hours; the temperature is raised to 86°C, and the temperature is kept for 1 hour...
Embodiment 2
[0041] (1) According to the formula, weigh the following components:
[0042]
[0043] The addition ratio of the above-mentioned composite combustion-supporting agent is: melamine modified ammonium polyphosphate, decabromodiphenylethane, and antimony trioxide in a mass ratio of 2:3:1.
[0044] (2) Add 2 / 3 weight of emulsifier, acrylic acid, methacrylic acid, lauryl methacrylate, methyl acrylate, ethyl acrylate, butyl acrylate, methyl methacrylate, butyl methacrylate Ester, 2-hydroxypropyl acrylate and 1 / 3 weight of sodium sulfate are added to water at a water-oil ratio of 2-0.6:1, and stirred at high speed for 30 minutes;
[0045] (3) Stir the remaining 1 / 3 weight of emulsifier and the remaining 2 / 3 weight of sodium sulfate to form a mixed emulsion;
[0046] (4). The reaction system of step (2) is heated to 80°C, the mixed emulsion in step (3) is added dropwise, and the addition is completed in 4 hours; the temperature is raised to 86°C, and the temperature is kept for 1 hour.
[0047]...
Embodiment 3
[0050] (1) According to the formula, weigh the following components:
[0051]
[0052]
[0053] The addition ratio of the above-mentioned composite combustion-supporting agent is: melamine modified ammonium polyphosphate, decabromodiphenylethane, and antimony trioxide in a mass ratio of 2:3:1.
[0054] (2) Add 2 / 3 weight of emulsifier, acrylic acid, methacrylic acid, lauryl methacrylate, methyl acrylate, ethyl acrylate, butyl acrylate, methyl methacrylate, butyl methacrylate Ester, 2-hydroxypropyl acrylate and 1 / 3 weight of sodium sulfate are added to water at a water-oil ratio of 2-0.6:1, and stirred at high speed for 30 minutes;
[0055] (3) Stir the remaining 1 / 3 weight of emulsifier and the remaining 2 / 3 weight of sodium sulfate to form a mixed emulsion;
[0056] (4) The reaction system of step (2) is heated to 80°C, the mixed emulsion in step (3) is added dropwise, and the dripping is completed in 3 hours; the temperature is raised to 86°C, and the temperature is kept for 1 hour....
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